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Evaporation Crucible for Organic Matter

Thin Film Deposition Parts

Evaporation Crucible for Organic Matter

Item Number : KME-YJG

Price varies based on specs and customizations


Material
Quartz crucible / Alumina crucible / Boron nitride crucible /
crucible size
13*13mm / 18*20mm / 25.4*30mm / 25.4*30mm / 10*25mm
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Application

The Evaporation crucible for organic matter is a special container used in the laboratory to control the evaporation of organic solvents. They have a wide and shallow design to maximize the heating surface area and allow for efficient solvent evaporation. These crucibles are commonly used for concentration, solvent removal and preparation of solid residues in various laboratory procedures. They are especially suitable for handling volatile organic compounds (VOCs) which evaporate easily at lower temperatures.

Detail & Parts

Boron nitride crucible
Boron nitride crucible
Quartz crucible
Quartz crucible
Alumina crucible
Alumina crucible

Evaporation crucible for organic matter

Evaporation crucible for organic matter

Evaporation crucible for organic matter

Technical specifications

crucible  size 13*13mm / 18*20mm / 25.4*30mm / 25.4*30mm / 10*25mm

The crucibles we show are available in different sizes and custom sizes are available on request.

Explanation of proper nouns

  • Thin Film Deposition: Evaporation crucible for organic matter play a vital role in thin film deposition techniques such as thermal evaporation or organic vapor deposition. By heating the crucible and allowing the material to evaporate, a thin film is deposited onto the substrate.
  • Sample Preparation: Evaporation crucible for organic matter are used to dry and concentrate solutions or suspensions of organic compounds, allowing the solvent to evaporate and leaving the desired solid residue.
  • Solvent Evaporation: Evaporation crucible for organic matter are used to remove solvents from solutions or mixtures by gentle heating.
  • Crystallization: Evaporation crucibles are used in the crystallization process. By slow evaporation of the solvent, a crystalline solid can form in the crucible.
  • Concentration and volume reduction: Evaporation crucibles are used to concentrate solutions or reduce the volume of liquid samples.
  • Precursor Synthesis: Evaporation crucible for organic matter are used for the synthesis of various organic and inorganic materials. They can be used to evaporate and heat precursor solutions to obtain desired compounds or materials.

Advantage

  • Heat resistance: It can withstand high temperature without deformation or melting.
  • Chemical resistance: inert and resistant to most organic solvents, preventing interaction or contamination.
  • Versatility: Compatible with various organic solvents.
  • Various sizes and shapes: Provide different sizes and shapes to meet the needs of experiments.
  • Sample Concentration: Facilitates sample concentration by removing solvent.
  • Easy to monitor: the shallow design can visually observe the evaporation process.
  • Cost-effective: Relatively cheap compared with other laboratory equipment.

Precautions

  • The heated crucible cannot be quenched, and it should be removed with a crucible clamp.
  • Heat the crucible on the clay triangle.
  • Before use, gradually heat the crucible to 500 degrees Celsius, and store it in a dry place after use.
  • Choose an appropriate amount of raw materials to fill the crucible, avoid overfilling to prevent cracks caused by thermal expansion.
  • Whenever possible, use a spoon rather than a caliper when removing molten metal. If calipers are used, make sure they conform to the shape of the crucible and apply minimal localized force to avoid shortening the life of the crucible.
  • Avoid spraying strong oxidizing flame directly on the crucible, which will oxidize the crucible material and reduce its service life.

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FAQ

The Difference Between Metal Crucible And Ceramic Crucible.

Organic evaporation crucibles are usually made of ceramic materials rather than metal. Ceramic materials, such as porcelain or borosilicate glass, are preferred due to their high temperature resistance and compatibility with organic solvents.Metal crucibles are more commonly used for high temperature applications involving inorganic substances. They can withstand higher temperatures than ceramic crucibles and are usually made of materials such as stainless steel or platinum. However, when using organic solvents, metal crucibles can react with or be corroded by certain solvents, compromising the integrity of the crucible and possibly contaminating the sample.Therefore, for organic evaporation, ceramic crucibles are preferred due to their thermal stability and chemical resistance to organic solvents. They provide safe and reliable containers for the controlled evaporation of organic solvents in laboratory environments.

What Are The Common Materials Used For Evaporating Crucibles?

Evaporating crucibles are commonly made from materials such as tungsten, tantalum, molybdenum, graphite, or ceramic compounds. These materials have high melting points and good thermal conductivity, making them suitable for the high-temperature conditions required during evaporation. The choice of crucible material depends on factors such as the evaporant material, desired film properties, and process parameters.

What Are The Advantages Of Using Evaporating Crucibles?

Evaporating crucibles offer several advantages in thin film deposition processes. They provide a controlled environment for the evaporation of materials, allowing for precise control over film thickness and uniformity. Crucibles can withstand high temperatures and provide efficient heat transfer, ensuring consistent evaporation rates. They are available in various sizes and shapes to accommodate different evaporation systems and substrate configurations. Evaporating crucibles also allow for the deposition of a wide range of materials, including metals, semiconductors, and ceramics. They can be easily loaded and unloaded, facilitating quick material changes or process adjustments. Overall, evaporating crucibles are essential tools in thin film deposition techniques, offering versatility, reliability, and reproducibility.

How Should Evaporating Crucibles Be Handled And Maintained?

Evaporating crucibles should be handled and maintained with care to ensure their longevity and performance. Crucibles should be cleaned thoroughly before each use to remove any residual material from previous depositions. Avoid using abrasive materials that could damage the crucible's surface. During loading and unloading, handle crucibles with clean gloves or specialized tools to prevent contamination. When not in use, store crucibles in a dry and clean environment to avoid corrosion or degradation. Regular inspection of crucibles for cracks, defects, or signs of wear is important to prevent unexpected failures during the evaporation process. Follow the manufacturer's recommendations for any specific maintenance procedures, such as annealing or surface treatment, to prolong the crucible's lifespan.
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Product Datasheet

Evaporation Crucible for Organic Matter

Category Catalog

Thin Film Deposition Parts


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