Blog Materials Science with the Lab Vacuum Furnace
Materials Science with the Lab Vacuum Furnace

Materials Science with the Lab Vacuum Furnace

1 year ago

What is vacuum furnace?

A vacuum furnace is a specialized type of furnace that is designed to operate in a vacuum environment. This means that the furnace is sealed and the air inside is pumped out, creating a low pressure or vacuum inside.

The vacuum helps to prevent contamination of the materials being heated and also allows for precise temperature control.

There are two main types of vacuum furnaces: cold wall and hot wall. Cold wall vacuum furnaces have a water-cooled recipient that is kept cold during the heat treatment process.

The heating elements are located inside the recipient, which is sealed and pumped to create the vacuum. Hot wall vacuum furnaces, on the other hand, have heating elements located outside the vacuum recipient, typically in the form of a ceramic or quartz tube. The recipient itself is heated and the vacuum is created by pumping out the air inside.

Vacuum furnaces are commonly used in a variety of industries, including materials science, aerospace, automotive, and electronics. They are used to perform a variety of heat treatment processes, such as annealing, sintering, and brazing.

The precise temperature control and low contamination levels offered by vacuum furnaces make them ideal for these types of processes.

What applications require vacuum furnace?

There are many applications that require the use of a vacuum furnace. One common application is vacuum soldering and brazing, where the vacuum helps to prevent contamination of the materials being joined and also allows for precise temperature control. Other applications that may require a vacuum furnace include vacuum annealing, which is used to improve the mechanical properties of materials; and sintering, which is a process used to produce solid objects from a powder material by heating it to a temperature below its melting point.

In addition to these specific applications, vacuum furnaces are also used for any type of heat treatment that requires a defined, non-oxidizing atmosphere. This could include processes such as hardening, tempering, and stress relieving. The use of a vacuum furnace allows for precise control of the atmosphere during the heat treatment process, which can be important for achieving the desired results.

Vacuum furnaces can also be useful for heat treatment with a defined oxygen concentration that is different from the air composition. For example, a vacuum furnace may be used to heat treat materials in a 100% pure oxygen atmosphere. This can be useful for improving the properties of certain materials or for producing certain types of materials.

Why high temperatures required vacuum furnace?

There are several reasons why a vacuum furnace may be required for high temperature heat treatment. One reason is that the maximum temperature that can be achieved using regular resistance-type heating elements in an air/oxidizing environment is typically limited to around 1800°C. To achieve higher temperatures, a vacuum furnace must be used and a non-oxidizing atmosphere must be applied.

Another reason why a vacuum furnace may be required for high temperature heat treatment is that it allows for precise temperature control. In a vacuum environment, the heat loss to the surroundings is minimized, which makes it easier to maintain a consistent temperature within the furnace. This is especially important for high temperature heat treatment, as small variations in temperature can have a significant impact on the final properties of the material being treated.

Finally, vacuum furnaces are able to achieve much higher temperatures than regular furnaces. With resistance-type heating elements, vacuum furnaces can reach temperatures up to 3000°C. This makes them ideal for a wide range of high temperature heat treatment applications, such as melting and casting, sintering, and annealing.

What are possible atmospheres for vacuum furnaces?

There are several types of atmospheres that are possible in a vacuum furnace. The most basic atmosphere is a vacuum itself, which is created by pumping out the air inside the furnace to create a low pressure environment. Depending on the application, the vacuum level can be varied from rough vacuum to fine vacuum to high vacuum to ultra-high vacuum.

In addition to a vacuum atmosphere, it is also possible to work with various gases or gas mixtures in a vacuum furnace. Some common gases that are used in vacuum furnaces include argon, nitrogen, hydrogen, carbon monoxide, and helium. The choice of gas or gas mixture will depend on the specific requirements of the heat treatment process and the properties of the material being treated.

Types of heating elements

There are several types of heating elements that are commonly used in vacuum furnaces. In a cold wall vacuum furnace, which is a type of furnace that has a water-cooled recipient that is kept cold during the heat treatment process, the most common heating elements are made of graphite, molybdenum, or tungsten.

These materials are chosen because they have low pressures even at high temperatures, which makes them well suited for use in a vacuum environment. For example, graphite heating elements can be used to achieve temperatures up to 2200°C in a vacuum furnace, while molybdenum and tungsten heating elements can reach temperatures of 1600°C and 2200°C, respectively.

Other types of heating elements may also be used in vacuum furnaces, depending on the specific requirements of the heat treatment process and the properties of the material being treated. For example, some vacuum furnaces use induction heating or radiant heating elements to achieve high temperatures.

Kindle Tech vacuum furnace

There are a variety of different types of vacuum furnaces available, each of which is suited to different applications and requirements. Some examples of the types of vacuum furnaces offered by Kindle Tech include:

  • Vacuum chamber furnaces: These furnaces have a sealed chamber that is pumped to create a vacuum, and are used for a wide range of heat treatment applications.
  • Vacuum hood furnaces: These furnaces have a hood or enclosure that is sealed and pumped to create a vacuum, and are often used for heat treatment processes that require a defined atmosphere.
  • Bottom loading furnaces: These furnaces have a sealed chamber that is accessed from the bottom, and are often used for heat treatment processes that require the material being treated to be loaded and unloaded from the bottom.
  • Laboratory vacuum furnaces: These are smaller, benchtop furnaces that are designed for use in a laboratory setting. They are often used for research and development, or for small scale heat treatment processes.
  • Vacuum tube furnaces: These furnaces have a sealed tube that is pumped to create a vacuum, and are often used for heat treatment processes that require a defined atmosphere or precise temperature control.

All of these vacuum furnaces can be used with either a reactive gas or an inert gas, depending on the specific requirements of the heat treatment process. They are also available with a choice of metal, graphite, or ceramic insulation, and some models can be configured to safely operate at up to 3000°C on request.

Vacuum options

Our vacuum furnaces offer a range of options and features that can be tailored to meet specific requirements and applications. Some examples of options that may be available for vacuum furnaces include advanced software, data loggers, and sophisticated digital controllers. These can provide additional levels of control over the operation of the furnace and also offer complete data recording capabilities.

Other options that may be available for vacuum furnaces include different pumps, vacuum systems, and cooling systems, which can be selected to meet specific requirements. These options can help to optimize the performance of the furnace and ensure that it is well suited for the intended application.

Our vacuum furnaces are used in a variety of applications, including brazing, sintering, annealing, degassing, drying, tempering, soldering, quenching, and hardening. They are also used for metal injection moulding (MIM) and ceramic inject moulding (CIM), as well as for metallization, siliconization, carbonization, and other industrial processes.

There are several different types of vacuum furnaces available, each of which is suited to different applications. For example, vacuum hood furnaces provide the highest possible purity and are well suited for applications that require a very clean environment. Vacuum furnace models with bottom loading capabilities offer easy access to samples, while laboratory vacuum furnaces have a more compact design that is well suited for a research environment. Vacuum tube furnaces are based on the corresponding non-vacuum models, but are modified and equipped with a purpose-built vacuum unit, and are available in a range of diameters and lengths. Some models, such as the HTRH-H2, are also able to operate in a hydrogen atmosphere.

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