Products Thermal Equipment MPCVD Drawing die nano-diamond coating HFCVD Equipment
Drawing die nano-diamond coating HFCVD Equipment

MPCVD

Drawing die nano-diamond coating HFCVD Equipment

Item Number : MP-CVD-100

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Application   

HFCVD chemical vapor deposition of diamond working principle is: mix a carbon-containing atmosphere with supersaturated hydrogen, activate it in a certain way, and then pass it through a certain atmosphere composition, activation energy, substrate temperature, and the distance between the substrate and the activation source, etc. Under these conditions, a diamond film is deposited on the bottom surface. It is generally believed that the nucleation and growth of diamond films can be divided into three stages:

  1. Carbon-containing gas and radon gas decompose into carbon, hydrogen atoms and other active free groups at a certain temperature. They combine with the matrix to first form a very thin carbide transition layer.
  2. Carbon atoms deposit diamond nuclei on the transition layer formed on the substrate.
  3. The formed diamond crystal nucleus grows into a diamond micro-item under a suitable environment, and then grows into a diamond film.

Detail & Parts

Working scene of wire drawing die nano diamond coating HFCVD equipment detial coating platform detail 01 coating platform detail 02 nano diamond coated drawing die detial 01 nano diamond coated drawing die detial 02

Technical specifications

 HFCVD technical composition
Technical Parameters  Equipment composition System Configuration
 Bell Jar: Dia. 500mm, Height 550mm, SUS304 stainless steel chamber; inner stainless steel skin insulation, lifting height is 350mm; A set of vacuum chamber (bell jar) main body (jacketed water-cooling structure)  Vacuum chamber (bell jar) main body;The cavity is made of high-quality 304 stainless steel; Vertical bell jar: the jacketed water-cooling jacket is installed on the overall periphery of the bell jar. The inner wall of the bell jar is insulated with stainless steel skin, and the bell jar is fixed on the side . Accurate and stable positioning ; Observation window: horizontally arranged in the middle of the vacuum chamber 200mm Observation window, water cooling, baffle, side and upper configuration 45 Degree bevel angle, 50° observation window (observe the same point as the horizontal observation window, and the sample supporting platform); the two observation windows maintain the existing position and size.Bell jar bottom is 20mm higher than the plane of the bench , set cooling; the holes reserved on the plane, such as large valves, air release valves, air pressure measurement, bypass valves, etc., are sealed with metal mesh and reserved for installing electrodes Interface; 
 Equipment table: L1550* W900*H1100mm  One set of drag sample table device (adopting double-axis drive )  Sample holder device: Stainless steel sample holder (welding water cooling ) 6- position device; it can be adjusted separately, only up and down adjustment, the up and down adjustment range is 25mm, and the left and right shaking is required to be less than 3% when going up and down ( that is, the left and right shaking of rising or falling by 1mm is less than 0.03mm ) , and the sample stage does not rotate when rising or falling.
Ultimate vacuum degree: 2.0×10-1Pa ; A set of vacuum system  Vacuum system: Vacuum system configuration: mechanical pump + vacuum valve + physical bleed valve + main exhaust pipe + bypass; (provided by the vacuum pump supplier), the vacuum valve uses a pneumatic valve; Vacuum system measurement: Membrane pressure. 
Pressure rise rate : ≤5Pa/h; Two channels mass flow meter gas supply system Gas supply system: The mass flow meter is configured by Party B, two-way air intake, the flow rate is controlled by the mass flow meter, after the two-way meeting, it enters the vacuum chamber from the top , and the inside of the air intake pipe is 50mm
 Sample table movement: up and down range is ± 25m; it is required to shake left and right ratio when up and down by ± 3%; One set of electrode device (2 channels) Electrode device: The length direction of the four electrode holes is parallel to the length direction of the support platform, and the length direction is facing the main observation window with a diameter of 200mm .
 Working pressure: use membrane gauge pressure gauge, measuring range: 0 ~ 10kPa; work constant at 1kPa ~5kPa,the constant pressure value changes plus or minus 0.1kPa; A set of cooling water system  Cooling water system: The bell jar, electrodes, and bottom plate are all equipped with circulating water cooling pipelines, and are equipped with insufficient water flow alarm device 3.7: control system. Switches, instruments, instruments and power supply for bell lifting, deflation, vacuum pump, main road, bypass, alarm, flow, air pressure, etc. are set on the side of the stand, and are controlled by a 14 -inch touch screen; the equipment has a fully automatic control program without manual intervention, and can store data and call data
Air intake position: air intake at the top of the bell jar, and the position of the exhaust port is located directly below the sample holder;   Control system
 Control System: PLC controller + 10-inch touch screen  A set of automatic pressure control system (original pressure control valve imported from Germany )
 Inflation system: 2 channels mass flow meter, flow range: 0-2000sccm and 0-200sccm; Pneumatic valve valve  Resistance Vacuum Gauge
3.1.10 Vacuum pump: D16C vacuum pump

Advantages

The nano-diamond composite coating drawing die uses cemented carbide (WC-Co) as the substrate, and uses the chemical vapor phase method ( CVD method for short ) to coat the conventional diamond and nano-diamond composite coating on the surface of the inner hole of the mold. And a brand new product obtained after grinding and polishing the coating . The nano-diamond composite coating coated on the surface of the inner hole not only has the characteristics of strong adhesion and wear resistance of the conventional diamond coating, but also has the advantages of flat and smooth surface of the nano-diamond coating, small friction coefficient and easy grinding and polishing. Coating technology not only solves the technical problem of coating adhesion, but also breaks through the bottleneck that the surface of diamond coating is not easy to polish, and removes the obstacles to the industrialization of CVD diamond film. 

Comparation table between traditional and nano diamond coated drawing die

Technical indicators

Traditional drawing die

Nano-diamond coated drawing die

Coating Surface Grain Size

none

20~80nm

Coating diamond content

none

≥99%

Diamond Coating Thickness

none

10 ~ 15mm

Surface roughness

Ra≤0.1mm

Class A: Ra≤0.1mm

Class B: Ra≤0.05mm

Coating drawing die inner hole diameter range

Ф3 ~ Ф70mm

Ф3 ~ Ф70mm

Service life span

Life span depends on working conditions

6-10 times longer

Surface friction coefficient

0.8

0.1

 

  • For the parallelism and straightness of the mold lifting platform of the equipment, our company has specially produced special tooling. The biaxial lifting method is enough to allow the two ends to be raised and lowered by about ±2 wires, so that smaller molds can be made.
  • For the tooling of the equipment, our company integrates the location of each company on the tooling, aiming at the tooling and process of the mold. Good tooling and clamping, stable and reliable, high precision, easy to operate.
  • For the shut-off valve of the equipment, other manufacturers use baffle valves, which cannot be adjusted linearly (that is, the gap increases quickly as soon as it is opened). Our company designs it according to the principle of the shut-off valve and stable pressure control, so that the shut-off gap can be linearly adjusted to achieve Stable pressure control;
  • The fully automatic control system automatically controls the pressure according to computer algorithms; it can reduce the operator's randomness and make the process more confidential. It saves labor, and the consistency of mold quality of the same specifications is more ideal;
  • For the stability of the lifting bell jar, our company uses self-lubricating bearings, which make the rotation more flexible and free of jamming. Basic process, diamond coating can be made according to each customer's diamond coating process.

 

Warnings

Operator safety is the top important issue! Please operate the equipment with cautions. Working with inflammable& explosive or toxic gases is very dangerous, operators must take all necessary precautions before starting the equipment. Working with positive pressure inside the reactors or chambers is dangerous, operator must fellow the safety procedures strictly. Extra caution must also be taken when operating with air-reactive materials, especially under vacuum. A leak can draw air into the apparatus and cause a violent reaction to occur.

Designed for You

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Would you please drop your ideas to us, our engineers are ready for you now!

FAQ

What is CVD diamond machine?

A CVD diamond machine is a device used to produce synthetic diamonds through a process called Chemical Vapor Deposition (CVD). This process involves the precipitation of chemical vapors to create a diamond, which has properties that are equivalent to natural diamonds. CVD diamond machines including filament-assisted thermal CVD, plasma-enhanced CVD, and combustion-flame assisted CVD etc. The resulting CVD diamonds are useful in the cutting tools industry due to their high hardness and long-lasting tool life, making them an important and cost-effective tool for cutting non-ferrous materials.

What is the basic principle of CVD?

The basic principle of Chemical Vapor Deposition (CVD) is to expose a substrate to one or more volatile precursors that react or decompose on its surface to produce a thin film deposit. This process can be used for various applications, such as patterning films, insulation materials, and conducting metal layers. CVD is a versatile process that can synthesize coatings, powders, fibers, nanotubes, and monolithic components. It is also capable of producing most of the metal and metal alloys and their compounds, semiconductors, and nonmetal systems. The deposition of a solid on a heated surface from a chemical reaction in the vapor phase characterizes the CVD process.

How does a CVD diamond machine work?

CVD diamond machines work by introducing a mixture of gases, typically methane and hydrogen, into a vacuum chamber. The gases are then activated using a variety of techniques such as microwave plasma or hot filament, which breaks down the molecules and releases carbon atoms. These carbon atoms then settle on the substrate, building up layer by layer to form a synthetic diamond.

What are the different types of CVD method?

The different types of CVD methods include atmospheric pressure CVD (APCVD), low-pressure CVD (LPCVD), ultrahigh vacuum CVD, CVD supported by aerosols, direct liquid injection CVD, hot wall CVD, cold wall CVD, microwave plasma CVD, plasma-enhanced CVD (PECVD), remote plasma-enhanced CVD, low-energy plasma-enhanced CVD, atomic layer CVD, combustion CVD, and hot filament CVD. These methods differ in the mechanism by which chemical reactions are triggered and the operating conditions.

What are the advantages of using CVD diamond machines?

CVD diamond machines offer several advantages over other methods of diamond production. Firstly, they allow for the creation of high-quality, near-flawless diamonds with precise control over their shape, size, and clarity. These machines also enable the production of diamonds with specific properties, such as color or electrical conductivity, by introducing appropriate dopant gases during the deposition process. Additionally, CVD diamond machines are more environmentally friendly compared to traditional diamond mining, as they minimize the social and environmental impacts associated with diamond extraction.

What are the advantages of using chemical vapor deposition machines?

Chemical vapor deposition machines offer several advantages in thin film deposition. They allow for precise control over the film's properties, such as thickness, composition, and uniformity. CVD can deposit films over large areas and complex shapes, making it suitable for a wide range of applications. The technique enables the deposition of a variety of materials, including metals, semiconductors, ceramics, and organic compounds. CVD films can exhibit excellent adhesion, purity, and conformality to the substrate surface. Additionally, CVD machines can operate at relatively low temperatures, reducing thermal stress on the substrate and enabling deposition on temperature-sensitive materials.

What considerations should be made when selecting a CVD diamond machine?

When selecting a CVD diamond machine, several factors should be considered. Firstly, the size and capacity of the machine should align with the intended production requirements. The deposition chamber size should accommodate the desired substrate dimensions and allow for scalability. The control and automation capabilities of the machine should also be assessed to ensure ease of operation and reproducibility. Additionally, the machine's heating and activation methods should be evaluated for efficiency and uniformity of diamond growth. It is also important to consider the availability of technical support, maintenance services, and the overall cost of ownership. Consulting with manufacturers and experts in the field can help in selecting the most suitable CVD diamond machine for specific production needs.

What are the applications of chemical vapor deposition machines?

Chemical vapor deposition machines find applications in various industries and research fields. In the semiconductor industry, CVD is used to deposit thin films for integrated circuits, such as silicon dioxide and silicon nitride. CVD is also employed in the production of thin film solar cells, where materials like cadmium telluride or copper indium gallium selenide are deposited. Other applications include the deposition of protective coatings, such as diamond-like carbon films, wear-resistant coatings, and anti-reflective coatings. CVD is also utilized in the production of optical coatings, such as thin films for mirrors, filters, and waveguides.

What are the common applications of diamonds produced by CVD diamond machines?

Diamonds produced by CVD diamond machines have a wide range of applications. They are commonly used in jewelry, as they offer the same beauty and durability as natural diamonds. CVD diamonds are also highly valued in industrial applications, such as cutting tools, abrasives, and heat sinks, due to their exceptional hardness and thermal conductivity. They are used in the electronics industry for high-performance electronic devices, such as high-power transistors and radiation detectors. CVD diamonds are also finding applications in the medical field, including surgical tools, optical components, and as coatings for implants due to their biocompatibility.

What factors should be considered when selecting a chemical vapor deposition machine?

Several factors should be considered when selecting a chemical vapor deposition machine. The required film properties, such as composition, thickness, and uniformity, should align with the capabilities of the machine. The size of the deposition chamber should accommodate the desired substrate size and shape. The machine's temperature and pressure range should match the specific deposition requirements. It is also important to consider the availability and compatibility of precursor gases for the desired material deposition. Other considerations include the ease of operation, maintenance requirements, and the level of automation or control capabilities. Additionally, consulting with experts or manufacturers can provide valuable guidance in selecting the most suitable CVD machine for a specific application.

Can chemical vapor deposition machines be used for multi-layered thin film deposition?

Yes, chemical vapor deposition machines can be used for multi-layered thin film deposition. By controlling the deposition parameters and sequentially introducing different precursor gases, it is possible to deposit multiple layers of different materials onto a substrate. This enables the creation of complex thin film structures with tailored properties and functionalities. The deposition sequence, temperature, pressure, and gas flow rates for each layer can be precisely controlled to achieve the desired film composition and thickness. Multi-layered thin films find applications in various fields, such as microelectronics, optoelectronics, and surface engineering, where different layers serve specific functions or enhance the overall performance of the material system.
View more faqs for this product

4.8

out of

5

The HFCVD Equipment is a game-changer in diamond coating technology. It's efficient, precise, and delivers superior results. Highly recommended!

Munetaka Takeda

4.9

out of

5

I'm thoroughly impressed with the quality and performance of the HFCVD Equipment. It has significantly improved our diamond coating process, resulting in exceptional results. A must-have for any lab!

Dr. Carla Rodriguez

4.7

out of

5

The HFCVD Equipment has exceeded my expectations. It's user-friendly, reliable, and produces high-quality diamond coatings consistently. A valuable addition to our laboratory.

Eng. Valentina Ivanova

4.9

out of

5

The HFCVD Equipment is a technological marvel. It has revolutionized our diamond coating research, enabling us to achieve remarkable results. Highly recommended for advanced materials research.

Prof. Olivier Dubois

4.8

out of

5

The HFCVD Equipment has transformed our laboratory's capabilities. It delivers exceptional diamond coatings with remarkable precision and efficiency. A valuable investment for any research institution.

Dr. Maria Fernandez

4.7

out of

5

I'm highly satisfied with the HFCVD Equipment. It has significantly improved our diamond coating process, resulting in enhanced product quality and reduced production time. Highly recommended!

Eng. Carlos Oliveira

4.9

out of

5

The HFCVD Equipment is a testament to cutting-edge technology. It has enabled us to achieve unprecedented results in diamond coating, opening up new possibilities for research and innovation.

Prof. Ahmed Hassan

4.8

out of

5

The HFCVD Equipment has proven to be an invaluable asset to our laboratory. It delivers consistent, high-quality diamond coatings, making it an essential tool for our research.

Dr. Svetlana Petrova

4.7

out of

5

I'm thoroughly impressed with the HFCVD Equipment. It's user-friendly, efficient, and produces exceptional diamond coatings. A must-have for any laboratory involved in materials research.

Eng. Juan Garcia

4.9

out of

5

The HFCVD Equipment is a remarkable piece of technology. It has enabled us to achieve breakthrough results in diamond coating, pushing the boundaries of materials science.

Prof. Li Wei

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