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Split Chamber CVD Tube Furnace with Vacuum Station Chemical Vapor Deposition System Equipment Machine

CVD & PECVD Furnace

Split Chamber CVD Tube Furnace with Vacuum Station Chemical Vapor Deposition System Equipment Machine

Item Number : KT-CTF12

Price varies based on specs and customizations


Max. temperature
1200 ℃
Constant work temperature
1100 ℃
Furnace tube diameter
60 mm
Heating zone length
1x450 mm
Heating rate
0-20 ℃/min
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Introduction

The Split Chamber CVD Tube Furnace With Vacuum Station is a versatile and high-performance laboratory equipment designed for chemical vapor deposition (CVD) applications. It features a split furnace chamber that allows for easy access to reaction samples and rapid cooling. The furnace tube is made of high-temperature quartz and has a diameter of 60 mm. The system includes a 4-channel MFC mass flow meter with source gases of CH4, H2, O2, and N2, providing precise control over gas flow rates. The vacuum station features a 4L/S rotary vane vacuum pump, achieving a maximum vacuum pressure of 10 Pa. With its advanced features and capabilities, the Split Chamber CVD Tube Furnace With Vacuum Station is an ideal choice for various research and development applications in materials science, semiconductor processing, and other fields.

Detail&Parts

1200C CVD machine with turbo high vacuum pump
1200C CVD machine with turbo high vacuum pump
1600C CVD furnace with turbo vacuum pump station
1600C CVD furnace with turbo vacuum pump station
Split CVD furnace with large quartz tube
Split CVD furnace with large quartz tube
High temperature CVD furnace with integrated  controller
High temperature CVD furnace with integrated  controller

Applications

The Split Chamber CVD Tube Furnace With Vacuum Station CVD Machine is a versatile and advanced piece of equipment designed for a variety of applications in the fields of material science, semiconductor manufacturing, and research and development. This machine is particularly useful for processes that require precise control over temperature, gas flow, and vacuum levels, making it an essential tool for high-quality material synthesis and processing.

  • Nanomaterial Synthesis: The furnace is ideal for the growth of nanowires, nanofilms, and other nanostructured materials, which are crucial in the development of advanced electronic and optoelectronic devices.
  • Vacuum Coating: It is extensively used for the deposition of thin films on various substrates, including metal films, ceramic films, and composite films, which are essential for enhancing the properties of materials in applications such as optics and electronics.
  • Battery Material Processing: The furnace is suitable for the drying and sintering of battery materials, which is a critical step in the production of high-performance batteries.
  • Material Drying and Sintering: It is used in the high-temperature sintering of ceramics, refractory materials, and specialty materials, ensuring the consolidation and densification of these materials.
  • Atmosphere and Vacuum Heat Treatment: The vertical tube furnace configuration allows for quenching, annealing, and tempering of small steel parts, as well as vertical CVD coating, making it a valuable asset in metallurgical processes.
  • Research and Development: It is widely used in universities, research institutes, and industrial and mining enterprises for conducting high-temperature experiments, atmosphere sintering, reducing atmosphere, and CVD/CVI experiments, contributing to the advancement of material science and technology.

Features

The Split Chamber CVD Tube Furnace With Vacuum Station CVD Machine is a sophisticated piece of equipment designed for advanced chemical vapor deposition (CVD) processes. This furnace integrates cutting-edge technology to enhance the efficiency and quality of film deposition, making it ideal for research and industrial applications. Here are the key features and their benefits:

  • High Film Deposition Rate: Utilizing radio frequency glow technology, this furnace significantly boosts the film deposition rate, reaching up to 10Å/S. This rapid deposition is crucial for high-throughput production and research, saving time and increasing productivity.
  • Large Area Uniformity: With advanced multi-point RF feed technology and specialized gas path distribution, the furnace ensures film uniformity of up to 8%. This uniformity is essential for creating consistent and high-quality coatings across large substrates, enhancing the reliability of the materials produced.
  • Consistent Deposition: The design incorporates advanced semiconductor industry concepts, resulting in a deviation of less than 2% between substrates. This high level of consistency is vital for applications requiring precise and repeatable results, such as in the production of electronic components.
  • Stable Process Control: The equipment's high stability ensures the continuity and consistency of the CVD process. This reliability is critical for maintaining process integrity and reducing the risk of defects or failures during operation.
  • Intelligent Control System: Patented by Bonage, the integrated control system includes a high-performance temperature control system that uses a closed-loop negative feedback mechanism. This system, combined with high-quality imported electrical components, enhances the overall performance and reliability of the equipment, making it virtually maintenance-free.
  • Versatile Applications: Suitable for depositing various types of films, including metal, ceramic, and composite films, the furnace supports continuous growth processes and can be easily expanded with additional functions like plasma cleaning and etching. This versatility makes it a valuable asset for diverse research and production needs.

Principle

The Split Chamber CVD Tube Furnace With Vacuum Station CVD Machine is a high-temperature vacuum furnace used for chemical vapor deposition (CVD) processes. CVD is a process in which a thin film of material is deposited on a substrate by the chemical reaction of a gas or vapor. The Split Chamber CVD Tube Furnace With Vacuum Station CVD Machine uses a split furnace chamber to allow for easy access to the substrate during the CVD process. The vacuum station is used to create a vacuum in the furnace chamber, which helps to remove impurities and improve the quality of the deposited film.

Advantages

  • Intuitive sample observation and rapid cooling: Split furnace chamber allows for direct observation of reaction samples and quick cooling.
  • High temperature capability: Max working temperature of up to 1200℃ for versatile applications.
  • Precise gas control: 4-channel MFC mass flow meter with CH4, H2, O2, and N2 sources ensures accurate and stable gas supply.
  • Vacuum compatibility: Vacuum station with a 4L/S rotary vane vacuum pump achieves a maximum vacuum pressure of up to 10Pa, enabling various vacuum processes.
  • High-speed heating and cooling: Furnace chamber sliding system facilitates rapid heating and cooling for efficient sample processing.
  • Advanced temperature control: PID programmable temperature control with excellent accuracy, remote control, and centralized control capabilities.
  • User-friendly interface: CTF Pro controller with a 7-inch TFT touch screen offers intuitive program setting and data analysis.
  • Versatile vacuum setup: Stainless steel vacuum flange with adaptable ports accommodates different vacuum pump stations for customized vacuum environments.
  • Energy efficiency: Water cooling system and gas afterflow design minimize energy consumption.
  • Wide applicability: Suitable for CVD, diffusion, and other thermo-treatments under vacuum and atmosphere protection.

Safety Advantage

  • Kindle Tech tube furnace owns over current protection and over temperature alarming function, furnace will turn off the power automatically
  • Furnace build in thermal couple detecting function, furnace will stop heating and alarm will be on once broken or failure detected
  • KT-CTF12 Pro support power failure restarting function,furnace will resume the furnace heating program when power is incoming after failure

Technical specifications

Furnace model KT-CTF12-60
Max. temperature 1200℃
Constant work temperature 1100℃
Furnace tube material High purity quartz
Furnace tube diameter 60mm
Heating zone length 1x450mm
Chamber material Japan alumina fiber
Heating element Cr2Al2Mo2 wire coil
Heating rate 0-20℃/min
Thermal couple Build in K type
Temperature controller Digital PID controller/Touch screen PID controller
Temperature control accuracy ±1℃
Sliding distance 600mm
Gas precise control unit
Flow meter MFC mass flow meter
Gas channels 4 channels
Flow rate MFC1: 0-5SCCM O2
MFC2: 0-20SCMCH4
MFC3: 0- 100SCCM H2
MFC4: 0-500 SCCM N2
Linearity ±0.5% F.S.
Repeatability ±0.2% F.S.
 Pipe line and valve Stainless steel
Maximum Operating Pressure 0.45MPa
Flow meter controller Digital Knob controller/Touch screen controller
Standard vacuum unit (Optional)
Vacuum pump Rotary vane vacuum pump
Pump flow rate 4L/S
Vacuum suction port KF25
Vacuum gauge Pirani/Resistance silicon vacuum gauge
Rated vacuum pressure 10Pa
High vacuum unit(Optional)
Vacuum pump Rotary vane pump+Molecular pump
Pump flow rate 4L/S+110L/S
Vacuum suction port KF25
Vacuum gauge Compound vacuum gauge
Rated vacuum pressure 6x10-5Pa
Above specifications and setups can be customized

Standard Package

No. Description Quantity
1 Furnace 1
2 Quartz tube 1
3 Vacuum flange 2
4 Tube thermal block 2
5 Tube thermal block hook 1
6 Heat resistant glove 1
7 Precise gas control 1
8 Vacuum unit 1
9 Operation manual 1

Optional Setup

  • In tube gases detecting and monitoring,like H2, O2 and so on
  • Independent furnace temperature monitoring and recording
  • RS 485 communication port for PC remote control and data exporting
  • Insert gases feeding flow rate control,like mass flowmeter and float flowmeter
  • Touch screen temperature controller with versatile operator friendly functions
  • High vacuum pump station setups, like vane vacuum pump,molecular pump,diffusion pump

Warnings

Operator safety is the top important issue! Please operate the equipment with cautions. Working with inflammable& explosive or toxic gases is very dangerous, operators must take all necessary precautions before starting the equipment. Working with positive pressure inside the reactors or chambers is dangerous, operator must fellow the safety procedures strictly. Extra caution must also be taken when operating with air-reactive materials, especially under vacuum. A leak can draw air into the apparatus and cause a violent reaction to occur.

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FAQ

What Is CVD Furnace?

Chemical vapor deposition (CVD) is a technology that uses various energy sources such as heating, plasma excitation or light radiation to chemically react gaseous or vapor chemical substances on the gas phase or gas-solid interface to form solid deposits in the reactor by means of chemical reaction.To put it simply, two or more gaseous raw materials are introduced into a reaction chamber, and then they react with each other to form a new material and deposit it on the substrate surface.

CVD furnace is one combined furnace system with high temperature tube furnace unit,gases control unit, and vacuum unit, it is widely used for experiment and production of composite material preparation, microelectronics process, semiconductor optoelectronic, solar energy utilization, optical fiber communication, superconductor technology, protective coating field.

What Is A Tube Furnace?

Laboratory tube furnace is one classic external heating high temperature tube furnace, also named hot wall heating furnace.

According to the different working temperature, furnace tube material usually can be transparent quartz tubes, high purity alumina ceramic tubes and high strength metal alloy tubes.

To meet different thermal researching purposes, tube furnace can be designed with multi heating zones, so as to have a flexible control of temperature gradient in the tube working chamber; furnace tube can work with a controlled atmosphere working environment or a high vacuum working environment.

What Is A Vacuum Furnace Used For?

A vacuum furnace is used for high-temperature processing of materials in a controlled environment without any contamination. It operates by surrounding the product with a vacuum, which prevents oxidation and heat loss from the product through convection. This furnace is commonly used for heat treatment of steel alloys at temperatures below 1200 °C. High-temperature vacuum furnaces can reach temperatures up to 3000°C and are used for industrial processes such as sintering, brazing, annealing, and heat treatment with high consistency and low contamination. The ability to achieve uniform heating across the entire workpiece is a key benefit of using a high-temperature vacuum furnace.

How Does CVD Furnace Work?

CVD furnace system consists of high temperature tube furnace unit, reacting gas source precise control unit, vacuum pump station and corresponding assembling parts.

Vacuum pump is to remove the air from the reacting tube,and make sure there is no unwanted gases inside the reaction tube, after that the tube furnace will heat the reaction tube to a target temperature, then reacting gas source precise control unit can introduce different gases with a set ratio into the furnace tube for the chemical reaction, the chemical vapor deposition will be formed in the CVD furnace.

How Does A Tube Furnace Work?

Tube furnace heating elements are placed surrounding the cylindrical cavity, furnace can only heat the samples in the cylindrical cavity through indirect thermal radiation, since furnace tube can prevent sample material from contacting with furnace heating elements and insulation materials, so tube furnace creates a clean isolated heat chamber and reduce risks of the sample material contaminating by the furnace.

What Is Mpcvd?

MPCVD stands for Microwave Plasma Chemical Vapor Deposition and it is a process of depositing thin films onto a surface. It uses a vacuum chamber, microwave generator, and gas delivery system to create a plasma made up of reacting chemicals and necessary catalysts. MPCVD is heavily used in the ANFF network to deposit layers of diamond using methane and hydrogen to grow new diamond on a diamond-seeded substrate. It is a promising technology for producing low-cost, high-quality large diamonds and is extensively used in the semiconductor and diamond cutting industry.

What Is The Process Of A Vacuum Furnace?

The process of a vacuum furnace involves loading the parts into the chamber and creating a vacuum inside it by utilizing a vacuum pump. The next step is to heat the parts using temperature controls, which can reach between 1,500 and 5,400 degrees Fahrenheit. This process eliminates the possibility of oxidation and contamination, resulting in a higher purity end product. After heating, the parts are cooled and finished before being removed from the vacuum furnace. The furnace consists of various components, including the vacuum system, furnace shell, electric heating element, temperature controls, power supply system, and transport apparatus.

Which Gas Is Used In CVD Process?

There are tremendous gas sources can be used in the CVD process, the common chemical reactions of CVD includes Pyrolysis, photolysis, reduction, oxidation, redox,so the gases involved in these chemical reactions can be used in the CVD process.

We take CVD Graphene growth for an example, the gases used in the CVD process will be CH4,H2,O2 and N2.

What Is The Application For Tube Furnace?

Tubular furnace is mainly used in metallurgy, glass, heat treatment, lithium anode and cathode materials, new energy, abrasives and other industries, and is a professional equipment for measuring materials under certain temperature conditions.

Tube furnace features simple structure, easy operation, easy control and continuous production.

Tube furnace is also widely applied in the CVD (chemical vapor deposition) and plasma enhanced CVD systems.

What Is Mpcvd Machine?

The MPCVD (Microwave Plasma Chemical Vapor Deposition) machine is a laboratory equipment used to grow high-quality diamond films. It uses a carbon-containing gas and a microwave plasma to create a plasma ball above the diamond substrate, which heats it to a specific temperature. The plasma ball doesn't contact the cavity wall, making the diamond growth process free from impurities and enhancing the diamond's quality. The MPCVD system consists of a vacuum chamber, a microwave generator, and a gas delivery system that controls the flow of gas into the chamber.

What Gas Is Used In A Vacuum Furnace?

Different gases can be used in a vacuum furnace depending on the application. In general, vacuum furnaces can work with gases or mixtures such as Argon, Nitrogen, Hydrogen, Carbon Monoxide, Helium, among others. The use of these gases allows for heat treatment in a defined, mostly non-oxidizing atmosphere, which is required for various applications such as vacuum soldering and brazing, vacuum annealing, and sintering. Additionally, it is possible to work with a defined oxygen concentration that is different from the air composition.

What Is The Advantage Of CVD System?

  • Wide range of films can be produced, metal film, nonmetal film and multi-component alloy film as required. At the same time, it can prepare high-quality crystals that are difficult to obtain by other methods, such as GaN, BP, etc.
  • The film forming speed is fast, usually several microns per minute or even hundreds of microns per minute. It is possible to simultaneously deposit large quantities of coatings with uniform composition, which is incomparable to other film preparation methods, such as liquid phase epitaxy (LPE) and molecular beam epitaxy (MBE).
  • The working conditions are carried out under normal pressure or low vacuum conditions, so the coating has good diffraction, and the workpieces with complex shapes can be uniformly coated, which is much superior to PVD.
  • Due to the mutual diffusion of reaction gas, reaction product and substrate, a coating with good adhesion strength can be obtained, which is crucial for preparing surface strengthened films such as wear-resistant and anti-corrosion films.
  • Some films grow at a temperature far lower than the melting point of the film material. Under the condition of low temperature growth, the reaction gas and reactor wall and impurities contained in them almost do not react, so a film with high purity and good crystallinity can be obtained.
  • Chemical vapor deposition can obtain a smooth deposition surface. This is because compared with LPE, chemical vapor deposition (CVD) is carried out under high saturation, with high nucleation rate, high nucleation density, and uniform distribution on the whole plane, resulting in a macroscopic smooth surface. At the same time, in chemical vapor deposition, the average free path of molecules (atoms) is much larger than LPE, so the spatial distribution of molecules is more uniform, which is conducive to the formation of a smooth deposition surface.
  • Low radiation damage, which is a necessary condition for manufacturing metal oxide semiconductors (MOS) and other devices

How Many Different Types Tube Furnace?

Tube furnace can work with different mechanical functions smoothly, so there are many different types tube furnace variations for different experiment purposes, typical furnace furnaces are as below:

  • Horizontal tube furnace
  • Vertical tube furnace
  • Split tube furnace
  • Rotary tube furnace
  • Tilting tube furnace
  • Sliding tube furnace
  • Fast heating and cooling tube furnace
  • Continuous feeding and discharging tube furnace

What Are The Advantages Of Mpcvd?

MPCVD has several advantages over other methods of diamond production, such as higher purity, less energy consumption, and the ability to produce larger diamonds.

What Is The Heating Element Used In A Vacuum Furnace?

The heating element in a vacuum furnace is critical to its proper functioning, and is dependent on factors such as maximum operating temperature, power load, partial pressure and quench gases, and life expectancy. Vacuum furnaces are heated by electric resistance elements made from a variety of materials, including high-temperature metallic alloys such as stainless steel, nickel-chromium, molybdenum, tungsten, tantalum, or of non-metallic materials such as graphite and silicon carbide. The choice of material for the heating element is important in maximizing its longevity, reliability, efficiency, and ultimately the process results.

What Does PECVD Stand For?

PECVD is a technology that uses plasma to activate reaction gas, promote chemical reaction on the surface of substrate or near surface space, and generate solid film. The basic principle of plasma chemical vapor deposition technology is that under the action of RF or DC electric field, the source gas is ionized to form a plasma, the low-temperature plasma is used as the energy source, an appropriate amount of reaction gas is introduced, and the plasma discharge is used to activate the reaction gas and realize chemical vapor deposition.

According to the method of generating plasma, it can be divided into RF plasma, DC plasma and microwave plasma CVD, etc...

What Are The Advantages Of Using A Tube Furnace?

Tube furnaces offer several advantages for high-temperature applications. Firstly, they provide precise and uniform temperature control, allowing for accurate and repeatable heating processes. This is crucial for materials research and heat treatment applications where temperature consistency is essential. Secondly, tube furnaces have a compact design, making them suitable for use in limited laboratory or industrial spaces. They are also versatile and can accommodate a wide range of sample sizes and shapes. Additionally, tube furnaces are energy-efficient, as they typically have good insulation and can reach high temperatures quickly. Some models also offer programmable temperature profiles, allowing for automated heating and cooling cycles. Overall, tube furnaces enable efficient and controlled high-temperature processes in various scientific and industrial fields.

Are CVD Diamonds Real Or Fake?

CVD diamonds are real diamonds and not fake. They are grown in a laboratory through a process called Chemical Vapor Deposition (CVD). Unlike natural diamonds that are mined from under the earth's surface, CVD diamonds are created using advanced technology in labs. These diamonds are 100% carbon and are the purest form of diamonds known as Type IIa diamonds. They have the same optical, thermal, physical, and chemical properties as natural diamonds. The only difference is that CVD diamonds are created in a lab and not mined from the earth.

What Is The Difference Between CVD And PECVD?

The difference between PECVD and traditional CVD technology is that the plasma contains a large number of high-energy electrons, which can provide the activation energy required in the chemical vapor deposition process, thus changing the energy supply mode of the reaction system. Since the electron temperature in the plasma is as high as 10000K, the collision between electrons and gas molecules can promote the chemical bond breaking and recombination of the reaction gas molecules to generate more active chemical groups, while the whole reaction system maintains a lower temperature.

So compared to the CVD process, PECVD can carry out the same chemical vapor deposition process with a lower temperature.

What Safety Precautions Should Be Taken When Using A Tube Furnace?

When using a tube furnace, it is important to follow safety precautions to prevent accidents and ensure operator and sample safety. Firstly, proper training should be provided to personnel operating the furnace to ensure they understand its operation, safety features, and emergency procedures. Secondly, appropriate personal protective equipment (PPE), such as heat-resistant gloves, goggles, and lab coats, should be worn to protect against burns and potential hazards. Thirdly, it is crucial to properly load the sample or material inside the furnace, ensuring it is securely positioned and does not obstruct airflow. Adequate ventilation should be provided to remove any potential gases or fumes generated during heating. It is also important to regularly inspect and maintain the furnace, including checking the heating elements and electrical connections, to ensure safe and reliable operation.
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Product Datasheet

Split Chamber CVD Tube Furnace with Vacuum Station Chemical Vapor Deposition System Equipment Machine

Category Catalog

Cvd & Pecvd Furnace


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