Products Sample Preparation Molds & Accessories XRF Boric Acid Lab Powder Pellet Pressing Mold for Laboratory Use
XRF Boric Acid Lab Powder Pellet Pressing Mold for Laboratory Use

Molds & Accessories

XRF Boric Acid Lab Powder Pellet Pressing Mold for Laboratory Use

Item Number : PMXB

Price varies based on specs and customizations


Material
Cr12MoV
Indenter hardness
HRC60-HRC62
Sample size
φ32 / φ40 mm
Cavity depth
45 mm
External dimensions
φ73×133 mm
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Applications

XRF Boric Acid Powder Pellet Pressing Mold wraps the sample with boric acid powder and then presses the powder into shape, which is mainly used for sample preparation of X-ray fluorescence spectrometer samples.

Special sizes press molds can be customized according to customer requirements.

Detail & Parts

XRF Boric Acid lab Powder Pellet Pressing Mold details
XRF Boric Acid Lab Powder Pellet Pressing Mold for Laboratory Use
Sample preparation process and demolding process
Sample preparation process and demolding process

Technical specifications

Instrument model PMXB
Press the shape of the sample
Mold material Alloy tool steel:C-12Nov
Indenter hardness HRC60-HRC62
Sample size Φ32、Φ40mm
Depth of cavity 45m (N)
External dimensions Φ73X133mm(LXH)
Mold weight 3.2Kg
Size diagram

Mold pressure conversion table

The pressure is strong.[Mpa] 50 100 200 300 400 600 800 1000 1200 1500
Φ32 T 4.02 8.04 16 24.1 32.1 48.2 64.3 80.4 96.5 120
Φ40 T 6.28 12.5 25.1 37.6 50.2 75.3 100 125 150 188
Tip: The mold is used in 100-800 MPa domestically, and the maximum meal limit of the mold is 1500 MPa.

Operation steps

Boracic acid dies are used to wrap the sample with boracic acid powder and then press the powder. It is suitable for forming of x-ray fluorescence spectrophotometer samples. Die sheet size: outer diameter 40 mm; sample size: 32mm; sheet thickness: 5~8 mm; special dies can be customized according to requirements.

Step 1: Assemble the die according to the operation diagram and install the sample in the cavity.

Step 1: Assemble the die according to the operation diagram and install the sample in the cavity.

Step 2: Put the die in the center of the hydraulic press and pressurize to required pressure.

Step 2: Put the die in the center of the hydraulic press and pressurize to required pressure.

Step 3: Assemble the die according to the release diagram , eject the sample out of the die bushing with the screw rod.

Step 3: Assemble the die according to the release diagram , eject the sample out of the die bushing with the screw rod.

Step 4: Take out the die from the hydraulic press , and remove the sample gently.

Step 4: Take out the die from the hydraulic press , and remove the sample gently.

Precautions for mold maintenance

To ensure accurate test results, clean the mold surface with dust-free paper before each use to avoid the anti-rust oil from affecting the sample. Avoid exceeding the maximum pressure when applying pressure. Clean the mold and samples after use to prevent corrosion. Apply anti-rust oil and store the mold in a dry environment if not used for a long time to prevent damage.

Step 1: Placing the Mold.

Step 1: Placing the Mold.

To begin, place the mold in the center of the tablet press. It is important to note that the maximum pressure of the mold cannot be exceeded when pressurized. This will prevent any damage to the mold and ensure accurate test results.

Step 2: Cleaning the Mold.

Step 2: Cleaning the Mold.

After each use, it is essential to clean the mold to prevent any contamination of the sample. Using dust-free paper, wipe the surface of the mold clean. If there are sample residues on the surface that cannot be removed, please do not use chemical reagents to clean and soak. This could potentially damage the mold and impact the accuracy of the test results.

Step 3: Applying Anti-Rust Oil.

Step 3: Applying Anti-Rust Oil.

If the mold is not used for an extended period, it is recommended to apply anti-rust oil on the surface of the mold to prevent rusting. This step will help prolong the life of the mold and ensure that it remains in good condition for future use.

Step 4: Storing the Mold.

Step 4: Storing the Mold.

Lastly, if the mold is not used for a long time, it needs to be stored in a dry environment. This will prevent any moisture from accumulating on the mold and causing damage.

Full range of lab press types

Full range of lab press types

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Full range of types of laboratory press molds

We have a full range of molds for you to choose from, and the molds fit the body perfectly.

If you need molds with special shapes, we can also customize them for you.

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Warnings

Operator safety is the top important issue! Please operate the equipment with cautions. Working with inflammable& explosive or toxic gases is very dangerous, operators must take all necessary precautions before starting the equipment. Working with positive pressure inside the reactors or chambers is dangerous, operator must fellow the safety procedures strictly. Extra caution must also be taken when operating with air-reactive materials, especially under vacuum. A leak can draw air into the apparatus and cause a violent reaction to occur.

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FAQ

What Is A Press Mold?

A press mold is a device used in material processing methods such as cold isostatic pressing (CIP) and metal mold pressing to create molded bodies from powder materials. In CIP, the mold containing the powder is immersed in a pressure medium, and isostatic pressure is applied to the outer surfaces of the mold to compress the powder into a shape. Metal mold pressing applies only uniaxial pressure to the powder material to create molded bodies. CIP can produce products with uniform density and homogeneity due to no frictions with a metal mold.

What Are The Applications Of Pellet Presses?

Pellet presses have a wide range of applications across various industries. They are commonly used in the pharmaceutical industry to produce uniform and compacted pellets for drug formulations. In the food industry, pellet presses are used to create animal feed pellets, as well as pellets for snacks and breakfast cereals. Pellet presses are also used in the chemical industry for catalysts, fertilizers, and chemical additives. Additionally, they find application in the biomass industry for the production of wood pellets for fuel, as well as in the metallurgical industry for the production of metal pellets for further processing.

What Is Press Mould In Ceramics?

Press moulding is a ceramic forming technique that involves the compaction of powders by applying either a rigid or flexible pressure. It can be either uniaxial or isostatic, depending on the shape required. Isostatic pressing is used for shapes that cannot be obtained by uniaxial pressing or for added value products that require high density and isotropic green bodies. The molds for axial-pressing are usually made of steel, while those for isostatic pressing are made of elastomers, silicone, and polyurethanes. This technology is applied in various fields like ceramics, MMC, CMC, and Silicon nitride for cutting tools, components of heavy-duty valves, wear parts for process technology, and more.

How Does A Pellet Press Work?

A pellet press works by feeding the material into a chamber where it is compressed by a rotating roller or extrusion plate. The pressure applied forces the material through a die with holes of a specific size and shape, which determines the size and shape of the pellets. The pellets are then cut to the desired length and collected for further processing or packaging. Some pellet presses may also include additional steps, such as drying or cooling the pellets, depending on the specific application.

How Do You Prepare Pressed Pellets For XRF?

Pressed pellets for XRF analysis are prepared by grinding the sample to a fine particle size and mixing it with a binder or grinding aid. The mixture is then poured into a pressing die and compressed at a pressure of between 15 and 35T. The resulting pellet is ready for analysis. It is important to consider the particle size of the sample, choice of binder, sample dilution ratio, pressure used for pressing, and the thickness of the pellet when designing a sample preparation recipe. Consistency in the preparation procedure is key to ensuring accurate and repeatable results.

How Are Pellet Molds Used?

To use a pellet mold, the powdered or granular material is first loaded into the mold cavity. The material is then compacted by applying pressure using a laboratory press or hydraulic machine. The pressure causes the material to conform to the shape of the mold, resulting in a solid pellet or cylindrical sample. After the compaction process, the pellet is removed from the mold and can be further processed or analyzed as needed.

What Are The Benefits Of Using A Pellet Press?

A pellet press works by feeding the material into a chamber where it is compressed by a rotating roller or extrusion plate. The pressure applied forces the material through a die with holes of a specific size and shape, which determines the size and shape of the pellets. The pellets are then cut to the desired length and collected for further processing or packaging. Some pellet presses may also include additional steps, such as drying or cooling the pellets, depending on the specific application.

What Pressure Should XRF Pellets Be?

XRF pellets should be pressed at pressures between 15 and 40 tons for 1-2 minutes to ensure that the binder recrystallizes and that there are no void spaces present in the pellet. The pressure applied by the hydraulic press should be enough for the sample to be completely compressed. The thickness of the pellet is also crucial, as it must be infinitely thick to the X-rays. Working with small particle sizes (<50µm or <75µm) is also important for effective analysis. These factors impact how well the sample binds together under pressure, which affects the analytical results.

What Types Of Materials Can Be Pelletized Using Pellet Molds?

Pellet molds can be used to pelletize a wide range of materials, including but not limited to powders, granules, metals, ceramics, pharmaceuticals, and catalysts. They are particularly useful for materials that require compaction or shaping before further analysis or processing. Pelletizing materials can improve their flow properties, density, and handling characteristics, making them suitable for applications such as tabletting, catalyst preparation, fuel pellet production, and sample preparation for spectroscopic or analytical techniques.

What Factors Should Be Considered When Selecting A Pellet Press?

Several factors should be considered when selecting a pellet press. These include the desired pellet size and shape, the material properties, the required production capacity, and the available space and resources. The type and condition of the material being processed, such as its moisture content, particle size, and flowability, can also influence the selection of the pellet press. Additionally, factors such as the power requirements, ease of operation and maintenance, and the availability of spare parts and technical support should be considered. It is important to choose a pellet press that aligns with the specific requirements and objectives of the application to ensure optimal performance and cost-effectiveness.

What Is The Advantage Of XRF Pressed Pellet Technique?

The advantage of XRF pressed pellet technique is that it produces high-quality results with a higher signal-to-noise ratio, allowing for the detection of even the lightest elements. Quantifying the elemental composition without pressed pellets can lead to significant discrepancies between expected and actual values. The grinding of the sample into fine particles and compressing it into a smooth and flat XRF pellet reduces background scattering and improves the detection of emissions. Pressed pellets are also relatively quick, low-cost, and lend themselves to simple and cost-effective automation for higher throughput laboratories.

How Can One Select The Appropriate Pellet Mold For Their Specific Application?

Pellet molds can be used to pelletize a wide range of materials, including but not limited to powders, granules, metals, ceramics, pharmaceuticals, and catalysts. They are particularly useful for materials that require compaction or shaping before further analysis or processing. Pelletizing materials can improve their flow properties, density, and handling characteristics, making them suitable for applications such as tabletting, catalyst preparation, fuel pellet production, and sample preparation for spectroscopic or analytical techniques.
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XRF Boric Acid Lab Powder Pellet Pressing Mold for Laboratory Use

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