Products Lab Consumables & Materials Thin Film Deposition Parts

Thin Film Deposition Parts

There are several common methods used for laboratory coating, such as evaporation coating, sputtering, and chemical vapor deposition.

We offers a comprehensive selection of coating accessories, such as evaporation boats made from various materials, evaporation crucibles, evaporation wires, boron nitride ceramics, an assortment of plates, and sputtering targets etc.

Tungsten Evaporation Boat

Tungsten Evaporation Boat

Item Number : LMF-TEB

Boron Nitride (BN) Ceramic Rod

Boron Nitride (BN) Ceramic Rod

Item Number : KM-D4

Electron Gun Beam Crucible

Electron Gun Beam Crucible

Item Number : KES01

Ceramic Evaporation Boat Set

Ceramic Evaporation Boat Set

Item Number : KME09

Graphite evaporation crucible

Graphite evaporation crucible

Item Number : KME07


Evaporation coating

Thin-film deposition often involves the use of evaporation as a primary method. During this process, the source material is evaporated within a vacuum, allowing the vapor particles to directly travel to the target object or substrate. Once there, the particles condense back into a solid state. This technique is utilized not only in microfabrication but also in the production of macro-scale products, including metallized plastic films.

Equipment used for evaporation coating

The use of a vacuum pump is an essential component in any evaporation system, which requires an energy source to evaporate the material to be deposited. Various energy sources are available, including:

In the thermal method, metal material is typically fed onto heated semimetal evaporators, also known as "boats," where a pool of melted metal forms in the boat cavity and evaporates into a cloud above the source. Alternatively, the source material may be placed in a crucible, radiatively heated by an electric filament, or hung from the filament itself (filament evaporation). 

Molecular beam epitaxy represents an advanced form of thermal evaporation.

In the electron-beam method, the source is heated by an electron beam with an energy of up to 15 keV.

Flash evaporation involves the continuous feeding of a fine wire or powder of source material onto a hot ceramic or metallic bar, which evaporates on contact.

Resistive evaporation is achieved by passing a large current through a resistive wire or foil containing the material to be deposited. The heating element is often referred to as an "evaporation source." Wire type evaporation sources are made from tungsten wire and can be formed into filaments, baskets, heaters, or looped shaped point sources. Boat type evaporation sources are made from tungsten, tantalum, molybdenum, or ceramic-type materials capable of withstanding high temperatures.

In some cases, the substrate is mounted on an out-of-plane planetary mechanism that rotates it around two axes simultaneously to minimize shadowing.

External links

Thin film evaporation reference - properties of common materials

KinTek Lab Film Coating Parts

We provide a complete range of coating accessories, including evaporation boats, crucibles, wires, boron nitride ceramics, plates, and sputtering targets etc. Contact us for consultation.

FAQ

What are tungsten boats?

Tungsten boats are small containers or trays made from tungsten metal. They are designed to hold and transport materials at high temperatures in various industrial and laboratory applications. Tungsten boats are commonly used in processes such as evaporation, sintering, and thermal analysis.

What are the advantages of using tungsten boats?

Tungsten boats offer several advantages in high-temperature applications. Firstly, tungsten has an extremely high melting point of 3,422°C, making it suitable for use in environments with extremely high temperatures. Tungsten boats also have excellent thermal conductivity, allowing for efficient heat transfer and uniform heating of the material being processed. They have high mechanical strength and can withstand deformation and warping even at elevated temperatures. Tungsten is highly resistant to chemical corrosion, making tungsten boats compatible with a wide range of materials and environments. Additionally, tungsten has a low vapor pressure, which means it has minimal vapor contamination, making it suitable for high-purity applications. Tungsten boats have a long lifespan and can be used repeatedly without significant deterioration.

What are the applications of Boron Nitride ceramic parts?

Boron Nitride ceramic parts find applications in various industries. They are commonly used in high-temperature environments, such as in thermal management systems, crucibles, heaters, and insulators. Due to their excellent thermal conductivity, Boron Nitride ceramic parts are used as heat sinks, substrates for electronic devices, and components in high-power electronics. They are also utilized in the aerospace industry for applications requiring lightweight and high-temperature resistance, such as rocket nozzles and thermal shields. Boron Nitride ceramic parts are also used in the semiconductor industry as wafer carriers, crucibles for crystal growth, and insulators. Additionally, they find applications in the chemical industry, where their chemical inertness and resistance to corrosion make them suitable for handling corrosive materials.

What is a thermal element?

A thermal element is a device that converts electrical energy into heat in order to raise the temperature of an object or space. There are several types of thermal elements, including tubular heating elements, radiative heating elements, and combination heating element systems. Heat transfer occurs through thermal resistance and thermal capacitance, and there are three sources of heat: a power source, a temperature source, and fluid flow. Thermal elements are commonly used in laboratory equipment, as well as in various domestic and industrial applications.

How are high-purity graphite crucibles made?

High-purity graphite crucibles are typically manufactured through a process called isostatic pressing. In this method, graphite powder is placed in a rubber mold, and then subjected to high pressure from all directions. This pressure compacts the graphite particles into a dense and uniform crucible shape. The crucible is then heated to a high temperature to remove any impurities and improve its purity.

What are the advantages of using Boron Nitride ceramic parts?

Using Boron Nitride ceramic parts offers several advantages. Firstly, their high thermal conductivity allows for efficient heat transfer, making them ideal for applications requiring heat dissipation or thermal management. Secondly, Boron Nitride ceramics exhibit excellent electrical insulation properties, making them suitable for electrical and electronic applications. They have low dielectric loss and high dielectric strength, allowing for reliable electrical insulation even at high temperatures. Additionally, Boron Nitride ceramic parts have a low coefficient of friction, providing excellent lubrication and wear resistance in applications where low friction is desired. They are also chemically inert, making them resistant to most acids, alkalis, and molten metals. Boron Nitride ceramic parts can withstand high temperatures without significant deformation or degradation, making them suitable for use in extreme environments.

How does a thermal element work?

A thermal element works by converting electrical energy into heat through the process of Joule heating. When an electric current flows through the element, it encounters resistance, and this results in heating of the element. Metal and ceramic heating elements operate on the principle of electric resistance heating, generating heat by resisting the flow of electricity through the material. The coefficient of electrical resistance of the material determines its ability to generate heat proportional to the amount of current flowing through it. The generated heat radiates outwards into the heat treatment chamber, making thermal elements a highly effective method of generating heat.

What are the common applications of high-purity graphite crucibles?

High-purity graphite crucibles have a wide range of applications in industries such as metallurgy, foundries, and laboratories. They are commonly used for melting and casting non-ferrous metals, including aluminum, copper, and precious metals. High-purity graphite crucibles are also utilized in the production of alloys and high-temperature ceramics. They are essential in processes such as chemical analysis, spectroscopy, and sample preparation in laboratories. Additionally, these crucibles find applications in the semiconductor industry for the melting and growing of silicon and other semiconductor materials.

What considerations should be made when selecting Boron Nitride ceramic parts?

Several considerations should be made when selecting Boron Nitride ceramic parts. Firstly, the specific application requirements should be evaluated, such as temperature range, electrical insulation properties, thermal conductivity, mechanical strength, and chemical resistance. This will help determine the appropriate grade or formulation of Boron Nitride ceramic to select. Secondly, the design and geometry of the ceramic part should be considered to ensure that it can be manufactured using the available processes and equipment. The dimensional tolerances and surface finish requirements should also be taken into account. Additionally, the cost and availability of the Boron Nitride ceramic parts should be considered, as different manufacturing processes and grades of Boron Nitride can vary in cost. It is advisable to consult with manufacturers or experts in the field to ensure that the selected Boron Nitride ceramic parts meet the specific application requirements.

What are the advantages of using evaporation boats?

Evaporation boats offer several advantages in thin film deposition processes. They provide a controlled environment for the evaporation of materials, ensuring precise control over film thickness and uniformity. Evaporation boats can withstand high temperatures and provide efficient heat transfer, allowing for consistent evaporation rates. They are available in various sizes and shapes, accommodating different evaporation systems and substrate configurations. Evaporation boats enable the deposition of a wide range of materials, including metals, semiconductors, and ceramics. They are easy to load and unload, facilitating quick material changes or process adjustments. Overall, evaporation boats are essential tools in thin film deposition techniques, offering versatility, reliability, and reproducibility.

What are the advantages of using thermal elements?

Thermal elements offer several advantages in temperature measurement. Firstly, they have a wide temperature range, allowing for accurate measurements across a broad spectrum, from extremely low temperatures to high temperatures. They also have high sensitivity, meaning they can detect even small temperature changes. Additionally, thermal elements have excellent stability and repeatability, providing reliable and consistent temperature readings over time. They are rugged and durable, making them suitable for use in harsh environments. Thermal elements can also be easily integrated into various systems and instruments for temperature monitoring and control.

What are the common materials used for evaporating crucibles?

Evaporating crucibles are commonly made from materials such as tungsten, tantalum, molybdenum, graphite, or ceramic compounds. These materials have high melting points and good thermal conductivity, making them suitable for the high-temperature conditions required during evaporation. The choice of crucible material depends on factors such as the evaporant material, desired film properties, and process parameters.

What factors should be considered when selecting high-purity graphite crucibles?

When selecting high-purity graphite crucibles, several factors should be considered. Firstly, the size and capacity of the crucible should align with the intended application and the amount of material to be melted or processed. The crucible's thermal conductivity, thermal shock resistance, and chemical compatibility should be evaluated to ensure they meet the specific process requirements. It is important to select crucibles made from high-quality graphite material with high purity levels to minimize contamination and ensure excellent performance. The crucible's design and construction should also be considered, such as the presence of handles or pouring spouts for easy handling. Additionally, it is advisable to consult with manufacturers or experts in the field to ensure the selection of the most suitable high-purity graphite crucibles for specific applications.

What manufacturing processes are used to produce Boron Nitride ceramic parts?

Several manufacturing processes can be used to produce Boron Nitride ceramic parts. The most common methods include hot pressing, hot isostatic pressing (HIP), and slip casting. Hot pressing involves compacting Boron Nitride powders under high pressure and temperature to form a dense ceramic. HIP involves subjecting the Boron Nitride powder compact to high temperature and pressure in an inert gas environment to achieve even higher density and eliminate any remaining porosity. Slip casting involves forming a slurry of Boron Nitride powder and a binder, pouring it into a mold, and then drying and firing the green body to produce the final ceramic part. Other processes, such as extrusion, injection molding, or machining, may be used for shaping and finishing the Boron Nitride ceramic parts, depending on the desired geometry and specifications.

What is the typical lifespan of an evaporation boat?

The lifespan of an evaporation boat can vary depending on several factors. It primarily depends on the material used for the boat, the operating conditions, and the frequency of use. Evaporation boats made of refractory metals like tungsten or molybdenum are generally more durable and have longer lifespans compared to boats made from ceramic materials. With proper handling, regular maintenance, and appropriate cleaning procedures, evaporation boats can typically be used for multiple deposition cycles. However, over time, evaporation boats may experience wear and tear, such as cracking or degradation, which may reduce their lifespan. It is important to monitor the condition of the evaporation boat, conduct regular inspections, and replace it when necessary to ensure consistent and reliable thin film deposition.

What are the different types of thermal elements?

There are several types of thermal elements, including thermocouples, resistance temperature detectors (RTDs), and thermistors. Thermocouples are made of two dissimilar metals joined together, and they generate a voltage proportional to the temperature difference between their junctions. RTDs are made of pure metals, such as platinum or copper, and their resistance changes with temperature. Thermistors are made of temperature-sensitive semiconducting materials and have a large change in resistance with temperature.

What are the advantages of using evaporating crucibles?

Evaporating crucibles offer several advantages in thin film deposition processes. They provide a controlled environment for the evaporation of materials, allowing for precise control over film thickness and uniformity. Crucibles can withstand high temperatures and provide efficient heat transfer, ensuring consistent evaporation rates. They are available in various sizes and shapes to accommodate different evaporation systems and substrate configurations. Evaporating crucibles also allow for the deposition of a wide range of materials, including metals, semiconductors, and ceramics. They can be easily loaded and unloaded, facilitating quick material changes or process adjustments. Overall, evaporating crucibles are essential tools in thin film deposition techniques, offering versatility, reliability, and reproducibility.

Can evaporation boats be reused?

Evaporation boats can be reused, but it depends on several factors. The boat's condition, cleanliness, and compatibility with different evaporant materials play a significant role in determining whether it can be reused. If the evaporation boat is in good condition, free from cracks or defects, and has been cleaned thoroughly, it can typically be reused for subsequent depositions. However, if the boat has been exposed to reactive materials or shows signs of degradation, it may not be suitable for reuse. Consider the potential for contamination or unwanted reactions when reusing evaporation boats. Regular inspection and proper cleaning procedures are essential to maintain the boat's performance and ensure its suitability for reuse.

How should thermal elements be calibrated and maintained?

Calibration and maintenance of thermal elements are crucial to ensure their accuracy and reliability. Regular calibration should be performed using certified reference thermometers or temperature standards to verify the accuracy of temperature readings. Calibration intervals may vary depending on the application and industry requirements. Proper storage and handling of the thermal elements are important to prevent damage or contamination. It is recommended to protect the elements from extreme temperatures, moisture, and corrosive substances. Regular inspection of the element's connections, insulation, and protective sheaths should be carried out, and any damage or wear should be addressed promptly. Proper cleaning of the elements, if required, should be done following manufacturer guidelines. It is important to follow the manufacturer's recommendations for maintenance and consult with experts when necessary.

How should evaporating crucibles be handled and maintained?

Evaporating crucibles should be handled and maintained with care to ensure their longevity and performance. Crucibles should be cleaned thoroughly before each use to remove any residual material from previous depositions. Avoid using abrasive materials that could damage the crucible's surface. During loading and unloading, handle crucibles with clean gloves or specialized tools to prevent contamination. When not in use, store crucibles in a dry and clean environment to avoid corrosion or degradation. Regular inspection of crucibles for cracks, defects, or signs of wear is important to prevent unexpected failures during the evaporation process. Follow the manufacturer's recommendations for any specific maintenance procedures, such as annealing or surface treatment, to prolong the crucible's lifespan.

How do you select the appropriate evaporation boat material?

The selection of the appropriate evaporation boat material depends on several factors. Consider the melting point of the material being evaporated and choose a boat material with a higher melting point to prevent boat failure. Also, consider the compatibility of the boat material with the evaporant to avoid reactions or contamination. The boat's thermal conductivity and heat capacity should be evaluated for efficient heat transfer and temperature control during evaporation. Additionally, consider the boat's mechanical properties, such as strength and durability, to ensure it can withstand repeated heating and cooling cycles.

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Downloads

Catalog of Thin Film Deposition Parts

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Catalog of Evaporation Boat

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Catalog of Thermal Evaporation Sources

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Catalog of Thermal Elements

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Catalog of Evaporation Crucible

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Catalog of Tungsten Boat

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Catalog of High Purity Graphite Crucible

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Catalog of Engineering Ceramics

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Catalog of Fine Ceramics

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Catalog of Boron Nitride Ceramics

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Catalog of Advanced Ceramics

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