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Electrochemical Electrolytic Cell for Laboratory Research and Testing

Assay Equipment Accessories & Consumables

Electrochemical Electrolytic Cell for Laboratory Research and Testing

Item Number : KT-DJ

Price varies based on specs and customizations


Chamber Volume Range
10 mL to 500 mL
Operating Temperature Range
-20°C to +150°C
Operating Pressure Rating
Full vacuum to 0.2 MPa
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Product Overview

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This electrolytic cell system is engineered to provide an exceptionally stable, contamination-free environment for demanding electrochemical investigations and analytical characterization. Fabricated from premium optical-grade borosilicate glass, high-purity quartz, and precision-machined PTFE or PEEK components, the apparatus guarantees broad chemical compatibility across aggressive acidic, alkaline, and non-aqueous organic electrolytes. By maintaining rigid geometric spatial alignment between working, reference, and counter electrodes, the cell eliminates measurement artifacts, minimizes uncompensated solution resistance, and ensures pristine reproducible baseline data across repeated testing cycles.

Designed primarily for academic research facilities, energy storage innovation hubs, industrial quality assurance departments, and metallurgy testing centers, this equipment serves as a foundational platform for electrocatalytic evaluation, cyclic voltammetry, electrochemical impedance spectroscopy (EIS), battery material qualification, and accelerated corrosion analysis. Its flexible, multi-port architecture effortlessly accommodates standard three-electrode assemblies, dedicated gas purging tubes, temperature probes, and auxiliary sensing instrumentation without compromising seal integrity.

Built to withstand rigorous continuous laboratory operation, the assembly incorporates robust sealing mechanisms that prevent solvent evaporation, atmospheric oxygen ingress, and cross-compartment contamination. Whether configured as a single-compartment vessel or a divided H-type cell utilizing selective ion-exchange membranes, this apparatus delivers consistent thermodynamic stability, exceptional optical clarity for visual verification, and mechanical resilience under varied thermal and chemical operating conditions.

Key Features

  • Superior Chemical Inertness and Thermal Stability: The cell body is constructed from annealed 3.3 borosilicate glass or high-purity quartz paired with virgin PTFE/PEEK caps, resisting concentrated mineral acids, strong bases, and polar organic solvents across operating temperatures ranging from -20°C to 150°C.
  • Optimized Three-Electrode Spatial Geometry: Dedicated ground-glass or threaded ports fix the relative distance between working, counter, and reference electrodes, drastically reducing ohmic drop (IR drop) and delivering uncompromised signal fidelity during high-current cyclic voltammetry and electrochemical impedance spectroscopy.
  • Precision Luggin Capillary Integration: An engineered adjustable Luggin-Haber capillary allows fine positioning of the reference electrode tip adjacent to the working electrode surface, minimizing uncompensated solution resistance while preventing reference electrolyte leakage into the bulk reaction volume.
  • High-Integrity Hermetic Sealing: Precision-machined fluoropolymer compression fittings, Viton or FFKM O-rings, and ground-glass joint clamps maintain hermetic sealing under inert gas overpressures up to 0.2 MPa, precluding trace atmospheric oxygen ingress and volatile solvent evaporation during extended multi-hour trials.
  • Configurable Divided and Undivided Architectures: Available in undivided single-chamber formats or H-type split configurations utilizing high-precision interchangeable ion-exchange membranes, fine-porosity glass frits, or salt bridges to prevent chemical crossover between anolyte and catholyte compartments.
  • Dual-Walled Water-Jacketed Temperature Regulation: Optional circulating thermostatic jackets provide uniform heating and chilling across the fluid column, maintaining target electrolyte temperatures within ±0.1°C to support precise non-isothermal kinetics and thermodynamic parameter determinations.
  • Integrated Gas Purging and Blanketing System: Multi-way PTFE stopcocks and sintered gas dispersion tubes enable rapid deoxygenation via high-efficiency micro-bubbling, alongside continuous headspace inert blanketing without surface solution agitation during measurement sweeps.
  • Modular Universal Port Accessibility: Standardized ground joints (such as 14/20, 19/22, and 24/29) and threaded bushings accommodate diverse electrode diameters, optical quartz inspection windows, external condenser columns, and analytical sensor probes simultaneously.
  • Optical In-Situ Interfacing: High-transmission flat optical quartz windows facilitate direct integration with Raman spectrometers, UV-Vis light guides, or microscope objectives, enabling synchronized in-situ spectroscopic and morphological tracking of interfacial electrochemical processes.
  • Ergonomic Maintenance and Decontamination: Threaded modular components and tool-free disassembly mechanisms allow rapid cleaning, chemical sterilization, and quick replacement of fragile frits or diaphragms, drastically shortening inter-test cycle turnaround times.

Applications

Application Description Key Benefit
Electrocatalyst Screening (HER/OER/ORR) Evaluation of advanced water-splitting catalysts and oxygen reduction reaction kinetics in acidic or alkaline media using gas-purged three-electrode assemblies. Delivers negligible ohmic drop and ultra-low background noise for accurate kinetic overpotential and Tafel slope measurements.
Battery & Energy Storage R&D Characterization of next-generation lithium, sodium, and zinc battery electrolyte formulations, solid-electrolyte interphase (SEI) growth, and charge-discharge dynamics. Hermetic sealing prevents electrolyte volatilization and moisture ingress, preserving ultra-dry conditions for air-sensitive chemistries.
Accelerated Corrosion & Passivation Testing Potentiodynamic polarization and EIS analysis of structural metals, coatings, and marine alloys exposed to simulated saline or industrial chemical environments. Rigid Luggin capillary positioning guarantees reproducible polarization curves and precise determination of pitting and breakdown potentials.
Carbon Dioxide (CO2) Electroreduction Selective reduction of carbon dioxide into synthetic fuels and chemical feedstocks using divided cell architectures under controlled gas flow conditions. Divided cell configuration with selective membrane clamping eliminates anolyte oxidation of cathode-generated organic reaction products.
Electroorganic Synthesis & Electrosynthesis Controlled-potential organic functional group transformations, radical couplings, and paired electrosynthetic processing at bench scale. Multi-port architecture accommodates high-surface-area working electrodes and continuous reagent dosing without breaking chamber atmosphere.
Biosensing & Environmental Electroanalysis Trace-level detection of heavy metal ions, pesticide residues, and biochemical biomarkers using strip-plate, disc, or microelectrode assemblies. Optical-grade vessel walls paired with inert PTFE caps yield minimal chemical leaching and zero analyte adsorption on cell surfaces.
Photochemical & Photoelectrochemical Cells Sunlight-driven water splitting and solar fuel generation coupling semiconductor photoanodes with optical quartz windows. High-transmission quartz transmission planes maximize incident photon efficiency while providing stable spatial alignment.

Technical Specifications

Parameter Category Specification Details (Model Series KT-DJ)
Base Model Series Identifier KT-DJ
Cell Body Construction Materials Annealed Schott Borosilicate 3.3 Glass / High-Purity Synthetic Quartz (JGS1)
Cap & Internal Component Materials Virgin PTFE / Medical-Grade PEEK / 316L Stainless Steel (Optional)
Standard Nominal Chamber Volumes 10 mL, 25 mL, 50 mL, 100 mL, 150 mL, 250 mL, 500 mL (Custom options up to 2000 mL)
Cell Architecture Configurations Single-Chamber Undivided, H-Type Divided (Membrane Clamped), Jacketed Thermostatic, Optical In-Situ
Separation Diaphragm Options (Divided) Ion-Exchange Membrane (Nafion/Anion), Sintered Glass Frit (Porosity G1 to G4), PEEK Micro-Mesh
Operating Temperature Range -20°C to +150°C (Standard Borosilicate/PTFE); -40°C to +250°C (Quartz/PEEK)
Temperature Uniformity (Jacketed) ±0.1°C across working zone via recirculating bath coupling
Hermetic Sealing Pressure Rating Up to 0.2 MPa (2 bar) positive pressure; Full vacuum down to 10⁻² mbar
Standard Sealing O-Ring Formulations Fluorocarbon Elastomer (Viton) Standard; Perfluoroelastomer (FFKM) Optional
Port Geometry & Joint Standards Ground Joints (10/19, 14/20, 19/22, 24/29) and Adjustable M9/M14/M16 Threaded PEEK Bushings
Standard Port Allocation Working Electrode (1x), Counter Electrode (1x), Reference Luggin Well (1x), Gas In/Out (2x), Temperature Well (1x)
Reference Well Capillary Outer Diameter 1.0 mm to 3.0 mm adjustable fine-tip Luggin-Haber capillary with ceramic/porous core
Optical Quartz Window Transmission ≥ 92% transmission across 200 nm – 2500 nm UV-Vis-NIR spectral range
Chemical Compatibility Concentrated acids (HCl, H₂SO₄, HNO₃), alkaline solutions (KOH, NaOH), organic solvents (acetonitrile, DMF, DMSO, PC)

Why Choose This Product

  • Industrial-Grade Manufacturing Precision: Every glass and quartz vessel is annealed according to strict thermal schedules to relieve internal mechanical stresses, ensuring high burst resistance and total dimensional consistency across production lots.
  • Zero-Contamination Fluidic Design: Precision CNC-machined virgin PTFE and PEEK cell caps eliminate the risk of plasticizer leaching, metallic ion contamination, or chemical degradation during sensitive analytical and high-purity battery testing.
  • Exceptional Experimental Reproducibility: Fixed-port geometries, micrometric Luggin capillary alignment, and standardized electrode spacings guarantee that experimental baseline curves remain dependable from operator to operator and run to run.
  • Modular and Adaptable Architecture: The universal port configuration allows quick interchanging of standard plate, wire, and disc electrodes, optical probes, and condenser columns without requiring proprietary adapter hardware.
  • Comprehensive Engineering & Customization Support: Backed by specialized technical consulting, custom port placement, bespoke chamber volumes, and complete integration with laboratory potentiostats, ensuring complete alignment with your specialized electrochemical protocol.

Contact our technical sales team today to request a quotation, discuss custom dimensional modifications, or select the ideal electrochemical configuration for your laboratory research requirements.

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Product Datasheet

Electrochemical Electrolytic Cell for Laboratory Research and Testing

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Assay Equipment Accessories & Consumables


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