Products Sample Preparation Milling Equipment Liquid nitrogen cryogenic vibration ball mill
Liquid nitrogen cryogenic vibration ball mill

Milling Equipment

Liquid nitrogen cryogenic vibration ball mill

Item Number : Kt-VBM100

Price varies based on specs and customizations


Maximum injection size
< 5 mm
Sample particle size range
20um
Grinding amount
1g-20g
Vibration frequency
3000-3600r/min
ISO & CE icon

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Introduction

KT-VBM100 is a laboratory desktop high-performance vibrating ball mill and sieving dual-purpose small and lightweight instrument. The vibrating platform with a vibration frequency of 36,000 times/min provides energy. The grinding ball with a diameter of 60mm and a volume of 150ml is used for grinding. The mortar, through the violent collision of the ball and the mortar, is used for conventional grinding of hard, brittle, and materials. At the same time, liquid nitrogen can be poured into the mortar to improve the brittleness of soft, elastic, fibrous, and other difficult-to-handle samples. For crushing or grinding, KT-VBM100 can also be used as a sieving machine with 2-5 layers of analytical sieves with a diameter of 100-150mm and a precision of 20µm-63mm. The sieving weight is 3kg, and it can be used for dry sieving or wet sieving.

  • Liquid nitrogen cryogenic vibration ball mill
  • Processing principle: impact force
  • Application sample characteristics: medium and low hardness | brittle | elastic | fibrous | soft
  • Processing Type: Grinding | Sieving
  • Main functions: continuous operation|intermittent operation|timing start|timer|one key repeat|power-off memory|temperature monitoring
  • Additional features: Quick-lock platen with viewing window | Funnel for pouring liquid nitrogen | Grinding chamber exhaust

Applications

The Liquid Nitrogen Cryogenic Vibration Ball Mill is a specialized piece of equipment designed for grinding and pulverizing materials under ultra-low temperatures, utilizing liquid nitrogen as a cooling agent. This technology is particularly beneficial for materials that are heat-sensitive or prone to degradation at higher temperatures. The applications of this mill are diverse and cater to various industries where maintaining the integrity of materials is paramount.

  • Material Science: Ideal for processing metallic powders and microstructured particles, especially those that require low-temperature conditions to prevent oxidation and maintain structural integrity.
  • Pharmaceuticals: Useful for grinding temperature-sensitive pharmaceutical compounds and biological samples, ensuring minimal degradation and preserving their efficacy.
  • Chemical Processing: Effective in pulverizing chemicals that are unstable at higher temperatures, facilitating safer and more efficient chemical reactions.
  • Food and Beverage: Applicable in the production of fine powders from temperature-sensitive food ingredients, enhancing product quality and consistency.
  • Plastics and Polymers: Essential for grinding plastics and polymers at low temperatures to prevent thermal degradation and maintain the physical properties of the materials.
  • Research and Development: Widely used in laboratories for experimental purposes, particularly in studies involving the mechanical and thermal properties of materials.
  • Environmental Remediation: Helps in the processing of materials used in environmental cleanup, ensuring that the materials remain effective and stable under controlled temperatures.

Features

The Liquid Nitrogen Cryogenic Vibration Ball Mill is a cutting-edge laboratory equipment designed to handle the grinding of brittle and heat-sensitive materials. This innovative tool leverages the power of cryogenic temperatures, typically below -150 °C, to ensure the preservation of sample integrity, particularly crucial for materials such as plastics, rubber, and biological samples. Here are the key features that make this mill stand out:

  • Ultra-Low Temperature Grinding: Utilizes liquid nitrogen to cool the grinding chamber, ensuring minimal thermal degradation and optimal preservation of chemical and physical properties of the samples.
  • Fine and Uniform Particle Production: Capable of producing particles with tolerances less than 5 μm, ensuring a high level of precision and uniformity in the ground material.
  • Cryomilling Technology: Combines cryogenic temperatures with mechanical milling to achieve nanostructured microstructures, suppressing recovery and recrystallization for finer grain structures.
  • Versatile Material Processing: Suitable for a wide range of materials including electronics, ceramics, chemicals, powdered metals, and pharmaceuticals, with options for different tank linings such as stainless steel, ceramic, and PTFE.
  • Advanced Control Systems: Features a vibratory feeder and a helical screw conveyor with adjustable speeds, allowing precise control over the grinding process and the feed rate of materials.
  • Efficient Nitrogen Circulation: Vaporized nitrogen is recycled back into the system, enhancing the efficiency of the cryogenic process and reducing waste.

These features not only enhance the grinding efficiency but also ensure that the integrity of sensitive materials is maintained, making the Liquid Nitrogen Cryogenic Vibration Ball Mill an indispensable tool for advanced materials research and processing.

Detail & Parts

Liquid nitrogen cryogenic vibration ball mill details

Liquid nitrogen cryogenic vibration ball mill details

Liquid nitrogen cryogenic vibration ball mill details

Liquid nitrogen cryogenic vibration ball mill details

Technical specifications

Maximum injection size < 5 mm
Sample particle size range 20um
Grinding amount 1g-20g
Vibration frequency 3000-3600r/min
Vibration amplitude 3mm
Vibration mode two dimensional
Liquid nitrogen freezing method Immersion
Grinding temperature -196°C — 40°C
Ball mill material Stainless Steel | Tungsten Carbide | Zirconia
Number of ball mill jars 1
Ball mill tank volume 150ml
Grinding ball material Stainless Steel | Tungsten Carbide | Zirconia
Grinding Ball Diameter 40-60mm
Grinding method Dry Grinding | Wet Grinding | Cryogenic Grinding
Screening method dry sieving | wet sieving
Mesh Diameter 100mm | 150mm
Dry screening range 20um - 63mm
Wet screening range 20um - 10mm
Maximum sieving weight 3kg
Screen layers 2-5 floors
Drive mod mechanical drive
Electrical description 100-120V/200-240V AC, 50-60Hz, 150W
Power port National Standard | European Standard | American Standard | British Standard, etc.
Net weight 35kg
Dimensions (width, depth and height) 400*300*200mm
Protection class IP65
Standard CE
Additional items Wet Screening Locking Platen and Screen Bottom with Nozzles, PC Shield for Cryogenic Grinding

Advantages

The Liquid Nitrogen Cryogenic Vibration Ball Mill offers a range of advantages that enhance the grinding process, particularly for heat-sensitive and brittle materials. Here are the key benefits:

  • Enhanced Material Integrity: By using liquid nitrogen to cool the grinding chamber, the mill preserves the chemical and physical properties of materials, especially crucial for plastics, rubber, and biological samples. This ensures minimal thermal degradation and maintains sample integrity.
  • Optimized Particle Size and Distribution: The cryogenic environment allows for the production of fine and uniform particles. This is particularly beneficial for applications requiring precise particle size distribution, enhancing the overall quality of the ground product.
  • Increased Productivity and Throughput: The mill's design and operation facilitate higher production rates and increased throughput. This is achieved through optimized particle size and efficient grinding mechanisms, leading to increased productivity.
  • Reduced Wear on Grinding Equipment: The use of liquid nitrogen helps in reducing the temperature of the grinding process, which in turn decreases wear on the grinding equipment. This extends the lifespan of the machinery and reduces maintenance costs.
  • Elimination of Caking and Clogging: Cryogenic grinding prevents caking and clogging within the mill, which are common issues in traditional grinding methods. This ensures a smoother operation and continuous production flow.
  • Energy Efficiency: The cryogenic mill operates with lower energy consumption compared to conventional mills. This not only reduces operational costs but also makes the process more environmentally friendly.
  • Improved Pouring Properties: The finely ground materials produced by the cryogenic mill improve the pouring properties of the product, which is beneficial in various industrial applications.
  • Reduction in Microbial Load: The ultra-low temperatures used in cryogenic grinding also help in reducing the microbial load in the ground materials, enhancing the safety and quality of the final product.
  • Separation of Composite Materials: The mill aids in the separation of composite materials within the grinding chamber, which is crucial for materials with multiple components.
  • Lower Grinding Costs: Overall, the combination of higher efficiency, reduced wear, and lower energy consumption leads to lower grinding costs, making the Liquid Nitrogen Cryogenic Vibration Ball Mill a cost-effective solution for grinding applications.

Warnings

Operator safety is the top important issue! Please operate the equipment with cautions. Working with inflammable& explosive or toxic gases is very dangerous, operators must take all necessary precautions before starting the equipment. Working with positive pressure inside the reactors or chambers is dangerous, operator must fellow the safety procedures strictly. Extra caution must also be taken when operating with air-reactive materials, especially under vacuum. A leak can draw air into the apparatus and cause a violent reaction to occur.

Designed for You

KinTek provide deep custom made service and equipment to worldwide customers, our specialized teamwork and rich experienced engineers are capable to undertake the custom tailoring hardware and software equipment requirements, and help our customer to build up the exclusive and personalized equipment and solution!

Would you please drop your ideas to us, our engineers are ready for you now!

FAQ

What is a cold trap chiller in lab?

A cold trap chiller is a device used in laboratory equipment to protect vacuum pumps from contamination by condensing or sublimating vapors in a separate apparatus. It prevents oil vapors from backstreaming from the pump into the system and maintains a chilled stainless steel or glass surface for vapors to condense or sublimate on. The device utilizes an active material such as dry ice or liquid nitrogen or a Peltier element for cooling and can be disassembled for easy cleaning. Cold traps are essential for efficient pump operation and longer service lives.

What is cryomilling and how does it differ from traditional grinding methods?

Cryomilling is a specialized mechanical milling process where samples, especially those that are temperature-sensitive or contain volatile components, are milled in a cryogen slurry or at cryogenic temperatures. This method differs from traditional grinding by operating at very low temperatures, typically using liquid nitrogen, to prevent heat generation, oxidation, and other issues associated with high temperatures. This helps in maintaining the integrity of the materials being processed.

What types of materials are best suited for processing in a Cryogenic Mill?

Cryogenic Mills are particularly effective for processing materials that are heat-sensitive, brittle, or prone to oxidation, such as plastics, rubber, pharmaceuticals, and biological samples. These mills help in maintaining the quality and integrity of these materials by operating at ultra-low temperatures.

How does the Cryogenic Grinding Mill system work?

The Cryogenic Grinding Mill system uses liquid nitrogen to cool the pulverized material to very low temperatures. The chilled material then enters a mechanical pulverizer where it is subjected to high-speed rotation, impact, collision, shearing, and friction, leading to effective pulverization. The system includes a classifier that sorts the pulverized material; finer particles are collected, while coarser particles are returned for further grinding.

What are the applications of pellet presses?

Pellet presses have a wide range of applications across various industries. They are commonly used in the pharmaceutical industry to produce uniform and compacted pellets for drug formulations. In the food industry, pellet presses are used to create animal feed pellets, as well as pellets for snacks and breakfast cereals. Pellet presses are also used in the chemical industry for catalysts, fertilizers, and chemical additives. Additionally, they find application in the biomass industry for the production of wood pellets for fuel, as well as in the metallurgical industry for the production of metal pellets for further processing.

What types of materials can be processed in a rotary furnace?

Rotary furnaces can process a wide range of materials, including ores, minerals, metals, chemicals, and waste materials. They are commonly used for processes such as calcination, drying, roasting, and thermal decomposition. For example, rotary furnaces are utilized in the cement industry for clinker production, in the metallurgical industry for smelting and refining operations, and in the chemical industry for the production of catalysts or chemical reactions requiring heat treatment. The versatility of rotary furnaces allows them to handle different material forms, such as powders, granules, and bulk solids, making them suitable for various applications across multiple industries.

What is the purpose of a cold trap chiller?

The purpose of a cold trap chiller is to protect vacuum pumps from contamination by condensing or sublimating vapors and preventing oil vapors from backstreaming into the system. It provides a chilled surface for vapors to condense or sublimate on and utilizes an active material such as dry ice or liquid nitrogen or a Peltier element for cooling. Cold traps are most commonly used to collect vapor from applications involving rotating discs or vacuum systems, but can also be used on other types of contamination including solids. Cryogenic cold traps are specifically manufactured for cryogenic applications such as the adsorption of noble gases.

How does a pellet press work?

A pellet press works by feeding the material into a chamber where it is compressed by a rotating roller or extrusion plate. The pressure applied forces the material through a die with holes of a specific size and shape, which determines the size and shape of the pellets. The pellets are then cut to the desired length and collected for further processing or packaging. Some pellet presses may also include additional steps, such as drying or cooling the pellets, depending on the specific application.

What are the rotary furnace types?

The rotary furnace types include rotary and tilting furnaces which have the ability to rotate and tilt, allowing for uniformity in drying and coating applications. KINTEK furnaces increase efficiency by offering multi-zone heating options, utilizing alumina fiber for refractory linings, and using temperature controllers. These furnaces are suitable for continuous processing and batch operations. Additionally, they can be opened up to use different tubes or reactors. The galvanized coating covered epoxy painted structure provides a longer lifetime and aesthetics. Overall, the rotary and tilting furnaces are popular for materials production, drying, aging, and oxidation processes.

Why is a cold trap placed before the vacuum pump?

A cold trap is placed before the vacuum pump to prevent vapors, such as vapor from water or solvents, from contaminating the vacuum pump and the airstream. The cold trap condenses or sublimates gases, preventing them from reaching areas of the system that could lead to malfunction. Cold traps collect vapor from applications involving rotating discs or vacuum systems and oil vapors from a pump to prevent them from flowing into the chamber. By using a cold trap, vacuum pumps operate more efficiently and have longer service lives.

What are the benefits of using a pellet press?

A pellet press works by feeding the material into a chamber where it is compressed by a rotating roller or extrusion plate. The pressure applied forces the material through a die with holes of a specific size and shape, which determines the size and shape of the pellets. The pellets are then cut to the desired length and collected for further processing or packaging. Some pellet presses may also include additional steps, such as drying or cooling the pellets, depending on the specific application.

What are the advantages of rotor furnace?

Rotary tube furnaces offer several advantages over static processes. The continuous movement of the sample ensures that the entire surface area is exposed to the atmosphere during processing which improves gas diffusion, reduces gas consumption and increases heat treatment efficiency. Additionally, the material is continuously passed through a hot furnace that is maintaining a consistent temperature profile, improving product homogeneity. Rotary furnaces also offer significant advantages of throughput and energy efficiency over other forms of continuous, high temperature equipment, making them the latest technology for high-temperature processing of powdered materials.

What factors should be considered when selecting a pellet press?

Several factors should be considered when selecting a pellet press. These include the desired pellet size and shape, the material properties, the required production capacity, and the available space and resources. The type and condition of the material being processed, such as its moisture content, particle size, and flowability, can also influence the selection of the pellet press. Additionally, factors such as the power requirements, ease of operation and maintenance, and the availability of spare parts and technical support should be considered. It is important to choose a pellet press that aligns with the specific requirements and objectives of the application to ensure optimal performance and cost-effectiveness.

What is the efficiency of a rotary furnace?

Rotary tube furnaces are highly efficient in transferring heat over a short period of time while continuously running batches of materials. They also minimize material handling, making them ideal for powder processing. KINTEK offers custom-designed rotary tube furnaces that can be built to specific requirements for maximum temperature control, workspace size, residence time, tube rotation rate, tube inclination angle, temperature profile, atmosphere flow rate, powder bed depth, and feed rate. When choosing a tube for the furnace, key considerations include rotational speed, amount of material, tube diameter, suspended length, and tube thickness. The choice of tube material should also be based on potential applications.

Can a rotary furnace be used for continuous production?

Yes, rotary furnaces can be used for continuous production depending on the specific application and process requirements. Continuous operation is achieved by feeding materials into the furnace at a controlled rate while maintaining a steady rotation speed. This allows for a continuous flow of processed materials out of the furnace. Rotary furnaces are often utilized in industries requiring continuous thermal treatment, such as cement production or metallurgical processes. However, it is important to ensure proper design, sizing, and integration of auxiliary equipment, such as feed systems and discharge mechanisms, to enable continuous operation effectively. Additionally, proper monitoring and control systems should be in place to maintain consistent process parameters and product quality throughout the continuous production cycle.

How can the performance of a rotary furnace be optimized?

The performance of a rotary furnace can be optimized through various means. Proper selection and control of process parameters, such as temperature, rotation speed, and residence time, are critical for achieving the desired results. Optimization can be achieved by adjusting these parameters based on the specific materials and process requirements. Regular maintenance, including cleaning, lubrication, and inspection of the furnace components, is essential to ensure optimal performance and prevent unexpected failures. Implementing advanced control systems and automation can enhance process efficiency, accuracy, and repeatability. Additionally, monitoring and analyzing process data, such as temperature profiles and energy consumption, can help identify opportunities for improvement and optimize energy efficiency. Collaboration with furnace manufacturers or process experts can provide valuable insights and recommendations for optimizing the performance of a rotary furnace.
View more faqs for this product

4.8

out of

5

Excellent mill for grinding various materials. The cryogenic feature is a game-changer for temperature-sensitive samples.

Tracy M. Smith

4.9

out of

5

This mill has exceeded our expectations. The speed and efficiency of the grinding process are remarkable.

Dr. Omar K. Patel

4.7

out of

5

The mill is very user-friendly and produces consistent results. We've seen a significant improvement in our sample preparation time.

Ms. Sophia A. Johnson

4.6

out of

5

The build quality of this mill is top-notch. It's evident that KINTEK SOLUTION puts a lot of care into their products.

Mr. David R. Garcia

4.9

out of

5

The technical support from KINTEK SOLUTION is outstanding. They were very responsive and helpful when we had questions about the mill.

Dr. Maria C. Rodriguez

4.8

out of

5

The mill is very versatile and can handle a wide range of materials. We've been able to use it for both dry and wet grinding applications.

Mr. Antonio J. Hernandez

4.7

out of

5

The mill is very quiet, which is a big plus for our lab. It doesn't disrupt our other experiments.

Ms. Sarah L. Kim

4.9

out of

5

The mill is very easy to clean and maintain. It saves us a lot of time and effort.

Mr. Michael D. Lee

4.8

out of

5

Overall, we are very satisfied with the Liquid nitrogen cryogenic vibration ball mill. It's a valuable addition to our lab.

Dr. Elizabeth S. Jones

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Catalog of Rotary Furnace

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Catalog of Cold Trap Chiller

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