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XRD X-ray diffraction grinder

Milling Equipment

XRD X-ray diffraction grinder

Item Number : KT-XRD180

Price varies based on specs and customizations

Power
220V 50HZ
Disc(Wheel) Type
Grinding Disc
Sample size range
< 1 um
Grinding method
Dry grinding、Wet grinding
ISO & CE icon

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Introduction

KT-XRD180 is a miniature desktop multifunctional horizontal grinder specially developed for sample preparation of X-ray diffraction (XRD) analysis. The product can be used in applications such as geology, chemistry, mining, new materials, and education and scientific research. The product uses a 180ml volume zirconia (or tungsten carbide) ball mill tank with 42 zirconia (or tungsten carbide) grinding columns arranged in a regular manner, and gently rubs the sample between the cylinder and the tank during rolling rotation, so as not to damage the structure of the sample as much as possible. The particle distribution of the sample is narrowed, and the product can achieve good results in both dry and wet grinding or mixing applications.

Principle

The XRD X-Ray Diffraction Grinder operates on the principle of grinding samples to a fine particle size (<75 µm) to enhance the clarity of X-ray diffraction patterns, reducing background scattering and improving the detection of emissions, crucial for accurate material characterization.

Applications

The XRD X-Ray Diffraction Grinder is a versatile tool used in various scientific fields for the preparation of samples for X-ray diffraction analysis. This technique is crucial for achieving a homogeneous and finely ground sample, which is essential for accurate and precise X-ray diffraction measurements. The applications of this grinder span across materials science, geology, pharmaceuticals, and more, where the structural analysis of materials is paramount.

  • Materials Science: Used for the analysis of crystalline structures in metals, ceramics, and polymers, helping in the development of new materials with desired properties.
  • Geology: Essential for the analysis of minerals and rocks, aiding in the study of Earth's composition and history.
  • Pharmaceuticals: Critical in the analysis of drug compounds to ensure their crystalline structure is consistent for effective medication.
  • Environmental Science: Used to analyze soil and sediment samples to understand environmental impacts and pollution levels.
  • Chemical Industry: Helps in the quality control of chemical products by ensuring the purity and consistency of chemical compounds.
  • Research and Development: Widely used in academic and industrial research labs for the characterization of new compounds and materials.

Features of XRD X-Ray Diffraction Grinder

The XRD X-Ray Diffraction Grinder is a specialized tool designed to prepare samples for X-ray diffraction analysis, particularly in the context of materials science and quality control in industries such as cement, metal and mineral ores, and electronics. This grinder is engineered to finely pulverize samples to a size that is optimal for XRD analysis, ensuring accurate and reproducible results. Here are the key features that benefit the user:

  • Precision Grinding Mechanism: The grinder is equipped with a high-precision mechanism that ensures samples are ground to the optimal particle size for XRD analysis. This precision is crucial for obtaining clear and interpretable diffraction patterns.
  • Automated Control: With automated controls, the XRD grinder allows for consistent and repeatable sample preparation, reducing operator error and variability in results. This feature is particularly beneficial for high-throughput laboratories.
  • Versatile Sample Handling: The grinder can handle a variety of sample types, from hard minerals to softer organic materials, making it a versatile tool in diverse research and industrial settings.
  • Ease of Use: Designed with user convenience in mind, the XRD grinder features intuitive controls and easy maintenance, ensuring that even less experienced operators can prepare samples effectively.
  • Safety Features: Equipped with safety mechanisms to protect the operator and prevent contamination of samples, the grinder ensures a secure working environment.

These features collectively enhance the efficiency and accuracy of sample preparation for XRD analysis, making the XRD X-Ray Diffraction Grinder an indispensable tool for laboratories involved in material characterization and quality control.

Advantages

The XRD X-Ray Diffraction Grinder offers several key advantages that enhance the efficiency and effectiveness of sample preparation for X-ray diffraction analysis. Here are some of the most notable benefits:

  • Multiple Grinding Bowls for High Efficiency: The grinder features a design that allows for the simultaneous processing of up to four different materials. This capability significantly increases the throughput of sample preparation, making it ideal for laboratories dealing with a variety of samples or high-volume testing.
  • Versatile Sample Processing: This grinder is suitable for a wide range of materials including ores, minerals, ferroalloys, ceramics, soils, aggregates, and chemicals. It can effectively grind samples to a fine consistency, with typical results showing 95% of the material being reduced to 75-50 microns within just 3 minutes.
  • Low Maintenance and High Output: Designed for durability and minimal upkeep, the grinder is particularly well-suited for high-volume mineral laboratories and remote locations where regular maintenance may not be feasible. Its robust construction and integral vibratory motor-driven system ensure consistent performance with minimal downtime.
  • Enhanced Sample Homogeneity: By providing a consistent and uniform grind, the XRD grinder ensures that the subsequent X-ray diffraction analysis is more accurate and reliable. This is crucial for obtaining precise measurements of the crystallite and amorphous structures within the sample.
  • Support for Advanced Analysis Techniques: The grinder's ability to prepare samples to the required standard supports the use of advanced X-ray diffraction techniques such as grazing incidence X-ray diffraction (GIXRD). This technique is essential for the characterization of thin films and surface structures, where the quality of the sample preparation directly impacts the quality of the diffraction data.
  • Customizable Configuration: Users can choose the number of grinding bowls from one to four, depending on their specific needs. This flexibility allows laboratories to optimize their setup for different workloads and sample types, ensuring that resources are used efficiently.

These features collectively enhance the efficiency and accuracy of sample preparation for XRD analysis, making the XRD X-Ray Diffraction Grinder an indispensable tool for laboratories involved in material characterization and quality control.

Detail & Parts

Details of XRD X-ray diffraction grinder

Details of XRD X-ray diffraction grinder

Details of XRD X-ray diffraction grinder

Functions

  • continuous grinding
  • intermittent grinding
  • alternate grinding
  • timing
  • Speed regulation
  • Power off memory
  • LED lighting
  • PC Windows

Technical specifications

Application samples fine | low to medium hardness | brittle | dry or low viscosity
Processing Type Grinding | Blending
Maximum injection size < 0.5 mm
Sample particle size range < 1 um
Number of ball mill jars  1
Grinding jar volume 180ml | 100ml | 50ml
Number of grinding columns 42
Grinding Media Type Cylindrical | Spherical
Grinding jar material Zirconia | Tungsten carbide
Grinding method dry grinding | wet grinding
Number of rubber rollers 2 pieces
Maximum speed 1800 r/min
Net weight 28kg
Dimensions 260*250*140 mm
Protection class IP65
Standard CE

Warnings

Operator safety is the top important issue! Please operate the equipment with cautions. Working with inflammable& explosive or toxic gases is very dangerous, operators must take all necessary precautions before starting the equipment. Working with positive pressure inside the reactors or chambers is dangerous, operator must fellow the safety procedures strictly. Extra caution must also be taken when operating with air-reactive materials, especially under vacuum. A leak can draw air into the apparatus and cause a violent reaction to occur.

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FAQ

What is a handheld XRF analyzer?

A handheld XRF analyzer, also known as a handheld X-ray fluorescence spectrometer, is a portable device used for elemental analysis. It provides fast and accurate results without the need to destroy samples, making it convenient for various industries.

What are the main types of glass materials available?

The main types of glass materials include Alkali-free/Boro-aluminosilicate glass, Optical ultra-clear glass, K9 quartz glass, Soda-lime optical glass, High-temperature resistant optical quartz glass, Glass oscillating beads, High borosilicate glass stirring rods, Glassy carbon sheets, Infrared silicon lenses, Glassy carbon electrodes, Glass tissue grinders, Micro-injectors, Lab pellet presses, and PTFE measuring cylinders.

What materials require preparation for XRF analysis?

Materials that are not already in powder, liquid, or solid disc form, such as plastics, fibers, alternative fuels, and materials subject to RoHS/WEEE legislation, need preparation for XRF analysis.

What are the general steps for preparing a sample for XRF analysis?

The general steps include crushing the material to reduce its size, grinding to produce a fine powder, and pressing or fusing to create a robust, homogeneous, and representative sample.

Why is it important to mill a sample to a fine powder for XRF?

Milling a sample to a fine and consistent powder ensures optimal distribution and evenness in the XRF sample, leading to better accuracy, repeatability, and consistency of results.

What is the difference between a standard and a ring XRF pellet die?

A standard XRF pellet die allows direct pressing of a sample, which can be used as is depending on the spectrometer's sample holder. Alternatively, a crushable aluminum support cup is commonly used.

How does XRD work in material characterization?

XRD uses Bragg’s Law of X-ray diffraction to identify and characterize compounds based on their diffraction patterns. It measures the degree of order or disorder in atomic placements inside the sample, characterizing both crystalline and amorphous parts of the material.

What is milling equipment used for?

Milling equipment is used for the precise shaping, sizing, and finishing of various materials. It is commonly employed in manufacturing processes to remove excess material, create complex shapes, and achieve tight tolerances. Milling machines are versatile tools capable of performing tasks such as cutting, drilling, boring, and contouring.

What are the main applications of handheld XRF analyzers?

Handheld XRF analyzers are used in multiple fields including metal material testing (e.g., military, aerospace, steel), environmental protection (e.g., soil, water, air analysis), construction (e.g., building material quality control), and archaeology (e.g., cultural relics protection). They help in identifying elemental composition, ensuring material quality, and monitoring environmental pollutants.

What is a sieving machine?

A sieving machine, also known as a sieve shaker or vibratory sieve, is a device used to separate particles based on their size or distribution. It consists of a vibrating screen or mesh that allows smaller particles to pass through while larger particles are retained on the screen surface. The machine typically operates by applying vibration or oscillation to the screen, causing the particles to move and separate based on size.

What are the applications of borosilicate glass?

Borosilicate glass is highly resistant to thermal expansion, making it suitable for applications that require resistance to temperature changes, such as laboratory glassware and cooking utensils. It is also used in optical applications due to its clarity and durability.

How do you prepare pressed pellets for XRF?

Pressed pellets for XRF analysis are prepared by grinding the sample to a fine particle size and mixing it with a binder or grinding aid. The mixture is then poured into a pressing die and compressed at a pressure of between 15 and 35T. The resulting pellet is ready for analysis. It is important to consider the particle size of the sample, choice of binder, sample dilution ratio, pressure used for pressing, and the thickness of the pellet when designing a sample preparation recipe. Consistency in the preparation procedure is key to ensuring accurate and repeatable results.

What are the different types of milling equipment?

There are several types of milling equipment, including vertical milling machines, horizontal milling machines, and gantry milling machines. Vertical milling machines have a vertically oriented spindle that moves the cutting tool up and down. Horizontal milling machines have a horizontally oriented spindle and are typically used for larger, heavy-duty applications. Gantry milling machines have a bridge-like structure that supports the spindle and allows for precise movement in multiple directions.

How does a handheld XRF analyzer work?

A handheld XRF analyzer works through four main steps: emission of X-rays, excitation of the sample causing it to fluoresce, measurement of the emitted X-rays by the detector, and analysis of the energy spectrum to determine the elements present and their quantities.

What are the advantages of using a sieving machine?

Sieving machines offer several advantages in particle size analysis and separation processes. They provide a quick and efficient method for separating particles into different size fractions, enabling accurate particle size distribution analysis. The machines are versatile and can handle a wide range of materials, including powders, granules, and bulk solids. They are also easy to use and require minimal operator intervention. Sieving machines can be equipped with different mesh sizes or screen types to accommodate various particle size ranges. Additionally, modern sieving machines often come with advanced features such as automated controls, programmable settings, and data logging capabilities, enhancing productivity and data accuracy.

What are the advantages of using optical glass in laboratory settings?

Optical glass is manufactured using specific chemicals that enhance properties crucial for optics applications, such as clarity, refractive index, and durability. It is widely used in telecommunications, astronomy, and other fields requiring precise light manipulation.

What pressure should XRF pellets be?

XRF pellets should be pressed at pressures between 15 and 40 tons for 1-2 minutes to ensure that the binder recrystallizes and that there are no void spaces present in the pellet. The pressure applied by the hydraulic press should be enough for the sample to be completely compressed. The thickness of the pellet is also crucial, as it must be infinitely thick to the X-rays. Working with small particle sizes (<50µm or <75µm) is also important for effective analysis. These factors impact how well the sample binds together under pressure, which affects the analytical results.

What materials can be processed using milling equipment?

Milling equipment can process a wide range of materials, including metals, plastics, composites, and wood. Common metals processed using milling machines include steel, aluminum, brass, and titanium. Plastics such as acrylic, PVC, and nylon can also be milled. Additionally, milling equipment can shape and finish composite materials like carbon fiber and fiberglass, as well as wood and other organic materials.

What are the advantages of using a handheld XRF analyzer?

The advantages include portability, ease of use on-site, non-destructive testing without the need for sample preparation, short detection times for reliable results, and minimal maintenance costs. They also offer a wide range of tools and a built-in alloy library for comprehensive analysis.

What types of materials can be sieved using a sieving machine?

Sieving machines can be used to sieve a wide range of materials, including but not limited to sands, soils, powders, granules, pharmaceuticals, food products, chemicals, and minerals. The machines are suitable for sieving materials with particle sizes ranging from a few micrometers to several millimeters. Different mesh sizes or screen types can be selected based on the desired particle size range. Sieving machines are commonly used in industries such as mining, pharmaceuticals, food processing, cosmetics, and chemical manufacturing, where particle size analysis and separation are critical for quality control and process optimization.

How is soda-lime glass manufactured, and what are its applications?

Soda-lime glass is created by floating molten glass on molten tin, ensuring uniform thickness and exceptionally flat surfaces. It is widely favored as an insulating substrate for thin/thick film deposition in laboratory settings.

What is the advantage of XRF pressed pellet technique?

The advantage of XRF pressed pellet technique is that it produces high-quality results with a higher signal-to-noise ratio, allowing for the detection of even the lightest elements. Quantifying the elemental composition without pressed pellets can lead to significant discrepancies between expected and actual values. The grinding of the sample into fine particles and compressing it into a smooth and flat XRF pellet reduces background scattering and improves the detection of emissions. Pressed pellets are also relatively quick, low-cost, and lend themselves to simple and cost-effective automation for higher throughput laboratories.

How does milling equipment work?

Milling equipment operates by rotating a cutting tool, typically a multi-point cutter, against the workpiece. The cutting tool removes material from the workpiece as it moves along various axes. The movement of the cutting tool and the workpiece can be controlled manually or through computer numerical control (CNC) systems. The cutting tool may have different geometries, such as end mills, ball mills, or face mills, depending on the desired outcome. The precise control of the cutting tool's movement allows for the creation of intricate shapes, precise dimensions, and smooth surface finishes.

Can handheld XRF analyzers be used for all elements?

Handheld XRF analyzers can measure a wide range of elements, typically from phosphorus to plutonium (P–Pu) on the periodic table. However, they may not be suitable for every element in the periodic table.

How does a sieving machine work?

A sieving machine operates by using vibration or oscillation to separate particles based on size. The machine consists of a vibrating screen or mesh that allows smaller particles to pass through while larger particles are retained on the screen surface. As the machine is turned on, a vibrating motor or other mechanism generates vibration or oscillation, causing the screen to move rapidly. This movement agitates the particles on the screen, allowing smaller particles to pass through the openings in the mesh, while larger particles are retained. The sieving process can be further enhanced by adjusting the amplitude and frequency of the vibrations to optimize separation efficiency. The separated fractions can then be collected and analyzed for particle size distribution or further processing.

What makes K9 quartz glass suitable for optical applications?

K9 glass, also known as K9 crystal, is a type of optical borosilicate crown glass renowned for its exceptional optical properties, including high clarity and precise refractive index, making it ideal for various optical applications.

What are the advantages of using milling equipment?

Milling equipment offers several advantages in manufacturing processes. Firstly, it allows for the precise removal of excess material, resulting in accurate and consistent part dimensions. Secondly, milling machines can create complex shapes and features that would be challenging or impossible to achieve using other methods. Thirdly, milling equipment provides high productivity, as it can remove material quickly and efficiently. Additionally, modern CNC milling machines offer automation and programming capabilities, reducing manual labor and increasing efficiency. Lastly, milling equipment provides versatility, as it can be used for a wide range of materials and applications.

How fast can a handheld XRF analyzer provide results?

Handheld XRF analyzers can provide results within 1-2 seconds for alloy grade identification, making them highly efficient for on-site use.

Can a sieving machine be used for wet sieving?

Yes, some sieving machines are designed specifically for wet sieving applications. These machines are equipped with waterproof enclosures and special screens or mesh that can withstand contact with liquids. Wet sieving is commonly used for analyzing particle size distribution in suspensions or slurries. The process involves immersing the sample in a liquid medium while sieving to prevent agglomeration or clogging of the mesh. The liquid medium helps to disperse the particles and facilitate their passage through the screen. Wet sieving is often utilized in industries such as ceramics, construction materials, and environmental testing, where particles are present in a liquid form. It is important to select a sieving machine specifically designed for wet sieving and follow proper procedures to ensure accurate and reliable results.

What are the benefits of using PTFE measuring cylinders in laboratories?

PTFE cylinders are chemically inert over a wide temperature range (up to 260º C), have excellent corrosion resistance, and maintain a low coefficient of friction, ensuring ease of use and cleaning. They are a rugged alternative to traditional glass cylinders.

What factors should be considered when selecting milling equipment?

Several factors should be considered when selecting milling equipment. These include the required machining capabilities, such as the size and complexity of the parts to be produced, as well as the desired precision and surface finish. The type of material to be processed is also crucial, as different milling machines may be better suited for specific materials. Other factors to consider include the available workspace, the required spindle speed and power, the availability of tooling and accessories, as well as the budget and maintenance requirements. It is important to choose milling equipment that aligns with the specific machining needs and production goals to ensure optimal performance and cost-effectiveness.

Are handheld XRF analyzers suitable for environmental monitoring?

Yes, handheld XRF analyzers are suitable for environmental monitoring. They can quickly analyze heavy metal content in soil, water, and air samples, helping to detect and address environmental pollution issues.

Why is glass a preferred material for laboratory equipment?

Glass has a smooth surface that offers an excellent view of what is going on inside the equipment, enhancing the efficiency of inspection in each process. It is also clear and provides good optical properties, making it a preferred material for laboratory equipment.

Do handheld XRF analyzers require extensive training to use?

No, handheld XRF analyzers are designed for ease of use, requiring minimal training. Their intuitive interfaces and simple menu navigation make them accessible even for minimally trained users.
View more faqs for this product

4.7

out of

5

The XRD X-ray diffraction grinder is a great tool for sample preparation. It's easy to use and produces high-quality results. I highly recommend it.

Mihaela Manea

4.8

out of

5

This grinder is a game-changer for our lab. It's incredibly efficient and has helped us save a lot of time and effort. The results are also very consistent and reliable.

Dr. Samir Saied

4.9

out of

5

I've been using this grinder for a few months now and I'm very impressed with its performance. It's very easy to operate and the results are always consistent. I highly recommend it to anyone who needs a reliable and efficient grinder.

Ms. Aylin Aydin

4.6

out of

5

This grinder is a great investment for any lab. It's very well-made and produces high-quality results. I'm very happy with my purchase.

Mr. Amir Hossein

4.7

out of

5

I'm very impressed with the XRD X-ray diffraction grinder. It's very easy to use and produces high-quality results. I highly recommend it to anyone who needs a reliable and efficient grinder.

Dr. Sonia Patel

4.8

out of

5

This grinder is a great addition to our lab. It's very efficient and has helped us save a lot of time and effort. The results are also very consistent and reliable.

Mr. David Cohen

4.9

out of

5

I've been using this grinder for a few months now and I'm very impressed with its performance. It's very easy to operate and the results are always consistent. I highly recommend it to anyone who needs a reliable and efficient grinder.

Ms. Amina Siddique

4.6

out of

5

This grinder is a great investment for any lab. It's very well-made and produces high-quality results. I'm very happy with my purchase.

Mr. Jorge Garcia

4.7

out of

5

I'm very impressed with the XRD X-ray diffraction grinder. It's very easy to use and produces high-quality results. I highly recommend it to anyone who needs a reliable and efficient grinder.

Dr. Sarah Khan

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