Assay Equipment Accessories & Consumables
Calorimeter Accessories Bomb Combustion Vessels Crucibles and Analytical Consumables
Item Number : KT-LRY
Price varies based on specs and customizations
- Vessel Hydrostatic Proof Pressure
- 30 to 32 MPa
- Standard Oxygen Charging Pressure
- 3.0 to 3.5 MPa
- Calibration Standard Purity
- 99.99% Benzoic Acid (26,454 J/g ± 5 J/g)
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Product Overview

Precision calorimetry demands uncompromising integrity across every component of the measurement chain. These specialized calorimeter accessories deliver the mechanical robustness, thermal stability, and chemical inertness required to achieve repeatable gross calorific value (GCV) determinations in laboratory and industrial testing environments. Designed to withstand extreme internal pressures and aggressive combustion byproducts, each accessory ensures absolute operator safety, minimizes thermal transfer variances, and preserves the sample integrity required for sensitive thermodynamic evaluations.
From high-throughput coal and petroleum testing facilities to advanced energetic material research centers, this comprehensive suite of accessories integrates seamlessly with standard bomb calorimeters, isoperibol systems, and automated oxygen combustion setups. By maintaining strict metallurgical and dimensional tolerances, these components support rigorous laboratory workflows across solid fuels, biomass pellets, organic waste, food proximate analysis, and hazardous substance characterization.
Engineered to eliminate fugitive heat loss, contact degradation, and corrosion-induced measurement drift, this equipment provides long-term operational consistency under demanding combustion cycles. Laboratory technicians and procurement managers gain dependable access to certified oxygen combustion vessels, precision-formed crucibles, high-purity ignition wires, benzoic acid reference materials, and high-integrity pressure seals designed for continuous duty.
Key Features
- Corrosion-Resistant Oxygen Combustion Vessels: Fabricated from high-tensile, stabilized austenitic stainless steel and nickel-chromium superalloys, these vessels withstand internal combustion pressures up to 30 MPa and resist harsh acid vapors generated during halogen and sulfur combustions.
- Precision-Machined Combustion Crucibles: Offered in high-purity quartz, analytical-grade stainless steel, and chemically inert platinum, these crucibles ensure zero sample contamination, rapid thermal equilibrium, and complete sample burnoff without catalytic bias.
- Calibrated Ignition Wire and Cotton Threads: Manufactured from certified nickel-chromium, platinum, or pure iron alloys, each ignition element delivers uniform resistance and a precisely documented heat of combustion to guarantee exact thermal corrections.
- Ultra-Durable High-Pressure Sealing Systems: Precision fluoropolymer and specialized elastomeric O-rings maintain hermetic sealing at 3.0 to 3.5 MPa oxygen charging pressures, preventing micro-leakage and protecting vessel closure threads from gas scouring.
- Certified Traceable Calibration Standards: High-purity benzoic acid pellets and liquid standards traceable to national metrological standards ensure dependable calorific heat capacity calibration with minimal uncertainty margins.
- Standardized Sample Pelleting and Preparation Tools: Heavy-duty benchtop pellet presses and precision dies compress fine powders and low-density biomass into uniform tablets, preventing flash dispersion and incomplete combustion during the ignition sequence.
- Quick-Connect Oxygen Filling and Release Valves: Engineered with integrated blow-out protection, check valves, and regulated exhaust nozzles to guarantee smooth oxygen charging and controlled de-gassing without sample spattering.
- Enhanced Safety Burst Disks and Venting Mechanisms: Integral overpressure safety relief mechanisms protect equipment and personnel by safely dispersing overpressure spikes during abnormal combustion reactions.
Applications
| Application | Description | Key Benefit |
|---|---|---|
| Coal and Coke Fuel Evaluation | Daily calorific testing of raw coal, pulverized fuel, and metallurgical coke in accordance with ASTM D5865 and ISO 1928 standards. | Resists corrosive sulfuric and nitric acid condensation, prolonging vessel operational life and ensuring reproducible calorific determinations. |
| Petroleum and Liquid Fuels Testing | Measurement of heat value across fuel oils, diesel, aviation kerosene, and heavy residual fractions using specialized gelatin or tape encapsulation. | Prevents unburned residue and volatile flash-off through secure ignition geometry and ultra-stable crucible positioning. |
| Biomass and Alternative Waste Fuels | Determination of gross energy content in wood pellets, agricultural residue, refuse-derived fuel (RDF), and municipal solid wastes. | Heavy-duty pelleting dies eliminate powder splattering, ensuring complete ignition and predictable combustion kinetics. |
| Hazardous Waste Halogen Profiling | Quantitative bomb wash analysis for total sulfur, chlorine, fluorine, and heavy metals following complete oxidative combustion. | Non-reactive internal vessel finishes guarantee complete recovery of ionic condensates without surface adsorption. |
| Food and Animal Feed Science | Gross energy quantification of grain blends, feed rations, dairy solids, and dietary formulations for nutritional balance studies. | High-precision thermal corrections and zero sample cross-contamination guarantee compliance with international food labeling regulations. |
| Energetic Materials and Chemical R&D | Controlled caloric evaluation of chemical propellants, pyrotechnic primers, and polymer formulations under high-pressure oxygen environments. | Certified high-strength vessel metallurgy and overpressure protection ensure absolute containment and operator safety under rapid energy release. |
| Commercial Testing and Inspection Labs | Continuous multi-shift testing running dozens of daily sample burns across diverse customer-submitted raw materials. | High-grade elastomeric seals and wear-resistant valve assemblies dramatically lower preventative maintenance downtime and consumable operating costs. |
Technical Specifications
| Component Category | Item Code | Material / Construction | Operating Limits / Capacity | Standard Compliance |
|---|---|---|---|---|
| Standard Oxygen Combustion Vessel | KT-LRY-BOMB-STD | Austenitic stainless steel (AISI 316Ti / 316L) | 3.5 MPa charging pressure; 30 MPa hydrostatic proof; 300 mL volume | ASTM D5865, ISO 1928, GB/T 213 |
| Halogen/Acid-Resistant Vessel | KT-LRY-BOMB-CR | Hastelloy C-276 / Inconel cladding | 3.5 MPa charging pressure; 32 MPa hydrostatic proof; 320 mL volume | ASTM D240, ASTM D4809, DIN 51900 |
| Quartz Combustion Crucibles | KT-LRY-CRU-QZ | High-purity fused optical quartz (>99.9% SiO2) | Thermal shock resistant up to 1200°C; 1.5 mL to 2.5 mL volume | Ash-free combustion, ISO 1716 |
| Stainless Steel Crucibles | KT-LRY-CRU-SS | Heat-resistant 310S stainless steel | Continuous duty up to 1050°C; 2.0 mL volume; 0.5 mm wall thickness | ASTM E711, ASTM D5865 |
| Platinum Crucibles | KT-LRY-CRU-PT | Chemically pure platinum (99.95% Pt) | Unreactive up to 1600°C; 2.0 mL volume; zero catalytic oxidation drift | High-precision thermodynamic research |
| Nickel-Chromium Ignition Wire | KT-LRY-IGN-NC | 80/20 Ni-Cr alloy wire (0.1 mm to 0.15 mm dia.) | 5.86 J/cm heat of combustion; resistance 14.5 Ω/m | ASTM D5865, ASTM D240, ISO 1928 |
| Platinum Ignition Wire | KT-LRY-IGN-PT | Pure platinum wire (0.1 mm dia.) | Non-consumable fuse wire; zero net calorific contribution | Micro-calorimetry and reference labs |
| Benzoic Acid Calibration Standard | KT-LRY-CAL-BA | Analytical grade benzoic acid (99.99% purity) | Certified calorific value: 26,454 J/g ± 5 J/g; 1.0 g pre-formed pellets | Traceable to NIST / Metrological references |
| Primary Vessel Main O-Rings | KT-LRY-SEAL-V | Fluoroelastomer (FKM / Viton) / High-density EPDM | Working pressure 0–35 MPa; temperature -20°C to 180°C | Chemical and aggressive solvent resistant |
| Benchtop Pellet Press | KT-LRY-PRS-MAN | Hardened alloy tool steel frame with hydraulic lever | 0 to 20 kN manual force; interchangeable 6 mm, 8 mm, and 13 mm dies | Solid fuel and biomass sample prep |
| Oxygen Charging Manifold & Hose | KT-LRY-OXY-KIT | Dual-stage brass/stainless regulator with safety valve | 0–5 MPa delivery range; 30 MPa input rating; integrated pressure gauge | CE, EN ISO 2503 |
| Combustion Fuse Cotton Thread | KT-LRY-IGN-CTN | 100% degreased natural pure cotton fiber | 17.5 J/cm heat of combustion; low residue (<0.02% ash) | Standard ignition booster application |
Why Choose This Product
- Metallurgical Integrity and Pressure Safety: Every vessel and pressure-retaining fitting undergoes hydrostatic pressure proofing and ultrasonic material integrity validation, ensuring complete operational confidence under repeated high-energy release cycles.
- Direct Compatibility Across Leading Platforms: Engineered to standardized dimensions and connection profiles, these components integrate cleanly into existing laboratory setups, providing a turnkey replacement solution that eliminates costly retrofit downtime.
- Precision Calibration and Analytical Reproducibility: Certified consumables, from ultra-pure benzoic acid tablets to uniform ignition wires, ensure tight thermal correction figures that prevent cumulative errors and maintain strict compliance with global testing methodologies.
- Long-Term Resistance to Aggressive Condensates: Proprietary surface finishes, acid-resistant alloy grades, and inert crucibles neutralize corrosion from sulfur dioxide, nitrous oxides, and halides, maintaining baseline volume stability over thousands of test runs.
- Comprehensive Consumable and Spare Parts Availability: Complete multi-part kits, high-pressure seals, electrodes, and sample preparation equipment are kept in ready stock to safeguard laboratory continuity and reduce procurement overhead.
For custom alloy vessels, specialized crucible configurations, or bulk laboratory consumable supply agreements, contact our technical sales team today to request a detailed engineering quotation.
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Product Datasheet
Calorimeter Accessories Bomb Combustion Vessels Crucibles and Analytical Consumables
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