Products Thermal Equipment Atmosphere Furnace Controlled Nitrogen Inert Hydrogen Atmosphere Furnace
Controlled Nitrogen Inert Hydrogen Atmosphere Furnace

Atmosphere Furnace

Controlled Nitrogen Inert Hydrogen Atmosphere Furnace

Item Number : KT-16AH

Price varies based on specs and customizations


Max. temperature
1600 ℃
Constant work temperature
1500 ℃
Vacuum pressure
0.1 Mpa
Effective volume
4.5-64 L
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Introduction

The Hydrogen Atmosphere Furnace is a specialized heating device designed for sintering or annealing materials in a controlled hydrogen or inert gas environment, adjustable up to 1600°C. It features a double-shell structure with air and water cooling systems, high-purity molybdenum wire heating elements, and advanced safety mechanisms including automatic hydrogen tail gas ignition and pressure control systems. Ideal for processing materials like optical materials and titanium alloys, this furnace ensures precise and safe operation in reducing or inert gas atmospheres.

Applications

The Hydrogen Atmosphere Furnace is a specialized equipment designed for various high-temperature processes that require a controlled environment, particularly in the presence of hydrogen or inert gases. This furnace is ideal for applications where the prevention of oxidation or other chemical reactions is crucial, ensuring the integrity and quality of the materials being processed. Below are the main application areas of this product:

  • Sintering of Advanced Materials: Ideal for the consolidation of powders into solid materials, especially for high-performance ceramics and metals that require a specific atmosphere to prevent oxidation.
  • Annealing Processes: Used for the controlled heating and cooling of materials, particularly metals, to remove internal stresses, soften materials, or alter electrical properties.
  • Heat Treatment of Titanium Alloys: Essential for the thermal processing of titanium and its alloys in a controlled hydrogen or inert gas environment to enhance mechanical properties and prevent surface contamination.
  • Processing of Optical Materials: Particularly useful for the sintering and annealing of optical materials like phosphors and other luminescent materials that require a clean, controlled atmosphere to maintain optical clarity and performance.
  • Research and Development: Widely used in laboratories and research facilities for experiments involving high-temperature reactions in controlled atmospheres, aiding in the development of new materials and processes.
  • Manufacturing of Electronic Components: Critical for the production of semiconductors and other electronic components that require precise temperature control and a clean environment to ensure high performance and reliability.

Detail & Parts

Hydrogen atmosphere furnace detail 1
The hydrogen atmosphere furnace is specially designed for sintering or annealing materials in a hydrogen environment or an inert gas environment. It uses alumina fiber as the furnace body material, molybdenum wire as the heating element, and a cooling water pipe is embedded in the sealing plate on the top of the furnace body to ensure the sealing of the instrument during operation. For materials that need to be sintered in an inert gas or reducing gas environment (such as fluorescent materials, titanium alloys, etc.), this electric furnace is a very good choice.

Hydrogen atmosphere furnace detail 2

Hydrogen atmosphere furnace detail 3Hydrogen atmosphere furnace detail 3

Double-shell structure
Double-shell structure: It adopts a double-layer shell structure with air cooling and water cooling systems to maintain the positive pressure inside the cavity up to 0.02MP and the negative pressure up to -0.1MP.
Flowmeter
Flowmeter: The furnace body is equipped with two large-range flowmeters (N2:0~3.5L/minH2:0~3.5L/min). The float flowmeter can freely control the gas flow entering the furnace body.
Hydrogen safety device
Hydrogen safety device: The flame detector will automatically ignite. If ignition fails, the hydrogen gas inlet will be automatically cut off, the nitrogen gas inlet valve will be opened, and nitrogen gas will be forcibly charged to ensure the safety of the electric furnace.

Features

The Hydrogen Atmosphere Furnace is a specialized heating device designed to provide precise control over the environment during sintering or annealing processes. This furnace is particularly beneficial for materials that require processing in a hydrogen or inert gas environment, such as optical materials and titanium alloys. Here are the key features that enhance its functionality and safety:

  • Double-Shell Structure with Advanced Cooling Systems: The furnace features a double-layer shell design that incorporates both air and water cooling systems. This setup ensures a stable internal pressure ranging from 0.02MPa positive to -0.1MPa negative, maintaining optimal conditions for the materials being processed.
  • High Precision Flow Meters: Equipped with two large-range flow meters for nitrogen and hydrogen (each ranging from 0 to 3.5L/min), the furnace allows for precise control over the gas flow rates. This feature is crucial for maintaining the desired atmosphere composition and ensuring consistent results.
  • Comprehensive Hydrogen Safety Mechanism: Safety is paramount in environments involving hydrogen. The furnace includes a hydrogen safety device that automatically ignites hydrogen tail gas. In case of ignition failure, the system is designed to cut off the hydrogen supply, open the nitrogen valve, and force nitrogen into the furnace, thereby preventing any hazardous situations.
  • High Purity Molybdenum Heating Element: Utilizing a high purity molybdenum wire (99.99% molybdenum content), the heating element ensures uniform and efficient heating, which is essential for achieving high-quality sintering and annealing results.
  • Temperature Flexibility: With an adjustable working temperature range from 0 to 1600°C, this furnace accommodates a wide variety of materials and processes, making it a versatile tool in the laboratory or industrial setting.

Principle

Hydrogen atmosphere furnaces utilize a ceramic tube with leak-tight flanges to enable heat treatment up to 1600 °C in a hydrogen atmosphere. Prior to introducing hydrogen gas, the tube is flooded with inert gas for safety. The flooding tank system, pressurized with inert gas, purges remaining oxygen from the tube before heat treatment. The gas outlet system connects to an afterburner to combust outgoing hydrogen. Exothermic hydrogen atmospheres reduce surface oxides, improving the wetting properties and flow of filler material during brazing.

Advantages

Hydrogen Atmosphere Furnaces offer a range of benefits that make them a superior choice for high-temperature processes. Here are some of the key advantages:

  • Enhanced Oxygen Exclusion: The pressurized environment of the furnace ensures that oxygen cannot enter under any circumstances, providing a completely controlled atmosphere for sensitive processes.
  • Maximized Reductive Power: With more reactive hydrogen molecules available compared to partial pressure atmospheres, these furnaces maximize the reductive power, crucial for processes requiring a strong reducing environment.
  • Versatility with Hydrogen Mixtures: The ability to use mixtures of inert gases like nitrogen or argon with hydrogen offers a valuable alternative. These mixtures retain some of the reducing capabilities of pure hydrogen atmospheres while potentially reducing operating and investment costs.
  • Advanced Safety Features: Equipped with a fully automated flow controller and devices adhering to SIL2 standards, the system ensures safety and reliability. A hydrogen sensor at the top of the furnace immediately responds to any leaks, triggering a switch to inert gas and securing the system.
  • User-Friendly Interface: The intuitive touch panel interface simplifies operation and control, making it accessible for users of varying technical backgrounds.
  • Flexibility in Temperature and Space: These furnaces can be adapted to different usable spaces and temperatures, with options like cold wall furnaces available for requirements exceeding 1800 °C.
  • Sealing Efficiency: The inclusion of a high-temperature-resistant silica gel seal ring on the furnace door ensures excellent sealing, allowing for the creation of a vacuum and various other atmospheres, enhancing the versatility of the furnace.

Technical specifications

Furnace model KT-16AH
Max. temperature 1600℃
Constant work temperature 1500℃
Vacuum pressure 0.1Mpa
Vacuum valve Needle valve
Chamber material Japan alumina fiber
Heating element Molybdenum wire
Heating rate 0-20℃/min
Temperature sensor B type thermal couple
Temperature controller  Touch screen PID controller
Temperature control accuracy ±1℃
Temperature uniformity ±5℃
Electric power supply AC110-220V,50/60HZ
Standard Chamber Sizes Stocks
Chamber size  (mm) Effective volume  (L) Chamber size  (mm) Effective volume  (L)
150x150x200 4.5 300x300x400 36
200x200x300 12 400x400x400 64
Customer design sizes and volume is accepted
Standard Temperature controlling
  • PID automatic control via SCR (Silicon Controlled Rectifier) power control with phase angle fired, current limiting resistor.
  • 51 programmable segments for precise control of heating rate, cooling rate and dwell time.
  • Built in PID Auto-Tune function with overheating & broken Thermocouple broken protection.
  • Over temperature protection and alarm allows for operation without attendant
Optional of Temperature controlling
  • Software (Furnace can be operated by PC by installing a control software)
  • Touch screen temperature controller
Furnace structure Double layer steel casing with dual cooling fan, surface temperature below 60℃
Furnace door
  • Power cutting off when furnace door open
Warranty
  • For this hydrogen furnace, One year limited warranty with life time support. (Consumable parts such as heating elements and crucibles are not covered by the warranty, please order the replacement at related products)
  • ATTENTION: Any damages caused by the use of corrosive and acidic gases are not under the coverage of One Year Limited Warranty.
Hydrogen Furnace Using Attentions
  • Cooling rate shall also not exceed 10℃/min.
  • Toxic or explosive gases are not recommended for use with this furnace without necessary safety controls and supervision.
  • Small cracks may appear on the surface of the refractory ceramics over extended use. This is a normal occurrence and the cracks may be repaired with alumina coating.
  • Refractory door block must be inserted before closing door.

Warnings

Operator safety is the top important issue! Please operate the equipment with cautions. Working with inflammable& explosive or toxic gases is very dangerous, operators must take all necessary precautions before starting the equipment. Working with positive pressure inside the reactors or chambers is dangerous, operator must fellow the safety procedures strictly. Extra caution must also be taken when operating with air-reactive materials, especially under vacuum. A leak can draw air into the apparatus and cause a violent reaction to occur.

Designed for You

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View more faqs for this product

4.8

out of

5

I'm very satisfied with this Hydrogen atmosphere furnace. It's a high-quality product with a reasonable price. The delivery was fast and the customer service was excellent.

Vickie Mcfarland

4.9

out of

5

This furnace is a lifesaver for our lab. It's easy to use and maintain, and it provides consistent results. We've been using it for over a year now and it's still going strong.

Curtis Hughes

4.7

out of

5

I highly recommend this Hydrogen atmosphere furnace. It's a great value for the money and it's made with high-quality materials. We've been using it for several months now and we've had no problems with it.

Sophia Mckinney

5.0

out of

5

This furnace is a game-changer for our lab. It's so easy to use and it produces consistent results. We've been using it for a few months now and we're very happy with it.

Jason Glover

4.6

out of

5

I'm really impressed with this Hydrogen atmosphere furnace. It's well-made and it works great. I've been using it for a few weeks now and I've had no problems with it.

Isabella Turner

4.9

out of

5

This furnace is a great addition to our lab. It's easy to use and it provides consistent results. We've been using it for a few months now and we're very happy with it.

Elijah King

5.0

out of

5

I'm so glad I bought this Hydrogen atmosphere furnace. It's made my work so much easier. It's easy to use and it produces consistent results. I highly recommend it.

Natalie Phillips

4.8

out of

5

This furnace is a great value for the money. It's well-made and it works great. I've been using it for a few months now and I've had no problems with it.

Lucas Martinez

4.7

out of

5

I'm very happy with this Hydrogen atmosphere furnace. It's a great product and it's made my work so much easier. I highly recommend it.

Mia Campbell

4.6

out of

5

This furnace is a great addition to our lab. It's easy to use and it provides consistent results. We've been using it for a few months now and we're very happy with it.

Benjamin Roberts

5.0

out of

5

I'm so glad I bought this Hydrogen atmosphere furnace. It's made my work so much easier. It's easy to use and it produces consistent results. I highly recommend it.

Amelia Harrison

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