Assay Equipment Accessories & Consumables
Laboratory Micro Oxygen Filling Instrument for Precision Bomb Calorimetry Charging
Item Number : KT-CYY
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Product Overview


This micro oxygen filling instrument is a specialized benchtop gas-regulation system engineered for the safe, precise pressurization of laboratory oxygen bombs, combustion calorimeters, and micro-reaction vessels. Sourcing gas directly from industrial high-pressure oxygen cylinders rated up to 20 MPa, this instrument down-regulates and meters output pressure into stable, application-specific charging bands between 0.1 and 3.5 MPa. By integrating an ultra-fine metering needle valve, heavy-duty pressure-relief mechanics, and a non-sparking, oil-free fluid circuit, the equipment ensures consistent oxygen partial pressures while mitigating the severe risks inherent to handling compressed pure oxygen.
Designed primarily for testing protocols governed by ASTM, ISO, and DIN analytical standards, this system is an indispensable front-end interface for coal evaluation, petrochemistry, bio-mass calorific profiling, waste-to-energy characterization, and energetic materials testing. The controlled inlet geometry prevents the mechanical disturbance or aerosolization of volatile powders and loose pellet specimens inside the combustion crucible, preserving sample integrity prior to ignition. Routine commercial testing laboratories and dedicated academic institutions rely on the equipment to streamline sample preparation workflows while enforcing rigorous laboratory safety standards.
Built to withstand continuous, high-cycle operation in industrial laboratories, the unit is assembled from ultrasonically degreased oxygen-compatible brass and 316L stainless steel alloys. Each mechanical sub-assembly undergoes hydrostatic proof-testing, helium leak integrity assessment, and microscopic particulate inspections. Operators gain steady, repeatable pressure control, effortless bomb coupling, and complete confidence in long-term operational resilience under heavy daily testing schedules.
Key Features
- Certified Oil-Free and Oxygen-Cleaned Architecture: Completely degreased in compliance with stringent oxygen-handling protocols, eliminating all traces of hydrocarbons and particulate contaminants to neutralize ignition risks caused by adiabatic compression in high-pressure pure oxygen atmospheres.
- Fine-Pitch Soft-Start Needle Throttle: An engineered needle valve mechanism allows micro-metered, laminar gas admission, preventing sudden acoustic pressure shocks or turbulent gas waves that could scatter fine powdered samples out of analytical crucibles.
- Precision Dual-Scale Pressure Indication: Outfitted with an industrial Class 1.6 Bourdon-tube pressure gauge featuring clear dual graduations (0–6.0 MPa and psi/bar), empowering technicians to hit target combustion pressures within tight tolerances of ±0.05 MPa.
- Integrated Pop-Off Safety Relief Valve: A tamper-resistant, factory-calibrated spring-loaded relief valve automatically discharges gas if system pressure exceeds 3.5 MPa, proactively protecting downstream combustion bomb vessels from over-pressurization.
- Ergonomic Quick-Coupling Snap Socket: Features an industrial-grade quick-connect interface designed for single-handed engagement with standard calorimeter bomb filling nipples, guaranteeing gas-tight sealing without thread wear, galling, or manual wrenching.
- Independent Fast-Action Decompression Bleed: A dedicated manual exhaust valve permits immediate, controlled venting of residual line pressure between the regulator and the bomb valve after charging, allowing effortless and safe connector disconnection without recoil.
- Forged Non-Sparking Wetted Metallurgy: All primary fluid pathways are precision-machined from high-density forged brass and 316L stainless steel, conferring exceptional resistance to cyclic fatigue, stress-corrosion cracking, and galvanic oxidation.
- Weighted Anti-Topple Benchtop Platform: Engineered with an ultra-low center of gravity, a heavy ballast base plate, and vibration-dampening elastomer feet that hold the instrument completely stationary during single-handed valve operation.
Applications
| Application | Description | Key Benefit |
|---|---|---|
| Solid Fuel Calorimetry (ASTM D5865 / ISO 1928) | Controlled oxygen charging of combustion bombs for coal, metallurgical coke, and lignite gross calorific value (GCV) determination. | Soft-metered gas flow prevents powdered coal ejection from sample crucibles, eliminating test invalidation. |
| Petroleum and Aviation Fuels (ASTM D240 / ISO 8217) | Pressurizing combustion vessels with 3.0 MPa oxygen to evaluate heat of combustion in jet fuel, diesel, and heavy bunker oils. | Ensures pure stoichiometric excess for 100% complete combustion without soot formation or partial oxidation. |
| Biomass and Waste-Derived Fuels (EN 14918 / ASTM E711) | Oxygen priming for calorific analysis of agricultural pellets, wood chips, and municipal refuse-derived fuel (RDF). | Reliable high-throughput charging cycle speeds up multi-sample daily testing in high-capacity energy audit labs. |
| Energetic Materials and Propellant Testing | Pressurizing specialized micro-bombs for thermochemical characterization of pyrotechnics, propellants, and reactive chemical precursors. | Ultra-clean fluid passage and certified overpressure relief safeguard personnel during sensitive ignition trials. |
| Food, Animal Nutrition, and Biomaterials | Preparing oxygen bomb vessels for direct nutritional caloric value measurement in raw foodstuffs, forage crops, and lipids. | Exceptional pressure repeatability (±0.05 MPa) delivers tight statistical standard deviation across test duplicates. |
| Hydrothermal and Small Autoclave Charging | Delivering controlled oxygen overpressures to benchtop micro-reactors used in wet air oxidation and hydrothermal digestion. | High-pressure needle control allows smooth dosing of partial pressures into sub-500 mL batch autoclave units. |
| Academic and Industrial Catalyst Oxidation Screening | Introducing high-purity reactive oxygen into small sealed test chambers to evaluate oxidation stability and catalyst lifetimes. | Standard G5/8" and CGA bottle adaptors ensure immediate plug-and-play integration into diverse research manifolds. |
Technical Specifications
| Specification Parameter | Value / Engineering Range |
|---|---|
| Product Item Number | KT-CYY |
| Compatible Working Media | Industrial Oxygen (O₂), High-Purity Oxygen (≥99.5%), Compressed Air, Inert Gases (N₂, Ar) |
| Maximum Cylinder Supply Pressure | 20.0 MPa (200 bar / ~2,900 psi) |
| Adjustable Output Charging Range | 0.1 to 3.5 MPa (1.0 to 35.0 bar / ~14.5 to 507 psi) |
| Standard Pre-Calibrated Operating Pressure | 2.8 to 3.0 MPa (Optimized for Standard Analytical Bomb Calorimeters) |
| Hydrostatic Proof Test Pressure | 6.0 MPa (60 bar / ~870 psi) |
| Ultimate Structural Safety Factor | > 4.0× nominal operating envelope |
| Pressure Gauge Range and Type | 0 to 6.0 MPa; Industrial Bourdon-tube analog dial with safety blow-out back |
| Pressure Gauge Accuracy Class | Class 1.6 (±1.6% of full span); Class 1.0 precision calibration available |
| Safety Relief Valve Activation Setting | Preset at 3.50 ± 0.10 MPa (Automatic atmospheric discharge) |
| Inflow Control Mechanism | Multi-turn needle valve with micro-finished hardened stainless spindle |
| Exhaust / Decompression System | Integrated finger-actuated knurled manual bleed valve |
| Inlet Gas Cylinder Connection | Standard G5/8" Male Thread (CGA 540 and DIN 477 No. 9 brass adapters available) |
| Bomb Interface Coupling | Self-locking quick-connect snap socket (Engineered for Ø 8.0 mm / Ø 10.0 mm bomb heads) |
| Wetted Body Materials | High-tensile forged brass (CW617N / HPb59-1) and 316L Austenitic Stainless Steel |
| Internal Sealing Components | Oxygen-grade Virgin Polytetrafluoroethylene (PTFE) and DuPont Viton FKM elastomers |
| Cleanliness and Degreasing Level | Fully solvent-degreased in accordance with ASTM G93 Level A and ISO 15001 standards |
| Base Footprint (Width × Depth × Height) | 260 mm × 180 mm × 295 mm (10.2" × 7.1" × 11.6") |
| Ambient Operating Temperature Range | 5°C to 45°C (41°F to 113°F) |
| Applicable Bomb Vessel Volumes | 200 mL to 450 mL standard combustion bombs and micro-reactors |
Why Choose This Product
- Uncompromising Oxygen Safety Engineering: Manufactured using proprietary degreasing processes aligned with international oxygen equipment safety codes, eliminating combustible surface residues and preventing explosive flash ignition from adiabatic gas compression.
- Precision Laminar Dosing: The finely threaded stainless steel needle throttling assembly ensures progressive gas introduction, completely preventing the sample spatter, powder blow-out, and crucible tip-overs common with generic industrial regulators.
- Built for Extreme Laboratory Duty Cycles: Unlike light-gauge regulatory units, this system uses solid forged brass blocks and precision-machined stainless components that resist cyclical strain, port galling, and seat leakages across tens of thousands of fills.
- Universal Bomb Compatibility: Engineered with a modular quick-coupling port that interfaces seamlessly with major analytical calorimeter brands and bespoke pressure vessels, making it a universal upgrade for testing facilities.
- Backed by Comprehensive Technical Support: Delivered with fully traceable factory pressure inspection documentation, available recalibration kits, and expert application assistance from KINTEK's technical engineering department.
Contact our laboratory instrumentation specialists today to receive a prompt quotation, confirm quick-coupling compatibility with your specific bomb models, or configure customized gas manifold assemblies.
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Product Datasheet
Laboratory Micro Oxygen Filling Instrument for Precision Bomb Calorimetry Charging
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