Products Thermal Equipment Vacuum Hot Press Furnace Spark plasma sintering furnace SPS furnace
Spark plasma sintering furnace SPS furnace

Vacuum Hot Press Furnace

Spark plasma sintering furnace SPS furnace

Item Number : KTSP

Price varies based on specs and customizations


Output current
0-30000 A
Rated temperature
2300 ℃
Rated pressure
100-500 KN
Sample size
Ø30-Ø200 mm
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Introduction

Spark Plasma Sintering (SPS) is a rapid material preparation method that utilizes pulsed current to sinter materials directly in a mold. It combines plasma activation, hot pressing, and resistance heating, offering several advantages over traditional sintering methods. SPS enables uniform heating, high heating rates, low sintering temperatures, short sintering times, and high production efficiency. It also purifies surfaces, inhibits grain growth, and facilitates the production of uniform and controllable structures. Compared to conventional sintering, SPS is environmentally friendly, cost-effective, and requires minimal operation time.

Application

Spark Plasma Sintering (SPS) furnaces offer a wide range of applications in various industries, including:

  • Materials Science: Sintering of metals, intermetallic compounds, refractory metals, hard alloys, high entropy alloys, and nanomaterials
  • Ceramic Materials: Sintering of ceramic materials, porous materials, metal glass materials, and functionally gradient materials
  • Advanced Materials: Preparation of cutting-edge composites, multi-element materials, and materials for biological use
  • Manufacturing: Solid phase diffusion connection between blocks with high product strength and air tightness
  • Detail & Parts

Features

The Spark Plasma Sintering Furnace (SPS) is a high-speed metal sintering furnace with many benefits for customers. These include:

  • Astonishing sintering speed: The SPS furnace uses pulsed DC to repeatedly energize the material with instantaneous high current, which drastically reduces sintering time.
  • Superior output compactness: The SPS furnace produces sintered materials with high density and compactness.
  • Small floor space: The SPS furnace has a compact design that occupies minimal floor space.
  • Fast deployment: The SPS furnace can be quickly and easily deployed, making it a great choice for businesses that need to get up and running quickly.
  • Industry-proven solution: The SPS furnace is a proven solution for sintering a wide variety of materials, including nanophase materials, functionally graded material (FGM), nanoscale thermoelectric materials, rare earth permanent magnets, target materials, nonequilibrium materials, and medical implants.

 

product details

product details

product details

Principle

Spark Plasma Sintering (SPS) is a rapid material preparation method that combines plasma activation, hot pressing, and resistance heating. It involves passing a pulse current directly through the mold and powder particles or bulk samples to induce sintering.

SPS utilizes the Joule heat generated by the current flow to heat the sample. The current passing through the powder creates spark discharge between adjacent particles, ionizing gas molecules and generating positrons and electrons. The resulting plasma purifies and activates the particle surfaces, promoting material migration and reducing sintering temperature and time.

The pulse current voltage applied provides high energy density, enabling rapid sintering and dispersion of the discharge point. This unique heating mode facilitates rapid cooling within the crystal structure, allowing for the preparation of high-quality amorphous and nano materials.

 Advantages

  • Rapid Sintering: SPS furnaces offer exceptionally fast heating rates, drastically reducing sintering time compared to traditional methods.
  • Compact Structure: The compact design of SPS furnaces minimizes floor space requirements, enabling efficient deployment.
  • Uniform Heating: SPS furnaces deliver uniform heating throughout the sample, ensuring consistent sintering results.
  • High Heating Rate: The high heating rate of SPS furnaces enables rapid temperature increases, allowing for shorter processing times.
  • Low Sintering Temperature: SPS furnaces operate at lower sintering temperatures than traditional methods, preserving material integrity.
  • Surface Purification: The plasma discharge in SPS furnaces purifies the surface of particles, removing impurities and enhancing bonding.
  • Grain Growth Inhibition: SPS furnaces minimize grain growth, resulting in a uniform and controllable product structure.
  • Versatile Material Compatibility: SPS furnaces can sinter a wide range of materials, including metals, alloys, ceramics, and composites.
  • Environmental Sustainability: SPS technology is environmentally friendly, reducing energy consumption and waste generation.
  • Cost-Effectiveness: SPS furnaces offer a cost-effective solution for high-speed sintering, reducing production time and expenses.
  • Solid-State Diffusion Bonding: SPS furnaces enable solid-state diffusion bonding between materials, providing high product strength and airtightness.
  • Advanced Material Synthesis: SPS furnaces facilitate the synthesis of advanced materials, such as nanomaterials, functionally graded materials, and rare earth magnets.

Technical parameters

Spark Plasma Sintering Furnace (SPS) upto 20 Ton pressure and 1600ºC , is a Spark Plasma Sintering System is designed for a wide range of material research upto 1600ºC. It can be used for sintering, sinter-bonding, surface treatment, and synthesis. The sample material can be metals, ceramics, nanostructured material and amorphous material. This system is perfectly fit solid electrolyte and electric thermal  material research.

Configuration
  • Stainless Steel Chamber - Suitable for Controlled Inert Gas or Vacuum Condition
  • Sintering Press Unit
  • Sintering DC Pulse Generator
  • Vacuum Unit
  • Sintering Control Unit
Temperature controller
  • Precision Eurotherm temperature controller is built in
  • Overshooting temperature is less than 5ºC at the feast heating rate
  • Temperature accuracy : < 0.1ºC
Hydraulic Press
  • Manual operated hydraulic press to apply pressure.
  • Max pressure: 20 T
  • Digital Pressure gauge is built in with over-pressure alarm.
Vacuum Chamber
  • Vertical vacuum Chamber
  • Inner Double Layers Stainless Steel Reflectors
  • Rotary Pump included
Dimension
  • Power Supply :760 L X 460 W X 1820 H,  mm   
  • Furnace:           970 L X 720 W X 1400 H, mm

Technical specifications

Model KTSP-10T-5 KTSP-20T-6 KTSP-20T-10 KTSP-50T-30
Rated power 50Kw 60Kw 100Kw 300Kw
Output current 0-5000A 0-6000A 0-10000A 0-30000A
Input voltage 0-10V 0-10V 0-10V 0-10V
Rated temperature 2300℃
Rated pressure 100KN 200KN 200KN 500KN
Sample size Ø30mm Ø50mm Ø100mm Ø200mm
Ram stroke 100mm 100mm 100mm 200mm
Ultimate vacuum 1Pa

Warnings

Operator safety is the top important issue! Please operate the equipment with cautions. Working with inflammable& explosive or toxic gases is very dangerous, operators must take all necessary precautions before starting the equipment. Working with positive pressure inside the reactors or chambers is dangerous, operator must fellow the safety procedures strictly. Extra caution must also be taken when operating with air-reactive materials, especially under vacuum. A leak can draw air into the apparatus and cause a violent reaction to occur.

Designed for You

KinTek provide deep custom made service and equipment to worldwide customers, our specialized teamwork and rich experienced engineers are capable to undertake the custom tailoring hardware and software equipment requirements, and help our customer to build up the exclusive and personalized equipment and solution!

Would you please drop your ideas to us, our engineers are ready for you now!

FAQ

What is the purpose of a vacuum hot press furnace?

The purpose of a vacuum hot press furnace is to combine vacuum or atmosphere, hot pressing, and high-temperature sintering to form new materials. It can be used in the vacuum sintering of transparent ceramics, industrial ceramics, and metals, as well as the high-temperature sintering of ceramic materials such as silicon carbide and silicon nitride. Additionally, it can be used for the heat treatment of powders and compacts at a temperature lower than the melting point of the main components, which improves their strength through metallurgical combination between particles. The finished materials have improved mechanical, electronic, and thermal properties.

What are the advantages of a vacuum hot press furnace?

Advantages of a vacuum hot press furnace include hot pressing sintering of metal and ceramic powders, preparation of ceramic/metal composites and intermetallic compounds, research and development of diffusion welding process, and densification hot press sintering of oxygen/nitrogen/boron/carbon compounds and their mixtures. The high temperature and pressure under vacuum or atmosphere help to bond raw materials solid particles together, decrease voids and grain boundaries, and improve the mechanical, electronic, and thermal properties of finished materials.

How does a vacuum hot press furnace work?

A vacuum hot press furnace is a piece of equipment that combines vacuum, hot pressing, and high-temperature sintering. It works by heating and pressurizing materials under vacuum or atmosphere to create a compact polycrystalline sintered body with improved mechanical, electronic, and thermal properties. The furnace is composed of several systems including furnace body, heating and heat preservation, temperature measurement system, vacuum system, air charging system, water cooling system, control system, and pressure system. Heating elements can be graphite heater, molybdenum heater, or induction heating, and one-way or two-way pressurization can be used for hydraulic pressurization.

What are the common applications of vacuum hot press furnaces?

Vacuum hot press furnaces have various applications in industries such as aerospace, automotive, electronics, and materials research. They are used for the production of advanced ceramics, such as ceramic matrix composites and sintered carbides, which are used in high-temperature applications. These furnaces are also utilized for the fabrication of metallic alloys, superalloys, and intermetallic compounds with tailored properties. Vacuum hot press furnaces play a crucial role in the production of diamond tools and cutting inserts, as well as in the development of advanced electronic materials and components. Additionally, these furnaces are employed in research laboratories for the synthesis and processing of novel materials with unique properties.

What factors should be considered when selecting a vacuum hot press furnace?

When selecting a vacuum hot press furnace, several factors need to be considered. Firstly, the size and capacity of the furnace should align with the intended application and production requirements. The furnace should accommodate the size and number of samples or components to be processed. The heating and pressure capabilities of the furnace should also be evaluated to ensure they meet the desired temperature and pressure conditions. It is important to consider the level of automation and control systems available, as well as the compatibility with specific materials and processes. Additionally, the reliability, service support, and overall cost of ownership should be assessed. Consulting with manufacturers and experts in the field can help in selecting the most suitable vacuum hot press furnace for specific processing needs.
View more faqs for this product

4.9

out of

5

The SPS furnace has brought about a remarkable improvement in our research capabilities, enabling us to conduct experiments and obtain results in a fraction of the time.

Ainsley Alhassan

4.8

out of

5

This sintering furnace is a game-changer. Its speed, efficiency, and versatility have made it an indispensable tool in our lab, allowing us to explore new materials and processes.

Carolina Sotomayor

4.7

out of

5

The SPS furnace is a well-built and reliable piece of equipment. Its user-friendly design and safety features make it an excellent choice for our research lab.

Dexter De La Cruz

4.9

out of

5

The SPS furnace has exceeded our expectations. The quality of the sintered materials is exceptional, and the furnace's durability ensures consistent performance.

Eleanor Abiodun

4.8

out of

5

The SPS furnace offers exceptional value for money. Its cost-effectiveness, combined with its high performance, makes it an attractive investment for any research institution.

Felix Andersson

4.7

out of

5

The SPS furnace is a testament to technological advancement. Its innovative features and groundbreaking capabilities have opened up new avenues of research for our team.

Georgeta Grigore

4.9

out of

5

The SPS furnace has significantly enhanced our research productivity. Its rapid sintering process has enabled us to complete experiments in a timely manner, leading to accelerated progress.

Harriet Akhtar

4.8

out of

5

The SPS furnace is a versatile tool that has facilitated the exploration of diverse materials and applications. Its ability to handle various materials sets it apart from other sintering furnaces.

Ignacio Silva

4.7

out of

5

The SPS furnace is an invaluable asset to our lab. Its speed, reliability, and ease of use have made it a favorite among our researchers.

Josefa Andreescu

4.9

out of

5

The SPS furnace is a remarkable piece of equipment. Its ability to produce high-quality sintered materials in a matter of minutes is truly impressive.

Konstantin Ivanov

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