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Laboratory High Pressure Vacuum Tube Furnace

Tube Furnace

Laboratory High Pressure Vacuum Tube Furnace

Item Number : KT-PTF

Price varies based on specs and customizations


Max. temperature
1100℃
Constant work temperature
1000℃
Furnace tube diameter
50 / 60 / 80 / 100 mm
Heating zone length
300 / 450 / 600 / 800 mm
Heating zone quantity
1-10 zones
Rated vacuum pressure
0.001 Pa/10E5 torr
Rated positive pressure
15 Mpa
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 Introduction

The High Pressure Tube Furnace is specialized equipment used in various industries including metallurgy, glass, and heat treatment, for processing materials under controlled atmospheres. It employs resistance heating elements to achieve high temperatures, crucial for processes like powder sintering and annealing. The furnace ensures sample integrity and prevents contamination, with features like optional vacuum or modified atmosphere setups and high-quality heating elements for precise temperature control.Applications

KT-PTF High pressure tube furnace is versatile laboratory equipment with a wide range of applications in various industries and research fields. Here are the main application areas of this product:

  • Annealing: Used to soften materials, improve machinability, and relieve internal stresses.
  • Brazing: Ideal for joining metals by melting a filler metal into the joint.
  • Calcining: Processes minerals and ores to remove volatile substances.
  • Ceramics: Essential for firing and sintering ceramic materials.
  • Crystal Growth: Facilitates the controlled growth of crystals in a specific atmosphere.
  • Firing: Critical for the ceramic and glass industries to harden materials.
  • Glass: Used for annealing, stress relieving, and research of glass materials.
  • Gradient Work: Allows for the creation of materials with varying compositions.
  • Heat Treating: Enhances the mechanical properties of metals and alloys.
  • Laboratory Research: Provides a controlled environment for various scientific experiments.
  • Materials Testing: Used to test the properties and behaviors of materials under high temperatures.
  • Melting: Ideal for melting metals and alloys for casting or further processing.
  • Powders: Used in the processing of metal and ceramic powders.

Principle

The High Pressure Tube Furnace operates under controlled atmospheres or high vacuum conditions using precise resistance heating. It utilizes a high-temperature nickel-based super alloy furnace tube that withstands both high temperatures and pressures. The furnace's working temperature reaches up to 1100°C, while its working pressure can reach 15 MPa at ambient temperature and 4 MPa at 800°C. The furnace tube flange seal employs a solid copper O-ring, adapting to both negative and positive pressures for an extended service life.

Detail & Parts

High pressure tube furnace front1.Electromagnetic valve 2.SS Flange 3.Furnace tube 4.Furnace 5.Fan 6.Pressure sensor 7.Valve 8.Vacuum port 9.Gas inlet port 10.Valve 11.Temperature controller 12.Pressure controller 13.Cooling ring 14.Mechanical pressure valve 15.Pressure release port
1.Electromagnetic valve 2.SS Flange 3.Furnace tube 4.Furnace 5.Fan 6.Pressure sensor 7.Valve 8.Vacuum port 9.Gas inlet port 10.Valve 11.Temperature controller 12.Pressure controller 13.Cooling ring 14.Mechanical pressure valve 15.Pressure release port

High pressure tube furnace front

Features

  • High Pressure Resistance: Withstands up to 15Mpa positive pressure at ambient temperature, allowing for high-pressure applications and enhanced safety.
  • Durable Furnace Tube Material: Constructed with high-temperature nickel-based super alloy, providing exceptional resistance to heat and chemical reactions, ensuring long-term reliability.
  • Versatile Atmosphere Control: Operates in both controlled atmosphere and high vacuum conditions, enabling a wide range of experimental possibilities.
  • Precise Pressure Regulation: Digital positive pressure meter with over-pressure alarming and emergency stop function ensures accurate pressure control and safety.
  • Automatic Pressure Release: Furnace tube automatically releases pressure when the set pressure value is reached, preventing over-pressurization and potential hazards.
  • Efficient Temperature Control: PID programmable temperature control provides excellent accuracy and stable heating performance, ensuring precise temperature regulation.
  • Remote Connectivity:Supports remote control and centralized control, allowing for convenient operation and monitoring from a distance.
  • Advanced Touch Screen Interface: PTF Pro model features a 7-inch TFT touch screen controller for user-friendly program setting and data analysis, simplifying operation and enhancing accessibility.
  • Wide Temperature Range: Kiln temperatures up to 1100°C, expanding the range of applications and enabling high-temperature processes.
  • Controlled Atmospheres:Capable of handling flammable gases and multiple atmospheres, providing flexibility for various experimental requirements.
  • Advanced Pusher Technology:Graphite pushers for high-temperature applications enhance temperature uniformity and reduce energy consumption.
  • Precise Atmosphere Control: Sophisticated gas distribution technology ensures accurate control of atmosphere dew point along the furnace length, optimizing process conditions.
  • Modular Design: Modular construction facilitates maintenance and replacement of parts, minimizing installation effort and downtime.
  • Independent Temperature Zones: Multiple independently controlled temperature zones allow for precise heating and cooling profiles, catering to complex process requirements.

Safety Advantage

  • PTF high pressure tube furnace will automatically release the positive pressure once tube inside pressure reached set pressure value
  • KINTEK tube furnace owns over current protection and over temperature alarming function, furnace will turn off the power automatically once over current detected
  • Furnace build in thermal couple detecting function, furnace will stop heating and alarm will be on once thermal couple broken or failure detected
  • PTF Pro support power failure restarting function,furnace will resume the furnace heating program when power is incoming after failure

Advantages

  • High-temperature resistance: The furnace tube is made of high-temperature nickel-based super alloy, which can withstand temperatures up to 1100°C.
  • High-pressure resistance: The furnace can operate under a positive pressure of up to 15Mpa at ambient temperature and 4Mpa at 800°C.
  • Versatile atmosphere control: The furnace can operate under a controlled atmosphere or high vacuum conditions, with a maximum vacuum pressure of 10E-5 torr.
  • Automatic pressure release: The furnace tube will automatically release pressure once the positive pressure reaches the set value, ensuring safety.
  • Double furnace shell design: The double furnace shell design with forced air flow keeps the furnace surface temperature low, improving safety and comfort.
  • Precise temperature control: PID programmable temperature controlprovides excellent control accuracy and stable heating performance, allowing for precise temperature adjustment.
  • Remote control and centralized control: The furnace supports remote control and centralized control, enabling convenient operation and monitoring.
  • User-friendly interface: The PTF Pro model features a 7-inch TFT touch screen controller for easy program setting and history data analysis, allowing for efficient operation and data management.

Technical specifications

Furnace model KT-PTF KT-PTF Pro
Temperature controller Digital PID controller Touch screen PID controller
Multi program preset no yes
Power failure restarting no yes
Max. temperature 1100℃
Constant work temperature 1000℃
Furnace tube material Super nickel based alloy
Furnace tube diameter 50 / 60 / 80 / 100 mm
Heating zone length 300 / 450 / 600 / 800 mm
Heating zone quantity 1-10 zones
Vacuum sealing solution SS 304 flange with solid copper seal ring
Rated vacuum pressure 0.001Pa/10E5 torr
Rated positive pressure 15 Mpa
Chamber material Japan Al2O3 alumina fiber
Heating element Cr2Al2Mo2 wire coil
Temperature sensor Build in K type Thermal couple
Temperature control accuracy ±1℃
Temperature uniformity ±5℃
Electric power supply AC110-220V,50/60HZ
Other super nickel based alloy tube size and heating zone length can be customized

Standard Package

No. Description Quantity
1 Furnace 1
2 Nickel-based Superalloy tube 1
3 Vacuum flange 2
4 Tube thermal block 2
5 Tube thermal block hook 1
6 Heat resistant glove 1
7 Operation manual 1

Optional Setup

  • In tube gases detecting and monitoring,like H2, O2 and so on
  • Independent furnace temperature monitoring and recording
  • RS 485 communication port for PC remote control and data exporting
  • Insert gases feeding flow rate control,like mass flowmeter and float flowmeter
  • Touch screen temperature controller with versatile operator friendly functions
  • High vacuum pump station setups, like vane vacuum pump,molecular pump,diffusion pump

Warnings

Operator safety is the top important issue! Please operate the equipment with cautions. Working with inflammable& explosive or toxic gases is very dangerous, operators must take all necessary precautions before starting the equipment. Working with positive pressure inside the reactors or chambers is dangerous, operator must fellow the safety procedures strictly. Extra caution must also be taken when operating with air-reactive materials, especially under vacuum. A leak can draw air into the apparatus and cause a violent reaction to occur.

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FAQ

What Is A Vacuum Furnace Used For?

A vacuum furnace is used for high-temperature processing of materials in a controlled environment without any contamination. It operates by surrounding the product with a vacuum, which prevents oxidation and heat loss from the product through convection. This furnace is commonly used for heat treatment of steel alloys at temperatures below 1200 °C. High-temperature vacuum furnaces can reach temperatures up to 3000°C and are used for industrial processes such as sintering, brazing, annealing, and heat treatment with high consistency and low contamination. The ability to achieve uniform heating across the entire workpiece is a key benefit of using a high-temperature vacuum furnace.

What Is The Process Of A Vacuum Furnace?

The process of a vacuum furnace involves loading the parts into the chamber and creating a vacuum inside it by utilizing a vacuum pump. The next step is to heat the parts using temperature controls, which can reach between 1,500 and 5,400 degrees Fahrenheit. This process eliminates the possibility of oxidation and contamination, resulting in a higher purity end product. After heating, the parts are cooled and finished before being removed from the vacuum furnace. The furnace consists of various components, including the vacuum system, furnace shell, electric heating element, temperature controls, power supply system, and transport apparatus.

What Gas Is Used In A Vacuum Furnace?

Different gases can be used in a vacuum furnace depending on the application. In general, vacuum furnaces can work with gases or mixtures such as Argon, Nitrogen, Hydrogen, Carbon Monoxide, Helium, among others. The use of these gases allows for heat treatment in a defined, mostly non-oxidizing atmosphere, which is required for various applications such as vacuum soldering and brazing, vacuum annealing, and sintering. Additionally, it is possible to work with a defined oxygen concentration that is different from the air composition.

What Is The Heating Element Used In A Vacuum Furnace?

The heating element in a vacuum furnace is critical to its proper functioning, and is dependent on factors such as maximum operating temperature, power load, partial pressure and quench gases, and life expectancy. Vacuum furnaces are heated by electric resistance elements made from a variety of materials, including high-temperature metallic alloys such as stainless steel, nickel-chromium, molybdenum, tungsten, tantalum, or of non-metallic materials such as graphite and silicon carbide. The choice of material for the heating element is important in maximizing its longevity, reliability, efficiency, and ultimately the process results.
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4.9 / 5

The automated pressure release is a game-changer for lab safety. It arrived faster than expected, and the build quality is exceptional. A brilliant investment!

Elara Vance

4.8 / 5

Incredible value. The 15MPa pressure handling and precise PID control have revolutionized our materials testing. Durability is top-notch. Highly recommended.

Soren Petrov

4.7 / 5

The 7-inch touchscreen makes complex programming a breeze. Such advanced tech in a robust package. It's the heart of our research now.

Anya Sharma

4.9 / 5

Speed of delivery was impressive. The furnace's versatility for sintering and annealing under vacuum is unmatched. Quality shines in every detail.

Caius Novak

4.8 / 5

A workhorse! The nickel-alloy tube withstands extreme conditions daily. This is what cutting-edge, durable lab equipment looks like. Love it.

Zara Al-Jamil

4.7 / 5

Perfect for crystal growth. The atmosphere control is incredibly precise. Set up was straightforward. Worth every penny for the results we get.

Leif Thorsen

4.9 / 5

The remote control feature is fantastic. The furnace handles high-pressure experiments with such reliability. A true technological marvel.

Mei Lin

4.8 / 5

Outstanding performance. The modular design simplifies maintenance. It's built to last and has significantly accelerated our R&D timeline.

Javier Costa

4.7 / 5

The temperature uniformity is exceptional. This furnace has paid for itself in improved experimental consistency and efficiency. Superb quality.

Ingrid Weiss

4.9 / 5

Flawless operation from day one. The safety features provide immense peace of mind. An incredibly smart and well-engineered piece of equipment.

Kenji Tanaka

Product Datasheet

Laboratory High Pressure Vacuum Tube Furnace

Category Catalog

Tube Furnace


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