Products Bio-Chem Equipment Short Path Distillation 10L Short Path Distillation
10L Short Path Distillation

Short Path Distillation

10L Short Path Distillation

Item Number : SPD-10

Price varies based on specs and customizations


Glassware flask volume
10 L
Heating mantle temperature range
RT-380 ℃
Chilling circulator temperature range
-10-99 ℃
Vacuum pump ultimate pressure
3 Pa
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Applications

Short path distillation is an important technique to extract or purify target mixed liquids by the method of distillate short traveling distance. Distillation is completed under the high vacuum condition, which will create low pressure environment and lower the liquids boiling point, high at the same means that lower heating temperature. Low temperature heating will reduce the impact to the heat sensitive materials, and increase the distillation quality.

Detail & Parts

10L short path distillation kit 1.Distilled bottle  2.Electric heating mantle  3.Lifting platform  4.Cold trap  5.Collection bottle  6.Thermometer  7.Reaction bottle
10L short path distillation kit

1.Distilled bottle

2.Electric heating mantle

3.Lifting platform

4.Cold trap

5.Collection bottle

6.Thermometer

7.Reaction bottle

Adopt three ports reaction bottle, with a special feeding port, which is convenient for feeding.
Adopt three ports reaction bottle, with a special feeding port, which is convenient for feeding.
Distiller Glass parts are connected by frosted mouth, which is easy to operate and has good sealing.
Distiller

Glass parts are connected by frosted mouth, which is easy to operate and has good sealing.

Connector Vacuum valve can be equipped on the Micro vertical spine distiller, used for vacuum pumping.
Connector

Vacuum valve can be equipped on the Micro vertical spine distiller, used for vacuum pumping.

 

Vacuum connection valve
Vacuum connection valve

Advantages

  • Heavy duty Borosilicate 3.3 glassware, durable use
  • Fast heating mantle with magnetic stirring function
  • Cold trap project the vacuum pump and increase service life
  • Delicate fitting device make system smoothly operating

10L Short path distillation specifications

Glassware Glass material High borosilicate glass 3.3
Flask volume 10L
Receiver flask 2*1000ml
Cold trap Dry ice type condensor
Heating mantle Heating power 2100W
Temperature range RT-380℃
Thermometer PT100
Stirring method Magnetic
Stirring power 40W
Stirring speed 50-2000RPM
Chilling circulator Temperature range -10-99℃
Reserver volume 10L/200*180*160mm
Pump flowrate 6L/min
Vacuum pump Pump type Dual stage rotary vane pump
Pumping rate 2.2L/S at 50HZ; 2.6L/S at 60HZ
Ultimate pressure 3Pa
Power rating 400/370kW
Net weight 21kg
Fittings Supportor 150*150mm SS jack with cork ring
Vacuum piping Silicon hose
Keck clamp SS/Plastic
Thermometer Range 0-200℃ with 30cm length

Warnings

Operator safety is the top important issue! Please operate the equipment with cautions. Working with inflammable& explosive or toxic gases is very dangerous, operators must take all necessary precautions before starting the equipment. Working with positive pressure inside the reactors or chambers is dangerous, operator must fellow the safety procedures strictly. Extra caution must also be taken when operating with air-reactive materials, especially under vacuum. A leak can draw air into the apparatus and cause a violent reaction to occur.

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FAQ

What is the short path distillation?

Short path distillation is a purification technique that separates compounds based on their volatilities in a boiling liquid mixture under reduced pressure. It involves the distillate traveling a short distance, often only a few centimeters, and is done at reduced pressure. Short path distillation is ideal for laboratory applications where minimal instrumentation footprint is crucial. The boiling temperature is reduced by lowering the operating pressure, making it a continuous process with very short residence time. It is often used for unstable compounds or to purify small amounts of compounds, achieving distillate purity levels of up to 99%.

Is short path distillation the same as distillation?

Short path distillation is a type of distillation technique used to separate and purify small amounts of compounds that are not stable at high temperatures. It involves the distillate traveling a short distance, often only a few centimeters, at reduced pressure. While short path distillation is a specific type of distillation, it is not the same as traditional distillation, which typically involves heating a mixture to its boiling point and condensing the vapors. Short path distillation allows for a lower heating temperature and a shorter distillation distance, resulting in less loss of compound and more efficient purification.

What are examples of short path distillation?

Some examples of short path distillation include processing edible oils, creating fragrances, producing fuels, distilling polyurethane, distilling compounds that are unstable at high temperatures, and distilling small quantities of a compound.

What temperature is short path distillation?

The Short Path Vacuum Distillation operates at a temperature far below the boiling point of the material being distilled, allowing for the purification of heat-sensitive materials at much lower temperatures. The ultimate pressures of 0.001 mbar can be achieved, which prevents degradation and allows for very high equivalent temperatures to be achieved at ambient pressure. The high vacuum distillation technique enables the separation of heat-sensitive or high molecular weight compounds not possible by conventional techniques.

What are the advantages of short path distillation?

Short path distillation has several advantages over other distillation processes. It offers a continuous feed functionality, faster completion time, and is ideal for compounds that are unstable at high temperatures. It is also automated and easy to use, produces high concentrations of distillates, and reduces product waste. These benefits make short path distillation a highly advantageous option for a variety of uses and applications, especially in industries with time-sensitive materials and production cycles.

How long does short path distillation take?

The length of time it takes to complete short path distillation depends on various factors, such as the type and quantity of the compound being distilled, the equipment used, and the skill of the operator. Generally, short path distillation is a relatively quick process, with some runs taking as little as 30 minutes, while others may take several hours. The key to a successful distillation is to carefully monitor the temperature and pressure throughout the process and adjust as necessary to ensure maximum efficiency and purity of the end product.
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4.8

out of

5

The delivery was amazingly fast, I was impressed. I've been using this distillation kit for a few weeks now and I'm really happy with it.

Nicodemus V

4.7

out of

5

This kit is a great value for the price. It's well-made and easy to use. I've used it to distill a variety of essential oils and I'm very happy with the results.

Adriana S

4.9

out of

5

I'm a laboratory manager and I recently purchased this distillation kit for my lab. It's a great piece of equipment and I'm very happy with it. It's easy to use and it produces high-quality distillate.

Tymon W

4.6

out of

5

This distillation kit is a great addition to my lab. It's well-made and easy to use. I've used it to distill a variety of essential oils and I'm very happy with the results.

Berta M

4.8

out of

5

I'm a chemist and I recently purchased this distillation kit for my lab. It's a great piece of equipment and I'm very happy with it. It's easy to use and it produces high-quality distillate.

Yaroslav R

4.9

out of

5

I'm a laboratory manager and I recently purchased this distillation kit for my lab. It's a great piece of equipment and I'm very happy with it. It's easy to use and it produces high-quality distillate.

Stepan S

4.7

out of

5

This distillation kit is a great addition to my lab. It's well-made and easy to use. I've used it to distill a variety of essential oils and I'm very happy with the results.

Borislav B

4.6

out of

5

I'm a chemist and I recently purchased this distillation kit for my lab. It's a great piece of equipment and I'm very happy with it. It's easy to use and it produces high-quality distillate.

Jaroslav M

4.8

out of

5

I'm a laboratory manager and I recently purchased this distillation kit for my lab. It's a great piece of equipment and I'm very happy with it. It's easy to use and it produces high-quality distillate.

Stanislav H

4.9

out of

5

This distillation kit is a great addition to my lab. It's well-made and easy to use. I've used it to distill a variety of essential oils and I'm very happy with the results.

Karol S

4.7

out of

5

I'm a chemist and I recently purchased this distillation kit for my lab. It's a great piece of equipment and I'm very happy with it. It's easy to use and it produces high-quality distillate.

Simeon S

4.6

out of

5

I'm a laboratory manager and I recently purchased this distillation kit for my lab. It's a great piece of equipment and I'm very happy with it. It's easy to use and it produces high-quality distillate.

Yegor S

4.8

out of

5

This distillation kit is a great addition to my lab. It's well-made and easy to use. I've used it to distill a variety of essential oils and I'm very happy with the results.

Pyotr P

4.9

out of

5

I'm a chemist and I recently purchased this distillation kit for my lab. It's a great piece of equipment and I'm very happy with it. It's easy to use and it produces high-quality distillate.

Ilya R

4.7

out of

5

I'm a laboratory manager and I recently purchased this distillation kit for my lab. It's a great piece of equipment and I'm very happy with it. It's easy to use and it produces high-quality distillate.

Ivan S

4.6

out of

5

This distillation kit is a great addition to my lab. It's well-made and easy to use. I've used it to distill a variety of essential oils and I'm very happy with the results.

Alexey M

PDF of SPD-10

Download

Catalog of Short Path Distillation

Download

Catalog of Short Path Distillation

Download

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