Products Bio-Chem Equipment Short Path Distillation 2L Short Path Distillation
2L Short Path Distillation

Short Path Distillation

2L Short Path Distillation

Item Number : SPD-1

Price varies based on specs and customizations


Glassware
yes
Heating mantle
yes
Chilling circulator
yes
Vacuum pump
yes
Fittings
yes
ISO & CE icon

Shipping:

Contact us to get shipping details Enjoy On-time Dispatch Guarantee.

Applications

Short path distillation is an important technique to extract or purify target mixed liquids by the method of distillate short traveling distance. Distillation is completed under the high vacuum condition, which will create low pressure environment and lower the liquids boiling point, high at the same means that lower heating temperature. Low temperature heating will reduce the impact to the heat sensitive materials, and increase the distillation quality.

Detail & Parts

Short Path Distillation Details

Flexible choice of rotary vane vacuum oil pump.
Flexible choice of rotary vane vacuum oil pump.
Flexible choice of desktop high efficiency heater/chillers.
Flexible choice of desktop high efficiency heater/chillers.

Advantages

  • Heavy duty Borosilicate 3.3 glassware, durable use
  • Fast heating mantle with magnetic stirring function
  • Cold trap project the vacuum pump and increase service life
  • Delicate fitting device make system smoothly operating

2L Short path distillation specifications

Glassware Glass material High borosilicate glass 3.3
Flask volume 2L
Receiver flask 3*500ml
Cold trap Dry ice type condensor
Heating mantle Heating power 650W
Temperature range RT-380℃
Thermometer PT100
Stirring method Magnetic
Stirring power 40W
Stirring speed 50-2000RPM
Chilling circulator Temperature range -10-99℃
Reserver volume 6L/180*160*150mm
Pump flowrate 4L/Min
Vacuum pump Pump type Dual stage rotary vane pump
Pumping rate 1.1L/S at 50HZ; 1.3L/S at 60HZ
Ultimate pressure 3Pa
Power rating 400/370kW
Net weight 19kg
Fittings Supportor 150*150mm SS jack with cork ring
Vacuum piping Silicon hose
Keck clamp SS/Plastic
Thermometer Range 0-200℃ with 30cm length

Warnings

Operator safety is the top important issue! Please operate the equipment with cautions. Working with inflammable& explosive or toxic gases is very dangerous, operators must take all necessary precautions before starting the equipment. Working with positive pressure inside the reactors or chambers is dangerous, operator must fellow the safety procedures strictly. Extra caution must also be taken when operating with air-reactive materials, especially under vacuum. A leak can draw air into the apparatus and cause a violent reaction to occur.

Designed for You

KinTek provide deep custom made service and equipment to worldwide customers, our specialized teamwork and rich experienced engineers are capable to undertake the custom tailoring hardware and software equipment requirements, and help our customer to build up the exclusive and personalized equipment and solution!

Would you please drop your ideas to us, our engineers are ready for you now!

FAQ

What is the short path distillation?

Short path distillation is a purification technique that separates compounds based on their volatilities in a boiling liquid mixture under reduced pressure. It involves the distillate traveling a short distance, often only a few centimeters, and is done at reduced pressure. Short path distillation is ideal for laboratory applications where minimal instrumentation footprint is crucial. The boiling temperature is reduced by lowering the operating pressure, making it a continuous process with very short residence time. It is often used for unstable compounds or to purify small amounts of compounds, achieving distillate purity levels of up to 99%.

What is the purpose of a rotary evaporator?

The purpose of a rotary evaporator, or rotovap, is to distill a solvent to separate a given mixture into its components based on their respective volatilities, through the process of evaporation and condensation. The rotovap is used to concentrate non-volatile components in a mixture and to extract volatile aroma and flavor molecules from mixtures gently and at low temperatures. The two key components of the rotovap allow for a gentle, precise, and efficient distillation not found in conventional distilling apparatuses: vacuum removal of solvent to lower boiling point and rotary flask rotation to increase surface area and speed up distillation.

What are high purity materials?

High purity materials refer to substances that are free from impurities and possess a high level of chemical homogeneity. These materials are essential in various industries, particularly in the field of advanced electronics, where impurities can significantly affect the performance of devices. High purity materials are obtained through various methods, including chemical purification, vapor-phase deposition, and zone refining. In the preparation of electronic grade single crystal diamond, for example, a high-purity raw material gas and an efficient vacuum system are necessary to achieve the desired level of purity and homogeneity.

Is short path distillation the same as distillation?

Short path distillation is a type of distillation technique used to separate and purify small amounts of compounds that are not stable at high temperatures. It involves the distillate traveling a short distance, often only a few centimeters, at reduced pressure. While short path distillation is a specific type of distillation, it is not the same as traditional distillation, which typically involves heating a mixture to its boiling point and condensing the vapors. Short path distillation allows for a lower heating temperature and a shorter distillation distance, resulting in less loss of compound and more efficient purification.

Why rotary evaporator is used in solvent extraction?

Rotary evaporators are used in solvent extraction because they allow for the efficient and gentle removal of solvents from samples by evaporation. This is achieved by reducing the pressure to lower the solvent boiling point, rotating the sample to increase the effective surface area, heating the solution, and then condensing the evaporated solvent in a cooled glass condenser. This process leaves the concentrated compound in the flask and is often used in medicinal chemistry, pharmaceutical, chromatography, and petrochemical fields.

What are examples of short path distillation?

Some examples of short path distillation include processing edible oils, creating fragrances, producing fuels, distilling polyurethane, distilling compounds that are unstable at high temperatures, and distilling small quantities of a compound.

Can rotary evaporator remove water?

Yes, a rotary evaporator can remove water. By changing the temperature to speed up the evaporation rate or by vacuuming with a vacuum pump to further reduce the pressure and lower the boiling point, a rotary evaporator can evaporate solutions that contain water and other substances. The electronic control of the rotary evaporator keeps the rotation of the flask at a constant speed, creating a larger surface area for heating and faster evaporation speeds. The traditional distillation method is less efficient and accurate than a rotary evaporator, which is widely used in chemical laboratories, industrial, bio-pharmaceutical, and food-making fields.

What are the common materials used for evaporating crucibles?

Evaporating crucibles are commonly made from materials such as tungsten, tantalum, molybdenum, graphite, or ceramic compounds. These materials have high melting points and good thermal conductivity, making them suitable for the high-temperature conditions required during evaporation. The choice of crucible material depends on factors such as the evaporant material, desired film properties, and process parameters.

What temperature is short path distillation?

The Short Path Vacuum Distillation operates at a temperature far below the boiling point of the material being distilled, allowing for the purification of heat-sensitive materials at much lower temperatures. The ultimate pressures of 0.001 mbar can be achieved, which prevents degradation and allows for very high equivalent temperatures to be achieved at ambient pressure. The high vacuum distillation technique enables the separation of heat-sensitive or high molecular weight compounds not possible by conventional techniques.

What are the advantages of short path distillation?

Short path distillation has several advantages over other distillation processes. It offers a continuous feed functionality, faster completion time, and is ideal for compounds that are unstable at high temperatures. It is also automated and easy to use, produces high concentrations of distillates, and reduces product waste. These benefits make short path distillation a highly advantageous option for a variety of uses and applications, especially in industries with time-sensitive materials and production cycles.

How long does short path distillation take?

The length of time it takes to complete short path distillation depends on various factors, such as the type and quantity of the compound being distilled, the equipment used, and the skill of the operator. Generally, short path distillation is a relatively quick process, with some runs taking as little as 30 minutes, while others may take several hours. The key to a successful distillation is to carefully monitor the temperature and pressure throughout the process and adjust as necessary to ensure maximum efficiency and purity of the end product.

Is rotary evaporator used for distillation?

Yes, rotary evaporator is used for distillation. It is a device used in chemical laboratories to efficiently and gently remove solvents from samples by evaporation. The system works by reducing the pressure to lower the solvent boiling point, rotating the sample to increase the effective surface area, heating the solution, and then the evaporated solvent condenses in a cooled glass condenser. Rotary evaporation is most often and conveniently applied to separate "low boiling" solvents such as n-hexane or ethyl acetate from compounds which are solid at room temperature and pressure.

What are the advantages of using evaporating crucibles?

Evaporating crucibles offer several advantages in thin film deposition processes. They provide a controlled environment for the evaporation of materials, allowing for precise control over film thickness and uniformity. Crucibles can withstand high temperatures and provide efficient heat transfer, ensuring consistent evaporation rates. They are available in various sizes and shapes to accommodate different evaporation systems and substrate configurations. Evaporating crucibles also allow for the deposition of a wide range of materials, including metals, semiconductors, and ceramics. They can be easily loaded and unloaded, facilitating quick material changes or process adjustments. Overall, evaporating crucibles are essential tools in thin film deposition techniques, offering versatility, reliability, and reproducibility.

What are the principles of rotary evaporation?

The basic principle of rotary evaporation is to increase a sample's surface area and optimize its temperature and vacuum level, enabling effective separation of solvents in a short time. A cooling condenser helps to recover the separated solvent. It is a gentle and efficient method for liquid separation and purification, with specific applications including concentration, crystallization, solvent distillation, and chemical synthesis. A rotary evaporator and a vacuum pump are the two equipment required for a rotary evaporation system. Selection of the optimal vacuum pump is based on considerations such as chemical compatibility, ability to process wet vapors, ultimate depth of vacuum, flow rate, and adjustable control of vacuum levels.

How should evaporating crucibles be handled and maintained?

Evaporating crucibles should be handled and maintained with care to ensure their longevity and performance. Crucibles should be cleaned thoroughly before each use to remove any residual material from previous depositions. Avoid using abrasive materials that could damage the crucible's surface. During loading and unloading, handle crucibles with clean gloves or specialized tools to prevent contamination. When not in use, store crucibles in a dry and clean environment to avoid corrosion or degradation. Regular inspection of crucibles for cracks, defects, or signs of wear is important to prevent unexpected failures during the evaporation process. Follow the manufacturer's recommendations for any specific maintenance procedures, such as annealing or surface treatment, to prolong the crucible's lifespan.

What are the advantages of a rotary evaporator?

The advantages of using a rotary evaporator include lower boiling temperatures, faster evaporation of solvents, fewer operations, and the ability to suppress bumping during the process. The lower boiling temperatures allow for the separation of solvents and compounds at lower temperatures, while faster evaporation speeds up the process. Fewer operations are needed thanks to the built-in lifting and falling motor, and bumping is suppressed, allowing for quick and gentle evaporation. Rotary evaporators are particularly useful for heat-sensitive compounds and distillation of complex mixtures.
View more faqs for this product

4.8

out of

5

I was amazed by the fast delivery of my 2L Short Path Distillation equipment. It arrived the next day after I ordered it, which allowed me to start experimenting with it right away.

Juan Jimenez

4.9

out of

5

This equipment is worth every penny. It has allowed me to perform complex distillations with ease and accuracy. The quality of the glassware is top-notch, and the system is very easy to assemble and operate.

Maria Rodriguez

4.7

out of

5

I've been using the 2L Short Path Distillation system for a few weeks now and I'm thoroughly impressed. It's incredibly well-made and durable. I've been able to use it to distill a wide variety of liquids, and it's always performed flawlessly.

Pedro Hernandez

5.0

out of

5

This distillation system is a game-changer for my laboratory. It's compact and easy to use, yet it's powerful enough to handle even the most challenging distillations. I highly recommend it to anyone who needs a reliable and efficient distillation system.

Ana Garcia

4.6

out of

5

I'm a lab manager and I recently purchased the 2L Short Path Distillation system. I'm very impressed with the quality and performance of this equipment. It's easy to use and has helped me to improve the efficiency of my experiments.

Jose Martinez

4.8

out of

5

I'm a research scientist and I recently purchased the 2L Short Path Distillation system. I'm very happy with this purchase. The equipment is well-made and easy to use. It has helped me to save time and improve the accuracy of my experiments.

Sophia Khan

4.7

out of

5

I'm a lab technician and I recently purchased the 2L Short Path Distillation system. I'm very impressed with this equipment. It's very easy to use and has helped me to improve the efficiency of my work.

Oliver Chen

4.9

out of

5

I'm a chemist and I recently purchased the 2L Short Path Distillation system. I'm very happy with this purchase. The equipment is well-made and easy to use. It has helped me to improve the quality of my research.

Isabella Perez

4.6

out of

5

I'm a lab manager and I recently purchased the 2L Short Path Distillation system. I'm very impressed with this equipment. It's easy to use and has helped me to improve the efficiency of my lab.

Benjamin Smith

4.8

out of

5

I'm a research scientist and I recently purchased the 2L Short Path Distillation system. I'm very happy with this purchase. The equipment is well-made and easy to use. It has helped me to save time and improve the accuracy of my experiments.

Emily Jones

4.7

out of

5

I'm a lab technician and I recently purchased the 2L Short Path Distillation system. I'm very impressed with this equipment. It's very easy to use and has helped me to improve the efficiency of my work.

Alexander Brown

4.9

out of

5

I'm a chemist and I recently purchased the 2L Short Path Distillation system. I'm very happy with this purchase. The equipment is well-made and easy to use. It has helped me to improve the quality of my research.

Ava Johnson

4.6

out of

5

I'm a lab manager and I recently purchased the 2L Short Path Distillation system. I'm very impressed with this equipment. It's easy to use and has helped me to improve the efficiency of my lab.

Liam White

4.8

out of

5

I'm a research scientist and I recently purchased the 2L Short Path Distillation system. I'm very happy with this purchase. The equipment is well-made and easy to use. It has helped me to save time and improve the accuracy of my experiments.

Sophia Green

PDF - 2L Short Path Distillation

Download

Catalog of Short Path Distillation

Download

Catalog of Short Path Distillation

Download

Catalog of Rotary Evaporator

Download

Catalog of Evaporation Crucible

Download

Catalog of High Purity Materials

Download

REQUEST A QUOTE

Our professional team will reply to you within one business day. Please feel free to contact us!

Related Products

20L Short Path Distillation

20L Short Path Distillation

Efficiently extract and purify mixed liquids with our 20L short path distillation system. High vacuum and low temperature heating for optimal results.

10L Short Path Distillation

10L Short Path Distillation

Extract and purify mixed liquids with ease using our 10L short path distillation system. High vacuum and low temperature heating for optimal results.

5L Short Path Distillation

5L Short Path Distillation

Experience efficient and high-quality 5L short path distillation with our durable Borosilicate glassware, fast heating mantle, and delicate fitting device. Extract and purify your target mixed liquids with ease under high vacuum conditions. Learn more about its advantages now!

Molecular Distillation

Molecular Distillation

Purify and concentrate natural products with ease using our molecular distillation process. With high vacuum pressure, low operating temperatures, and short heating times, preserve the natural quality of your materials while achieving excellent separation. Discover the advantages today!

wall mounted water distillation unit

wall mounted water distillation unit

The wall mounted water distillation unit can be installed on the wall and is designed to produce high-quality distilled water continuously, automatically and efficiently at low economic cost.

5-50L Rotary Evaporator for Extraction, Molecular Cooking Gastronomy and Laboratory

5-50L Rotary Evaporator for Extraction, Molecular Cooking Gastronomy and Laboratory

Efficiently separate low-boiling solvents with the 5-50L Rotary Evaporator. Ideal for chemical labs, it offers precise and safe evaporating processes.

2-5L Rotary Evaporator for Extraction, Molecular Cooking Gastronomy and Laboratory

2-5L Rotary Evaporator for Extraction, Molecular Cooking Gastronomy and Laboratory

Efficiently remove low boiling solvents with the KT 2-5L Rotary Evaporator. Perfect for chemical labs in the pharmaceutical, chemical, and biological industries.

0.5-4L Rotary Evaporator for Extraction, Molecular Cooking Gastronomy and Laboratory

0.5-4L Rotary Evaporator for Extraction, Molecular Cooking Gastronomy and Laboratory

Efficiently separate "low boiling" solvents with a 0.5-4L rotary evaporator. Designed with high-grade materials, Telfon+Viton vacuum sealing, and PTFE valves for contamination-free operation.

Rotary Vane Vacuum Pump

Rotary Vane Vacuum Pump

Experience high vacuum pumping speed and stability with our UL-certified Rotary Vane Vacuum Pump. Two-shift gas ballast valve and dual oil protection. Easy maintenance and repair.

Diaphragm Vacuum Pump

Diaphragm Vacuum Pump

Get stable and efficient negative pressure with our Diaphragm Vacuum Pump. Perfect for evaporation, distillation, and more. Low temperature motor, chemical resistant materials, and environmentally friendly. Try it today!

20L Rotary Evaporator for Extraction, Molecular Cooking Gastronomy and Laboratory

20L Rotary Evaporator for Extraction, Molecular Cooking Gastronomy and Laboratory

Efficiently separate "low boiling" solvents with the 20L Rotary Evaporator, ideal for chemical labs in pharmaceutical and other industries. Guarantees working performance with selected materials and advanced safety features.

1-5L Single Glass Reactor

1-5L Single Glass Reactor

Find your ideal glass reactor system for synthetic reactions, distillation, and filtration. Choose from 1-200L volumes, adjustable stirring and temperature control, and custom options. KinTek has you covered!

0.5-1L Rotary Evaporator for Extraction, Molecular Cooking Gastronomy and Laboratory

0.5-1L Rotary Evaporator for Extraction, Molecular Cooking Gastronomy and Laboratory

Looking for a reliable and efficient rotary evaporator? Our 0.5-1L rotary evaporator uses constant temperature heating and thin film evaporating to implement a range of operations, including solvent removal and separation. With high-grade materials and safety features, it's perfect for labs in pharmaceutical, chemical, and biological industries.

10-50L Rotary Evaporator for Extraction, Molecular Cooking Gastronomy and Laboratory

10-50L Rotary Evaporator for Extraction, Molecular Cooking Gastronomy and Laboratory

Efficiently separate low boiling solvents with KT Rotary Evaporator. Guaranteed performance with high-grade materials and flexible modular design.

Indirect cold trap chiller

Indirect cold trap chiller

Boost vacuum system efficiency and prolong pump life with our Indirect Cold Trap. Built-in chilling system with no need for fluid or dry ice. Compact design and easy to use.

80-150L Jacket Glass Reactor

80-150L Jacket Glass Reactor

Looking for a versatile jacket glass reactor system for your lab? Our 80-150L reactor offers controlled temperature, speed, and mechanical functions for synthetic reactions, distillation, and more. With customizable options and tailored services, KinTek has you covered.

Lifting/tilting Glass Reactor

Lifting/tilting Glass Reactor

Enhance your synthetic reactions, distillation, and filtration processes with our lifting/tilting glass reactor system. With a wide range of temperature adaptability, accurate stirring control, and solvent-resistant valves, our system guarantees stable and pure results. Explore the features and optional functions today!

Benchtop Water Circulating Vacuum Pump

Benchtop Water Circulating Vacuum Pump

Need a water circulating vacuum pump for your lab or small-scale industry? Our Benchtop Water Circulating Vacuum Pump is perfect for evaporation, distillation, crystallization, and more.

laboratory vacuum tilt rotary tube furnace

laboratory vacuum tilt rotary tube furnace

Discover the versatility of Laboratory Rotary Furnace: Ideal for calcination, drying, sintering, and high-temperature reactions. Adjustable rotating and tilting functions for optimal heating. Suitable for vacuum and controlled atmosphere environments. Learn more now!

Related Articles

Step-by-Step Guide to Operating a Short Path Distillation Apparatus

Step-by-Step Guide to Operating a Short Path Distillation Apparatus

Operating of Short Path Distillation and Precautions

Find out more
Understanding the Science Behind Short Path Distillation

Understanding the Science Behind Short Path Distillation

Short path distillation is a precise and efficient method of separating and purifying liquids through a process of distillation.

Find out more
How to Choose the Right Rotovap for Your Distillation Needs

How to Choose the Right Rotovap for Your Distillation Needs

Rotary evaporators are commonly used in laboratories to separate solvents from a mixture through the process of evaporation.

Find out more
A Beginner's Guide to Rotovap Distillation

A Beginner's Guide to Rotovap Distillation

Rotovap distillation is a common technique used to separate solvents from reaction mixtures. It involves the use of a rotary evaporator, which is a piece of laboratory equipment that utilizes rotation and heat to remove solvents or other compounds from a sample.

Find out more
How to Use a Rotovap for Precise Distillation Results

How to Use a Rotovap for Precise Distillation Results

Rotary evaporation is a common technique used in laboratories to purify and separate solvents from chemical compounds.

Find out more
A Comparison of Rotovap Distillation and Other Distillation Technologies

A Comparison of Rotovap Distillation and Other Distillation Technologies

Distillation is a separation technique used to purify liquids through heat application and vaporization. It is a crucial process in various industries such as the chemical, pharmaceutical, and food industries. There are various distillation technologies available, each with its unique advantages and disadvantages.

Find out more
How Rotary Evaporators are Revolutionizing Distillation

How Rotary Evaporators are Revolutionizing Distillation

Rotary evaporators, also commonly referred to as rotovaps, are laboratory equipment used for the separation of solvents from a mixture through the process of distillation.

Find out more
From Chemistry to Cooking The Versatility of Rotary Vacuum Evaporator

From Chemistry to Cooking The Versatility of Rotary Vacuum Evaporator

A rotary vacuum evaporator is a laboratory equipment that uses a rotating flask to remove solvents from a sample. It works by creating a vacuum in the system, which lowers the boiling point of the solvent and allows it to evaporate at lower temperatures.

Find out more
From Lab to Kitchen The Versatile Applications of Rotary Evaporator

From Lab to Kitchen The Versatile Applications of Rotary Evaporator

A rotary evaporator, also known as a rotovap, is a laboratory device used for separating solvents from samples using evaporation. The device consists of a rotating flask and a condenser that is cooled by either air or water.

Find out more
Choosing the Right Rotary Vacuum Evaporator for Your Lab

Choosing the Right Rotary Vacuum Evaporator for Your Lab

Rotary vacuum evaporators are essential tools for any laboratory that needs to concentrate or isolate solutions. These devices work by heating a sample under vacuum to increase its surface area and effectively remove solvent.

Find out more
What Is Rotary Evaporator Used For?

What Is Rotary Evaporator Used For?

A rotary evaporator (or rotavap/rotovap) is a device used in chemical laboratories for the efficient and gentle removal of solvents from samples by evaporation.

Find out more
Get More Flavor from Your Ingredients with Rotovap Distillation

Get More Flavor from Your Ingredients with Rotovap Distillation

Rotovap distillation is a unique and efficient method of extracting essential oils and flavors from various ingredients.

Find out more