Short Path Distillation

10L Short Path Distillation

Name: 10L Short Path Distillation
Brand: Kintek Solution
SKU: SPD-10
Rating: 4.75 (16 reviews)

Item Number : SPD-10

Price varies based on specs and customizations

Glassware flask volume: 10 L
Heating mantle temperature range: RT-380 ℃
Chilling circulator temperature range: -10-99 ℃
Vacuum pump ultimate pressure: 3 Pa

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Applications

Short path distillation is an important technique to extract or purify target mixed liquids by the method of distillate short traveling distance. Distillation is completed under the high vacuum condition, which will create low pressure environment and lower the liquids boiling point, high at the same means that lower heating temperature. Low temperature heating will reduce the impact to the heat sensitive materials, and increase the distillation quality.

Detail & Parts

10L short path distillation kit 1.Distilled bottle 2.Electric heating mantle 3.Lifting platform 4.Cold trap 5.Collection bottle 6.Thermometer 7.Reaction bottle — 10L short path distillation kit

1.Distilled bottle

2.Electric heating mantle

3.Lifting platform

4.Cold trap

5.Collection bottle

6.Thermometer

7.Reaction bottle

Adopt three ports reaction bottle, with a special feeding port, which is convenient for feeding.

Distiller Glass parts are connected by frosted mouth, which is easy to operate and has good sealing. — Distiller

Glass parts are connected by frosted mouth, which is easy to operate and has good sealing.

Connector Vacuum valve can be equipped on the Micro vertical spine distiller, used for vacuum pumping. — Connector

Vacuum valve can be equipped on the Micro vertical spine distiller, used for vacuum pumping.

Advantages

Heavy duty Borosilicate 3.3 glassware, durable use
Fast heating mantle with magnetic stirring function
Cold trap project the vacuum pump and increase service life
Delicate fitting device make system smoothly operating

10L Short path distillation specifications

Glassware	Glass material	High borosilicate glass 3.3
	Flask volume	10L
	Receiver flask	2*1000ml
	Cold trap	Dry ice type condensor
Heating mantle	Heating power	2100W
	Temperature range	RT-380℃
	Thermometer	PT100
	Stirring method	Magnetic
	Stirring power	40W
	Stirring speed	50-2000RPM
Chilling circulator	Temperature range	-10-99℃
	Reserver volume	10L/200180160mm
	Pump flowrate	6L/min
Vacuum pump	Pump type	Dual stage rotary vane pump
	Pumping rate	2.2L/S at 50HZ; 2.6L/S at 60HZ
	Ultimate pressure	3Pa
	Power rating	400/370kW
	Net weight	21kg
Fittings	Supportor	150*150mm SS jack with cork ring
	Vacuum piping	Silicon hose
	Keck clamp	SS/Plastic
	Thermometer	Range 0-200℃ with 30cm length

Warnings

Operator safety is the top important issue! Please operate the equipment with cautions. Working with inflammable& explosive or toxic gases is very dangerous, operators must take all necessary precautions before starting the equipment. Working with positive pressure inside the reactors or chambers is dangerous, operator must fellow the safety procedures strictly. Extra caution must also be taken when operating with air-reactive materials, especially under vacuum. A leak can draw air into the apparatus and cause a violent reaction to occur.

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FAQ

What is the short path distillation?

Short path distillation is a purification technique that separates compounds based on their volatilities in a boiling liquid mixture under reduced pressure. It involves the distillate traveling a short distance, often only a few centimeters, and is done at reduced pressure. Short path distillation is ideal for laboratory applications where minimal instrumentation footprint is crucial. The boiling temperature is reduced by lowering the operating pressure, making it a continuous process with very short residence time. It is often used for unstable compounds or to purify small amounts of compounds, achieving distillate purity levels of up to 99%.

What is the purpose of a rotary evaporator?

The purpose of a rotary evaporator, or rotovap, is to distill a solvent to separate a given mixture into its components based on their respective volatilities, through the process of evaporation and condensation. The rotovap is used to concentrate non-volatile components in a mixture and to extract volatile aroma and flavor molecules from mixtures gently and at low temperatures. The two key components of the rotovap allow for a gentle, precise, and efficient distillation not found in conventional distilling apparatuses: vacuum removal of solvent to lower boiling point and rotary flask rotation to increase surface area and speed up distillation.

What are high purity materials?

High purity materials refer to substances that are free from impurities and possess a high level of chemical homogeneity. These materials are essential in various industries, particularly in the field of advanced electronics, where impurities can significantly affect the performance of devices. High purity materials are obtained through various methods, including chemical purification, vapor-phase deposition, and zone refining. In the preparation of electronic grade single crystal diamond, for example, a high-purity raw material gas and an efficient vacuum system are necessary to achieve the desired level of purity and homogeneity.

Is short path distillation the same as distillation?

Short path distillation is a type of distillation technique used to separate and purify small amounts of compounds that are not stable at high temperatures. It involves the distillate traveling a short distance, often only a few centimeters, at reduced pressure. While short path distillation is a specific type of distillation, it is not the same as traditional distillation, which typically involves heating a mixture to its boiling point and condensing the vapors. Short path distillation allows for a lower heating temperature and a shorter distillation distance, resulting in less loss of compound and more efficient purification.

Why rotary evaporator is used in solvent extraction?

Rotary evaporators are used in solvent extraction because they allow for the efficient and gentle removal of solvents from samples by evaporation. This is achieved by reducing the pressure to lower the solvent boiling point, rotating the sample to increase the effective surface area, heating the solution, and then condensing the evaporated solvent in a cooled glass condenser. This process leaves the concentrated compound in the flask and is often used in medicinal chemistry, pharmaceutical, chromatography, and petrochemical fields.

What are examples of short path distillation?

Some examples of short path distillation include processing edible oils, creating fragrances, producing fuels, distilling polyurethane, distilling compounds that are unstable at high temperatures, and distilling small quantities of a compound.

Can rotary evaporator remove water?

Yes, a rotary evaporator can remove water. By changing the temperature to speed up the evaporation rate or by vacuuming with a vacuum pump to further reduce the pressure and lower the boiling point, a rotary evaporator can evaporate solutions that contain water and other substances. The electronic control of the rotary evaporator keeps the rotation of the flask at a constant speed, creating a larger surface area for heating and faster evaporation speeds. The traditional distillation method is less efficient and accurate than a rotary evaporator, which is widely used in chemical laboratories, industrial, bio-pharmaceutical, and food-making fields.

What temperature is short path distillation?

The Short Path Vacuum Distillation operates at a temperature far below the boiling point of the material being distilled, allowing for the purification of heat-sensitive materials at much lower temperatures. The ultimate pressures of 0.001 mbar can be achieved, which prevents degradation and allows for very high equivalent temperatures to be achieved at ambient pressure. The high vacuum distillation technique enables the separation of heat-sensitive or high molecular weight compounds not possible by conventional techniques.

What are the advantages of short path distillation?

Short path distillation has several advantages over other distillation processes. It offers a continuous feed functionality, faster completion time, and is ideal for compounds that are unstable at high temperatures. It is also automated and easy to use, produces high concentrations of distillates, and reduces product waste. These benefits make short path distillation a highly advantageous option for a variety of uses and applications, especially in industries with time-sensitive materials and production cycles.

How long does short path distillation take?

The length of time it takes to complete short path distillation depends on various factors, such as the type and quantity of the compound being distilled, the equipment used, and the skill of the operator. Generally, short path distillation is a relatively quick process, with some runs taking as little as 30 minutes, while others may take several hours. The key to a successful distillation is to carefully monitor the temperature and pressure throughout the process and adjust as necessary to ensure maximum efficiency and purity of the end product.

Is rotary evaporator used for distillation?

Yes, rotary evaporator is used for distillation. It is a device used in chemical laboratories to efficiently and gently remove solvents from samples by evaporation. The system works by reducing the pressure to lower the solvent boiling point, rotating the sample to increase the effective surface area, heating the solution, and then the evaporated solvent condenses in a cooled glass condenser. Rotary evaporation is most often and conveniently applied to separate "low boiling" solvents such as n-hexane or ethyl acetate from compounds which are solid at room temperature and pressure.

What are the principles of rotary evaporation?

The basic principle of rotary evaporation is to increase a sample's surface area and optimize its temperature and vacuum level, enabling effective separation of solvents in a short time. A cooling condenser helps to recover the separated solvent. It is a gentle and efficient method for liquid separation and purification, with specific applications including concentration, crystallization, solvent distillation, and chemical synthesis. A rotary evaporator and a vacuum pump are the two equipment required for a rotary evaporation system. Selection of the optimal vacuum pump is based on considerations such as chemical compatibility, ability to process wet vapors, ultimate depth of vacuum, flow rate, and adjustable control of vacuum levels.

What are the advantages of a rotary evaporator?

The advantages of using a rotary evaporator include lower boiling temperatures, faster evaporation of solvents, fewer operations, and the ability to suppress bumping during the process. The lower boiling temperatures allow for the separation of solvents and compounds at lower temperatures, while faster evaporation speeds up the process. Fewer operations are needed thanks to the built-in lifting and falling motor, and bumping is suppressed, allowing for quick and gentle evaporation. Rotary evaporators are particularly useful for heat-sensitive compounds and distillation of complex mixtures.

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4.8

out of

5

The delivery was amazingly fast, I was impressed. I've been using this distillation kit for a few weeks now and I'm really happy with it.

Nicodemus V

4.7

out of

5

This kit is a great value for the price. It's well-made and easy to use. I've used it to distill a variety of essential oils and I'm very happy with the results.

Adriana S

4.9

out of

5

I'm a laboratory manager and I recently purchased this distillation kit for my lab. It's a great piece of equipment and I'm very happy with it. It's easy to use and it produces high-quality distillate.

Tymon W

4.6

out of

5

This distillation kit is a great addition to my lab. It's well-made and easy to use. I've used it to distill a variety of essential oils and I'm very happy with the results.

Berta M

4.8

out of

5

I'm a chemist and I recently purchased this distillation kit for my lab. It's a great piece of equipment and I'm very happy with it. It's easy to use and it produces high-quality distillate.

Yaroslav R

4.9

out of

5

I'm a laboratory manager and I recently purchased this distillation kit for my lab. It's a great piece of equipment and I'm very happy with it. It's easy to use and it produces high-quality distillate.

Stepan S

4.7

out of

5

This distillation kit is a great addition to my lab. It's well-made and easy to use. I've used it to distill a variety of essential oils and I'm very happy with the results.

Borislav B

4.6

out of

5

I'm a chemist and I recently purchased this distillation kit for my lab. It's a great piece of equipment and I'm very happy with it. It's easy to use and it produces high-quality distillate.

Jaroslav M

4.8

out of

5

I'm a laboratory manager and I recently purchased this distillation kit for my lab. It's a great piece of equipment and I'm very happy with it. It's easy to use and it produces high-quality distillate.

Stanislav H

4.9

out of

5

This distillation kit is a great addition to my lab. It's well-made and easy to use. I've used it to distill a variety of essential oils and I'm very happy with the results.

Karol S

4.7

out of

5

I'm a chemist and I recently purchased this distillation kit for my lab. It's a great piece of equipment and I'm very happy with it. It's easy to use and it produces high-quality distillate.

Simeon S

4.6

out of

5

I'm a laboratory manager and I recently purchased this distillation kit for my lab. It's a great piece of equipment and I'm very happy with it. It's easy to use and it produces high-quality distillate.

Yegor S

4.8

out of

5

This distillation kit is a great addition to my lab. It's well-made and easy to use. I've used it to distill a variety of essential oils and I'm very happy with the results.

Pyotr P

4.9

out of

5

I'm a chemist and I recently purchased this distillation kit for my lab. It's a great piece of equipment and I'm very happy with it. It's easy to use and it produces high-quality distillate.

Ilya R

4.7

out of

5

I'm a laboratory manager and I recently purchased this distillation kit for my lab. It's a great piece of equipment and I'm very happy with it. It's easy to use and it produces high-quality distillate.

Ivan S

4.6

out of

5

This distillation kit is a great addition to my lab. It's well-made and easy to use. I've used it to distill a variety of essential oils and I'm very happy with the results.

Alexey M

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Step-by-Step Guide to Operating a Short Path Distillation Apparatus

Operating of Short Path Distillation and Precautions

Find out more

Understanding the Science Behind Short Path Distillation

Short path distillation is a precise and efficient method of separating and purifying liquids through a process of distillation.

Find out more

How to Choose the Right Rotovap for Your Distillation Needs

Rotary evaporators are commonly used in laboratories to separate solvents from a mixture through the process of evaporation.

Find out more

A Comparison of Rotovap Distillation and Other Distillation Technologies

Distillation is a separation technique used to purify liquids through heat application and vaporization. It is a crucial process in various industries such as the chemical, pharmaceutical, and food industries. There are various distillation technologies available, each with its unique advantages and disadvantages.

Find out more

A Beginner's Guide to Rotovap Distillation

Rotovap distillation is a common technique used to separate solvents from reaction mixtures. It involves the use of a rotary evaporator, which is a piece of laboratory equipment that utilizes rotation and heat to remove solvents or other compounds from a sample.

Find out more

How to Use a Rotovap for Precise Distillation Results

Rotary evaporation is a common technique used in laboratories to purify and separate solvents from chemical compounds.

Find out more

How Rotary Evaporators are Revolutionizing Distillation

Rotary evaporators, also commonly referred to as rotovaps, are laboratory equipment used for the separation of solvents from a mixture through the process of distillation.

Find out more

Get More Flavor from Your Ingredients with Rotovap Distillation

Rotovap distillation is a unique and efficient method of extracting essential oils and flavors from various ingredients.

Find out more

How Rotovap Distillation Simplifies Solvent Recovery

Rotovap distillation is a method of solvent removal that uses a rotary evaporator to remove solvents from a solution. It is a popular method used in laboratory settings for its efficiency in removing solvents from a sample.

Find out more

How Rotavapor Can Improve Your Distillation Process and Save You Time

A Rotavapor, also known as a rotary evaporator, is a laboratory apparatus used for distillation, purification, and extraction of solvents. It consists of a heating bath, rotation flask, and a condenser, which work together to remove the solvent from a sample.

Find out more

How To Use A Rotary Evaporator

Rotary evaporators (also called "rotavaps") are used to remove solvents from reaction mixtures and can accommodate volumes as large as 3 liters.

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How to Create Delicious Infusions with a Rotary Evaporator

Rotary evaporator infusions are a popular way to create flavorful tinctures, extracts, and infusions. A rotary evaporator is a device that uses vacuum and heat to remove solvents from samples, leaving behind a concentrated extract. This process is ideal for creating infusions because it minimizes the risk of overheating and damaging the ingredients.

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Hot Tags

short path distillation rotary evaporator high purity materials

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10L Short Path Distillation

Shipping:

Applications

Detail & Parts

Advantages

10L Short path distillation specifications

Warnings

Designed for You

FAQ

What is the short path distillation?

What is the purpose of a rotary evaporator?

What are high purity materials?

Is short path distillation the same as distillation?

Why rotary evaporator is used in solvent extraction?

What are examples of short path distillation?

Can rotary evaporator remove water?

What temperature is short path distillation?

What are the advantages of short path distillation?

How long does short path distillation take?

Is rotary evaporator used for distillation?

What are the principles of rotary evaporation?

What are the advantages of a rotary evaporator?

PDF - 10L Short Path Distillation

Catalog of Short Path Distillation

Catalog of Short Path Distillation

Catalog of Rotary Evaporator

Catalog of High Purity Materials

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Related Products

Related Articles

Step-by-Step Guide to Operating a Short Path Distillation Apparatus

Understanding the Science Behind Short Path Distillation

How to Choose the Right Rotovap for Your Distillation Needs

A Comparison of Rotovap Distillation and Other Distillation Technologies

A Beginner's Guide to Rotovap Distillation

How to Use a Rotovap for Precise Distillation Results

How Rotary Evaporators are Revolutionizing Distillation

Get More Flavor from Your Ingredients with Rotovap Distillation

How Rotovap Distillation Simplifies Solvent Recovery

How Rotavapor Can Improve Your Distillation Process and Save You Time

How To Use A Rotary Evaporator

How to Create Delicious Infusions with a Rotary Evaporator

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