Short Path Distillation

2L Short Path Distillation

Name: 2L Short Path Distillation
Brand: Kintek Solution
SKU: SPD-1
Rating: 4.77 (14 reviews)

Item Number : SPD-1

Price varies based on specs and customizations

Glassware: yes
Heating mantle: yes
Chilling circulator: yes
Vacuum pump: yes
Fittings: yes

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Applications

Short path distillation is an important technique to extract or purify target mixed liquids by the method of distillate short traveling distance. Distillation is completed under the high vacuum condition, which will create low pressure environment and lower the liquids boiling point, high at the same means that lower heating temperature. Low temperature heating will reduce the impact to the heat sensitive materials, and increase the distillation quality.

Detail & Parts

Short Path Distillation Details

Flexible choice of rotary vane vacuum oil pump.

Flexible choice of desktop high efficiency heater/chillers.

Advantages

Heavy duty Borosilicate 3.3 glassware, durable use
Fast heating mantle with magnetic stirring function
Cold trap project the vacuum pump and increase service life
Delicate fitting device make system smoothly operating

2L Short path distillation specifications

Glassware	Glass material	High borosilicate glass 3.3
	Flask volume	2L
	Receiver flask	3*500ml
	Cold trap	Dry ice type condensor
Heating mantle	Heating power	650W
	Temperature range	RT-380℃
	Thermometer	PT100
	Stirring method	Magnetic
	Stirring power	40W
	Stirring speed	50-2000RPM
Chilling circulator	Temperature range	-10-99℃
	Reserver volume	6L/180160150mm
	Pump flowrate	4L/Min
Vacuum pump	Pump type	Dual stage rotary vane pump
	Pumping rate	1.1L/S at 50HZ; 1.3L/S at 60HZ
	Ultimate pressure	3Pa
	Power rating	400/370kW
	Net weight	19kg
Fittings	Supportor	150*150mm SS jack with cork ring
	Vacuum piping	Silicon hose
	Keck clamp	SS/Plastic
	Thermometer	Range 0-200℃ with 30cm length

Warnings

Operator safety is the top important issue! Please operate the equipment with cautions. Working with inflammable& explosive or toxic gases is very dangerous, operators must take all necessary precautions before starting the equipment. Working with positive pressure inside the reactors or chambers is dangerous, operator must fellow the safety procedures strictly. Extra caution must also be taken when operating with air-reactive materials, especially under vacuum. A leak can draw air into the apparatus and cause a violent reaction to occur.

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FAQ

What Is The Short Path Distillation?

Short path distillation is a purification technique that separates compounds based on their volatilities in a boiling liquid mixture under reduced pressure. It involves the distillate traveling a short distance, often only a few centimeters, and is done at reduced pressure. Short path distillation is ideal for laboratory applications where minimal instrumentation footprint is crucial. The boiling temperature is reduced by lowering the operating pressure, making it a continuous process with very short residence time. It is often used for unstable compounds or to purify small amounts of compounds, achieving distillate purity levels of up to 99%.

What Is The Purpose Of A Rotary Evaporator?

The purpose of a rotary evaporator, or rotovap, is to distill a solvent to separate a given mixture into its components based on their respective volatilities, through the process of evaporation and condensation. The rotovap is used to concentrate non-volatile components in a mixture and to extract volatile aroma and flavor molecules from mixtures gently and at low temperatures. The two key components of the rotovap allow for a gentle, precise, and efficient distillation not found in conventional distilling apparatuses: vacuum removal of solvent to lower boiling point and rotary flask rotation to increase surface area and speed up distillation.

What Are High Purity Materials?

High purity materials refer to substances that are free from impurities and possess a high level of chemical homogeneity. These materials are essential in various industries, particularly in the field of advanced electronics, where impurities can significantly affect the performance of devices. High purity materials are obtained through various methods, including chemical purification, vapor-phase deposition, and zone refining. In the preparation of electronic grade single crystal diamond, for example, a high-purity raw material gas and an efficient vacuum system are necessary to achieve the desired level of purity and homogeneity.

Is Short Path Distillation The Same As Distillation?

Short path distillation is a type of distillation technique used to separate and purify small amounts of compounds that are not stable at high temperatures. It involves the distillate traveling a short distance, often only a few centimeters, at reduced pressure. While short path distillation is a specific type of distillation, it is not the same as traditional distillation, which typically involves heating a mixture to its boiling point and condensing the vapors. Short path distillation allows for a lower heating temperature and a shorter distillation distance, resulting in less loss of compound and more efficient purification.

Why Rotary Evaporator Is Used In Solvent Extraction?

Rotary evaporators are used in solvent extraction because they allow for the efficient and gentle removal of solvents from samples by evaporation. This is achieved by reducing the pressure to lower the solvent boiling point, rotating the sample to increase the effective surface area, heating the solution, and then condensing the evaporated solvent in a cooled glass condenser. This process leaves the concentrated compound in the flask and is often used in medicinal chemistry, pharmaceutical, chromatography, and petrochemical fields.

What Are Examples Of Short Path Distillation?

Some examples of short path distillation include processing edible oils, creating fragrances, producing fuels, distilling polyurethane, distilling compounds that are unstable at high temperatures, and distilling small quantities of a compound.

Can Rotary Evaporator Remove Water?

Yes, a rotary evaporator can remove water. By changing the temperature to speed up the evaporation rate or by vacuuming with a vacuum pump to further reduce the pressure and lower the boiling point, a rotary evaporator can evaporate solutions that contain water and other substances. The electronic control of the rotary evaporator keeps the rotation of the flask at a constant speed, creating a larger surface area for heating and faster evaporation speeds. The traditional distillation method is less efficient and accurate than a rotary evaporator, which is widely used in chemical laboratories, industrial, bio-pharmaceutical, and food-making fields.

What Are The Common Materials Used For Evaporating Crucibles?

Evaporating crucibles are commonly made from materials such as tungsten, tantalum, molybdenum, graphite, or ceramic compounds. These materials have high melting points and good thermal conductivity, making them suitable for the high-temperature conditions required during evaporation. The choice of crucible material depends on factors such as the evaporant material, desired film properties, and process parameters.

What Temperature Is Short Path Distillation?

The Short Path Vacuum Distillation operates at a temperature far below the boiling point of the material being distilled, allowing for the purification of heat-sensitive materials at much lower temperatures. The ultimate pressures of 0.001 mbar can be achieved, which prevents degradation and allows for very high equivalent temperatures to be achieved at ambient pressure. The high vacuum distillation technique enables the separation of heat-sensitive or high molecular weight compounds not possible by conventional techniques.

What Are The Advantages Of Short Path Distillation?

Short path distillation has several advantages over other distillation processes. It offers a continuous feed functionality, faster completion time, and is ideal for compounds that are unstable at high temperatures. It is also automated and easy to use, produces high concentrations of distillates, and reduces product waste. These benefits make short path distillation a highly advantageous option for a variety of uses and applications, especially in industries with time-sensitive materials and production cycles.

How Long Does Short Path Distillation Take?

The length of time it takes to complete short path distillation depends on various factors, such as the type and quantity of the compound being distilled, the equipment used, and the skill of the operator. Generally, short path distillation is a relatively quick process, with some runs taking as little as 30 minutes, while others may take several hours. The key to a successful distillation is to carefully monitor the temperature and pressure throughout the process and adjust as necessary to ensure maximum efficiency and purity of the end product.

Is Rotary Evaporator Used For Distillation?

Yes, rotary evaporator is used for distillation. It is a device used in chemical laboratories to efficiently and gently remove solvents from samples by evaporation. The system works by reducing the pressure to lower the solvent boiling point, rotating the sample to increase the effective surface area, heating the solution, and then the evaporated solvent condenses in a cooled glass condenser. Rotary evaporation is most often and conveniently applied to separate "low boiling" solvents such as n-hexane or ethyl acetate from compounds which are solid at room temperature and pressure.

What Are The Advantages Of Using Evaporating Crucibles?

Evaporating crucibles offer several advantages in thin film deposition processes. They provide a controlled environment for the evaporation of materials, allowing for precise control over film thickness and uniformity. Crucibles can withstand high temperatures and provide efficient heat transfer, ensuring consistent evaporation rates. They are available in various sizes and shapes to accommodate different evaporation systems and substrate configurations. Evaporating crucibles also allow for the deposition of a wide range of materials, including metals, semiconductors, and ceramics. They can be easily loaded and unloaded, facilitating quick material changes or process adjustments. Overall, evaporating crucibles are essential tools in thin film deposition techniques, offering versatility, reliability, and reproducibility.

What Are The Principles Of Rotary Evaporation?

The basic principle of rotary evaporation is to increase a sample's surface area and optimize its temperature and vacuum level, enabling effective separation of solvents in a short time. A cooling condenser helps to recover the separated solvent. It is a gentle and efficient method for liquid separation and purification, with specific applications including concentration, crystallization, solvent distillation, and chemical synthesis. A rotary evaporator and a vacuum pump are the two equipment required for a rotary evaporation system. Selection of the optimal vacuum pump is based on considerations such as chemical compatibility, ability to process wet vapors, ultimate depth of vacuum, flow rate, and adjustable control of vacuum levels.

How Should Evaporating Crucibles Be Handled And Maintained?

Evaporating crucibles should be handled and maintained with care to ensure their longevity and performance. Crucibles should be cleaned thoroughly before each use to remove any residual material from previous depositions. Avoid using abrasive materials that could damage the crucible's surface. During loading and unloading, handle crucibles with clean gloves or specialized tools to prevent contamination. When not in use, store crucibles in a dry and clean environment to avoid corrosion or degradation. Regular inspection of crucibles for cracks, defects, or signs of wear is important to prevent unexpected failures during the evaporation process. Follow the manufacturer's recommendations for any specific maintenance procedures, such as annealing or surface treatment, to prolong the crucible's lifespan.

What Are The Advantages Of A Rotary Evaporator?

The advantages of using a rotary evaporator include lower boiling temperatures, faster evaporation of solvents, fewer operations, and the ability to suppress bumping during the process. The lower boiling temperatures allow for the separation of solvents and compounds at lower temperatures, while faster evaporation speeds up the process. Fewer operations are needed thanks to the built-in lifting and falling motor, and bumping is suppressed, allowing for quick and gentle evaporation. Rotary evaporators are particularly useful for heat-sensitive compounds and distillation of complex mixtures.

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4.8

out of

5

I was amazed by the fast delivery of my 2L Short Path Distillation equipment. It arrived the next day after I ordered it, which allowed me to start experimenting with it right away.

Juan Jimenez

4.9

out of

5

This equipment is worth every penny. It has allowed me to perform complex distillations with ease and accuracy. The quality of the glassware is top-notch, and the system is very easy to assemble and operate.

Maria Rodriguez

4.7

out of

5

I've been using the 2L Short Path Distillation system for a few weeks now and I'm thoroughly impressed. It's incredibly well-made and durable. I've been able to use it to distill a wide variety of liquids, and it's always performed flawlessly.

Pedro Hernandez

5.0

out of

5

This distillation system is a game-changer for my laboratory. It's compact and easy to use, yet it's powerful enough to handle even the most challenging distillations. I highly recommend it to anyone who needs a reliable and efficient distillation system.

Ana Garcia

4.6

out of

5

I'm a lab manager and I recently purchased the 2L Short Path Distillation system. I'm very impressed with the quality and performance of this equipment. It's easy to use and has helped me to improve the efficiency of my experiments.

Jose Martinez

4.8

out of

5

I'm a research scientist and I recently purchased the 2L Short Path Distillation system. I'm very happy with this purchase. The equipment is well-made and easy to use. It has helped me to save time and improve the accuracy of my experiments.

Sophia Khan

4.7

out of

5

I'm a lab technician and I recently purchased the 2L Short Path Distillation system. I'm very impressed with this equipment. It's very easy to use and has helped me to improve the efficiency of my work.

Oliver Chen

4.9

out of

5

I'm a chemist and I recently purchased the 2L Short Path Distillation system. I'm very happy with this purchase. The equipment is well-made and easy to use. It has helped me to improve the quality of my research.

Isabella Perez

4.6

out of

5

I'm a lab manager and I recently purchased the 2L Short Path Distillation system. I'm very impressed with this equipment. It's easy to use and has helped me to improve the efficiency of my lab.

Benjamin Smith

4.8

out of

5

I'm a research scientist and I recently purchased the 2L Short Path Distillation system. I'm very happy with this purchase. The equipment is well-made and easy to use. It has helped me to save time and improve the accuracy of my experiments.

Emily Jones

4.7

out of

5

I'm a lab technician and I recently purchased the 2L Short Path Distillation system. I'm very impressed with this equipment. It's very easy to use and has helped me to improve the efficiency of my work.

Alexander Brown

4.9

out of

5

I'm a chemist and I recently purchased the 2L Short Path Distillation system. I'm very happy with this purchase. The equipment is well-made and easy to use. It has helped me to improve the quality of my research.

Ava Johnson

4.6

out of

5

I'm a lab manager and I recently purchased the 2L Short Path Distillation system. I'm very impressed with this equipment. It's easy to use and has helped me to improve the efficiency of my lab.

Liam White

4.8

out of

5

I'm a research scientist and I recently purchased the 2L Short Path Distillation system. I'm very happy with this purchase. The equipment is well-made and easy to use. It has helped me to save time and improve the accuracy of my experiments.

Sophia Green

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Step-by-Step Guide to Operating a Short Path Distillation Apparatus

Operating of Short Path Distillation and Precautions

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Understanding the Science Behind Short Path Distillation

Short path distillation is a precise and efficient method of separating and purifying liquids through a process of distillation.

Find out more

How to Choose the Right Rotovap for Your Distillation Needs

Rotary evaporators are commonly used in laboratories to separate solvents from a mixture through the process of evaporation.

Find out more

A Beginner's Guide to Rotovap Distillation

Rotovap distillation is a common technique used to separate solvents from reaction mixtures. It involves the use of a rotary evaporator, which is a piece of laboratory equipment that utilizes rotation and heat to remove solvents or other compounds from a sample.

Find out more

How to Use a Rotovap for Precise Distillation Results

Rotary evaporation is a common technique used in laboratories to purify and separate solvents from chemical compounds.

Find out more

A Comparison of Rotovap Distillation and Other Distillation Technologies

Distillation is a separation technique used to purify liquids through heat application and vaporization. It is a crucial process in various industries such as the chemical, pharmaceutical, and food industries. There are various distillation technologies available, each with its unique advantages and disadvantages.

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How Rotary Evaporators are Revolutionizing Distillation

Rotary evaporators, also commonly referred to as rotovaps, are laboratory equipment used for the separation of solvents from a mixture through the process of distillation.

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From Chemistry to Cooking The Versatility of Rotary Vacuum Evaporator

A rotary vacuum evaporator is a laboratory equipment that uses a rotating flask to remove solvents from a sample. It works by creating a vacuum in the system, which lowers the boiling point of the solvent and allows it to evaporate at lower temperatures.

Find out more

From Lab to Kitchen The Versatile Applications of Rotary Evaporator

A rotary evaporator, also known as a rotovap, is a laboratory device used for separating solvents from samples using evaporation. The device consists of a rotating flask and a condenser that is cooled by either air or water.

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Choosing the Right Rotary Vacuum Evaporator for Your Lab

Rotary vacuum evaporators are essential tools for any laboratory that needs to concentrate or isolate solutions. These devices work by heating a sample under vacuum to increase its surface area and effectively remove solvent.

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What Is Rotary Evaporator Used For?

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Hot Tags

short path distillation rotary evaporator evaporation crucible high purity materials

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2L Short Path Distillation

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Applications

Detail & Parts

Advantages

2L Short path distillation specifications

Warnings

Designed for You

FAQ

What Is The Short Path Distillation?

What Is The Purpose Of A Rotary Evaporator?

What Are High Purity Materials?

Is Short Path Distillation The Same As Distillation?

Why Rotary Evaporator Is Used In Solvent Extraction?

What Are Examples Of Short Path Distillation?

Can Rotary Evaporator Remove Water?

What Are The Common Materials Used For Evaporating Crucibles?

What Temperature Is Short Path Distillation?

What Are The Advantages Of Short Path Distillation?

How Long Does Short Path Distillation Take?

Is Rotary Evaporator Used For Distillation?

What Are The Advantages Of Using Evaporating Crucibles?

What Are The Principles Of Rotary Evaporation?

How Should Evaporating Crucibles Be Handled And Maintained?

What Are The Advantages Of A Rotary Evaporator?

PDF - 2L Short Path Distillation

Catalog of Short Path Distillation

Catalog of Short Path Distillation

Catalog of Rotary Evaporator

Catalog of Evaporation Crucible

Catalog of High Purity Materials

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Related Products

Related Articles

Step-by-Step Guide to Operating a Short Path Distillation Apparatus

Understanding the Science Behind Short Path Distillation

How to Choose the Right Rotovap for Your Distillation Needs

A Beginner's Guide to Rotovap Distillation

How to Use a Rotovap for Precise Distillation Results

A Comparison of Rotovap Distillation and Other Distillation Technologies

How Rotary Evaporators are Revolutionizing Distillation

From Chemistry to Cooking The Versatility of Rotary Vacuum Evaporator

From Lab to Kitchen The Versatile Applications of Rotary Evaporator

Choosing the Right Rotary Vacuum Evaporator for Your Lab

What Is Rotary Evaporator Used For?

Get More Flavor from Your Ingredients with Rotovap Distillation

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