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Caking Index Determination Apparatus Spare Parts and Consumables for Coal Quality Testing

Assay Equipment Accessories & Consumables

Caking Index Determination Apparatus Spare Parts and Consumables for Coal Quality Testing

Item Number : KT-ZJ

Price varies based on specs and customizations


Applicable Test Standards
GB/T 5447, GB/T 14181-2010
Static Compaction Force
6.5 kg (Nominal Pressure)
Crucible Specification
30 mL (Ø40 mm Top × Ø20 mm Base × 40 mm Height)
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Product Overview

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This specialized suite of caking index determination apparatus spare parts provides certified hardware and calibrated consumables engineered for standardized coal adhesiveness and plastic mass evaluation. Designed to uphold analytical repeatability, this component ecosystem ensures precise sample preparation, uniform static consolidation, and dependable thermal carbonization during critical coal quality assessments.

Engineered for demanding industrial workflows, these spare parts support coke production plants, metallurgical steel facilities, commercial inspection agencies, and geological research laboratories. The complete assembly supplies all necessary replacement elements to formulate standardized coal-anthracite mixtures, execute static compaction, and conduct rapid high-temperature volatile matter expulsion.

Each replacement item is fabricated to withstand severe thermal cycling, corrosive volatile vapors, and abrasive mechanical wear. By maintaining strict compliance with established coal testing standards, this equipment eliminates analytical variances, protects test validity, and ensures dependable long-term laboratory operation.

Key Features

  • Certified Standard Anthracite Reference Material: Sourced exclusively from the lower slice of the designated No. 2-1 coal seam within the Ningxia Rujigou mining basin, this calibrated anthracite strictly satisfies GB/T 14181-2010 quality standards to guarantee predictable volatile yield and structural carbon matrix consistency.
  • Calibrated Gravimetric Static Presser: Built with a rigid mechanical alignment frame, this static consolidation device consistently applies an exact nominal load of 6.5 kg across sample crucibles to establish standardized packing density and eliminate operator-dependent compression errors.
  • Oxidation-Resistant Nickel-Chromium Compacting Weights: Machined from premium nickel-chromium alloy, each cylindrical block maintains an exact mass between 110 g and 115 g with an axial relief hole, ensuring uniform top-layer compression without thermal warping or surface scaling at high operating temperatures.
  • Thermal-Shock Resistant Porcelain Crucibles and Lids: Fabricated from high-grade refractory porcelain with a 30 mL volume and precise geometric taper, these vessels endure rapid insertion into 850°C furnace zones without micro-fissuring, sealing volatile matter effectively against atmospheric oxidation.
  • Rigid Nickel-Chromium Wire Crucible Stand: Constructed from heavy-gauge 3 mm to 4 mm heat-resistant nickel-chromium wire, this 4-position rack retains level structural geometry under extreme heat, facilitating rapid, balanced batch handling and uniform thermal exposure inside the furnace chamber.
  • Standardized Rigid Metal Stirring Wires: Formed from durable 1.0 mm to 1.5 mm hard metal wire featuring an 8 mm circular loop and an ergonomic handle, these precision tools ensure rapid, homogeneous blending of coal and anthracite without bending or shedding metallic particles.
  • Strict Dimensional Standardization: Every component is precision-machined to exact dimensional tolerances conforming to GB/T 5447 guidelines, guaranteeing immediate interchangeability with standard coking test furnaces and laboratory apparatus.
  • Corrosion and Oxidation Resistance: High-grade metallurgical alloys and inert ceramic compounds resist degradation from hot coal gases, sulfur dioxide, and heavy tar fractions, preserving gravimetric accuracy over extended analytical runs.

Applications

The determination of coal caking index provides essential predictive insight into the plastic, swelling, and agglomerating properties of bituminous coals during high-temperature carbonization. The following table highlights typical industrial and laboratory applications where these precision spare parts are essential.

Application Description Key Benefit
Coking Coal Blending and Optimization Testing raw and washed coking coal samples to determine plastic layer development and agglomeration properties prior to oven charging. Ensures optimal coal blend recipes, reducing reliance on expensive prime coking coals while protecting coke battery wall stability.
Blast Furnace Coke Quality Assurance Routine quality screening of metallurgical coal feedstocks to evaluate post-carbonization mechanical strength and lump cohesion. Accurately predicts drum strength indices (M40/M10) and coke strength after reaction (CSR), preventing furnace permeability loss.
Commercial Coal Cargo Arbitration and Trade Performing independent third-party laboratory verification of contractually specified caking parameters for export and domestic coal shipments. Provides verifiable analytical precision matching national standards, preventing settlement disputes between suppliers and buyers.
Geological Seam Exploration and Core Profiling Analyzing drill core samples from newly explored coal basins to map spatial variations in coal rank, adhesiveness, and industrial utility. Delivers reliable caking index classification from limited core sample masses, accelerating mine feasibility and resource valuation.
Coal Washing and Preparation Plant Monitoring Monitoring clean coal fractions, middlings, and flotation products to evaluate the efficiency of beneficiation circuits on coking potential. Verifies that cleaning processes do not selectively wash out reactive petrographic components responsible for thermoplastic bonding.
Research on Carbonization Kinetics and Additives Investigating the influence of biomass blends, petroleum coke additives, or pitch binders on the agglutinating behavior of secondary coals. Maintains rigorous baseline testing repeatability, enabling researchers to isolate subtle thermo-chemical kinetic interactions.

Technical Specifications

The following tables detail the technical parameters, structural dimensions, material compositions, and manufacturing standards for the complete suite of replacement components and reference consumables.

Component Portfolio and Model Identification

Component Description Model Identifier Material Specification Primary Dimensional Attributes Governing Standard
Complete Caking Index Spare Parts Suite KT-ZJ Multi-Component Assembly Full Analytical Suite Configuration GB/T 5447, GB/T 14181-2010
Standard Anthracite Reference Material KT-ZJ-AC Ningxia Rujigou No. 2-1 Lower Seam Net Weight: 1 kg Hermetic Pack GB/T 14181-2010
Static Pressure Loading Device KT-ZJ-SP Fabricated Carbon Steel with Guide Shaft 220 mm × 220 mm × 420 mm GB/T 5447
Nickel-Chromium Compacting Weight Block KT-ZJ-PB Heat-Resistant Nickel-Chromium Steel Outer Ø31 mm × H21 mm; Center Hole Ø10 mm × D15 mm GB/T 5447
Porcelain Crucible and Cover Set KT-ZJ-CR High-Density Refractory Porcelain Top Ø40 mm, Base Ø20 mm, Height 40 mm, Capacity 30 mL GB/T 5447
Four-Aperture Wire Crucible Stand KT-ZJ-CS Heavy-Gauge Nickel-Chromium Wire (Ø3–4 mm) 110 mm × 110 mm × 60 mm; Aperture ID Ø42 mm GB/T 5447
Hard Metal Stirring Wire Tool KT-ZJ-SW Rigid High-Tensile Drawn Metal Wire Total Length 110 mm; Loop Ø8 mm; Handle 25 mm × 5 mm GB/T 5447

Comprehensive Dimensional and Mechanical Tolerances

Parameter Group Technical Property Nominal Specification Permissible Tolerance / Operational Criteria
Standard Anthracite Reference Mine Origin and Geological Horizon Ningxia Rujigou Coal Mine (Xigou Pingjiong) Both sides of No. 2-1 coal seam, lower slice
Standard Anthracite Reference Packaging Net Weight 1 kg Moisture-proof sealed container
Standard Anthracite Reference Standard Certification GB/T 14181-2010 Certified ash yield and volatile matter baseline
Static Consolidation Presser Nominal Compaction Force 6.5 kg Calibrated vertical dead-weight application
Static Consolidation Presser Frame Footprint Dimensions 220 mm (W) × 220 mm (L) × 420 mm (H) Precision upright dual-post alignment
Static Consolidation Presser Total Device Weight 12.5 kg Weighted anti-tipping cast-iron base
Ni-Cr Compacting Weight Material Composition Nickel-Chromium Alloy Steel High-temperature oxidation resistant formulation
Ni-Cr Compacting Weight Outer Cylinder Diameter Ø31 mm ±0.2 mm ground cylindrical tolerance
Ni-Cr Compacting Weight Total Block Height 21 mm ±0.2 mm vertical profile
Ni-Cr Compacting Weight Concentric Relief Hole Diameter Ø10 mm Centered axial aperture
Ni-Cr Compacting Weight Relief Hole Internal Depth 15 mm Standard volatile expansion cavity
Ni-Cr Compacting Weight Calibrated Mass Range 110 g to 115 g Strict gravimetric verification per piece
Crucible and Lid Assembly Internal Working Volume 30 mL Sized for standard 1:5 coal-anthracite blend
Crucible and Lid Assembly Top Rim Outer Diameter Ø40 mm Precision tapered mouth with recessed rim
Crucible and Lid Assembly Base Outer Diameter Ø20 mm Flat ground base for stable positioning
Crucible and Lid Assembly Total Crucible Height 40 mm Standard vertical clearance profile
Crucible and Lid Assembly Thermal Shock Limit 850°C ± 10°C Rapid furnace transfer with zero structural spalling
Wire Crucible Stand Frame Material Nickel-Chromium Heat-Resistant Wire Wire diameter: Ø3.0 mm to Ø4.0 mm
Wire Crucible Stand Holding Capacity 4 Crucibles Symmetrical 2 × 2 cell arrangement
Wire Crucible Stand Cell Ring Internal Diameter Ø42 mm Smooth drop-in fit for Ø40 mm crucibles
Wire Crucible Stand Overall External Dimensions 110 mm (W) × 110 mm (L) × 60 mm (H) Engineered for standard laboratory muffle furnaces
Metal Stirring Wire Tool Construction Material Rigid Hard Drawn Metal Wire High flexural rigidity, non-shedding
Metal Stirring Wire Tool Core Wire Diameter Ø1.0 mm to Ø1.5 mm Prevents bending during sample blending
Metal Stirring Wire Tool Total Overall Length 110 mm Provides ample clearance above 40 mm crucible walls
Metal Stirring Wire Tool Circular Loop Diameter Ø8 mm Formed closed circular mixing end
Metal Stirring Wire Tool Handle Plate Dimensions 25 mm Length × 5 mm Width Flattened grip for ergonomic control

Procedural Integration and Testing Protocol

To ensure audit-ready analytical results in compliance with GB/T 5447, these components are utilized in a standardized analytical sequence:

  1. Sample Proportioning and Preparation: Precisely 1.00 g of air-dried pulverized coal sample (<0.2 mm particle size) is weighed into the ceramic crucible alongside 5.00 g of the standard anthracite reference material.
  2. Mechanical Homogenization: Using the rigid metal stirring wire, the operator blends the two components for 1 minute with a standardized circular motion, ensuring uniform distribution of coking and inert coal grains without loss of fines.
  3. Surface Flattening and Static Consolidation: The coal mixture surface is leveled horizontally, and the nickel-chromium compacting weight block is centered directly on top of the bed. The crucible is placed into the static pressure device, where a constant 6.5 kg force is applied vertically for exactly 30 seconds to produce a consolidated, uniform cylindrical coal cake.
  4. Controlled Pyrolysis: With the compacting block remaining seated on the sample, the crucible lid is fitted tightly. Four crucibles are loaded simultaneously into the nickel-chromium wire stand and introduced into a high-temperature volatile determination furnace maintained at 850°C ± 10°C for precisely 15 minutes.
  5. Abrasion Resistance Assessment: Following cooling in a desiccator, the carbonized residue undergoes standardized tumbling cycles within a specialized drum apparatus and subsequent sieving to determine the final G-index value.

Why Choose This Product

  • Certified Metrological Standard Compliance: Every batch of standard anthracite and each precision-machined hardware accessory conforms strictly to GB/T 14181-2010 and GB/T 5447 criteria, providing complete auditability for accredited ISO/IEC 17025 coal testing laboratories.
  • Superior High-Temperature Metallurgical Integrity: Machined from premium oxidation-resistant nickel-chromium alloys and thermal-shock-resistant refractory ceramics, these components resist creep, warping, and mass loss through repetitive 850°C thermal cycles.
  • Exceptional Gravimetric and Dimensional Consistency: Strict manufacturing tolerances across static pressure loading fixtures, compacting weights, and crucibles eliminate instrument-induced artifacts and optimize cross-laboratory reproducibility.
  • Seamless Interoperability with Standard Testing Infrastructure: Designed as a cohesive testing ecosystem, each accessory integrates directly into existing laboratory muffle furnaces, drum tumblers, and sample preparation stations without requiring mechanical adjustments.
  • Responsive Global Supply and Batch Traceability: Backed by comprehensive inventory reserves and dedicated technical support, replacement consumables and certified reference coals are supplied promptly to prevent operational downtime.

Contact our technical sales engineers today to request a quotation, review batch inspection certificates, or establish scheduled consumable delivery agreements for your laboratory.

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Caking Index Determination Apparatus Spare Parts and Consumables for Coal Quality Testing

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