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Vertical tube furnace

Tube Furnace

Vertical tube furnace

Item Number : KT-VTF

Price varies based on specs and customizations


Max. temperature
1800℃
Furnace tube diameter
50 / 60 / 80 / 100 mm
Heating zone length
300 / 450 / 600 / 800 mm
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Introduction

Vertical tube furnaces are laboratory equipment used for high-temperature processing of materials under controlled atmospheric conditions. They consist of a vertically oriented quartz tube enclosed within a heating chamber, which allows for precise temperature control and uniform heat distribution. These furnaces are commonly employed for various applications, including heat treatment, quenching, annealing, crystal growth, and chemical vapor deposition (CVD) coating. With advanced features such as programmable temperature controllers, vacuum sealing capabilities, and specialized accessories for sample manipulation, vertical tube furnaces offer versatility and accuracy in materials processing. Their ability to create controlled atmospheres and achieve high temperatures makes them essential tools in research and development, materials science, and industrial applications.

Applications

Vertical tube furnaces are versatile heating devices with a wide range of applications in various industries and laboratory settings. They are particularly useful for processes that require precise temperature control and the ability to operate under vacuum or controlled gas atmospheres.

  • Gas Quenching Tests: Vertical tube furnaces are commonly used for gas quenching tests, where samples are rapidly cooled from high temperatures into a quenching medium such as ice water or oil. This allows researchers to study material phase transitions and the effects of rapid cooling on material properties.
  • Heat Treatment:  Vertical tube furnaces are used for a variety of heat treatment processes, including annealing, tempering, and stress relieving. These processes can improve the mechanical properties of materials, such as their strength, hardness, and ductility.
  • Chemical Vapor Deposition (CVD):  Vertical tube furnaces are used for CVD processes, where a thin film is deposited on a substrate by chemical reactions in a gaseous environment. This technique is commonly used in the semiconductor industry to create electronic devices.
  • Crystal Growth: Vertical tube furnaces are used for crystal growth, where crystals are grown from a molten or vapor phase. This technique is used to produce high-quality crystals for use in optics, electronics, and other applications.
  • Materials Testing: Vertical tube furnaces are used for materials testing, such as thermal conductivity measurements, melting point determinations, and phase transitions. These tests provide valuable information about the properties of materials.
  • Other Applications: Vertical tube furnaces are also used in various other applications, including:
    • Sintering
    • Brazing
    • Calcination
    • Ceramics
    • Glassworking
    • Laboratory research
    • Powders processing

Detail&Parts

1. electrostatic spraying furnace body 2. heating chamber 3. 30-segment programmable PID control 4. heating tube
1. electrostatic spraying furnace body 2. heating chamber 3. 30-segment programmable PID control 4. heating tube

 

product details

Sealing system
Sealing system
product details
1. High-temperature corundum tube: corrosion-resistant, high transmittance, high-pressure resistance, high temperature resistance up to 1700 ℃
2. Electronic digital display panel: accurate temperature control, preset multi-stage heat treatment process.
3. Alumina polycrystalline fiber hearth: high temperature resistance, long use without deformation, no cracking. 

Principle

Vertical tube furnaces operate on the principle of radiant heat transfer. The heating element, typically made of molybdenum disilicide (MoSi2) or silicon carbide (SiC), is located around the vertical tube, emitting infrared radiation that is absorbed by the sample inside. This radiation heats the sample uniformly, providing precise and efficient temperature control. The furnace's design allows for rapid heating and cooling rates, making it suitable for various applications, including material synthesis, heat treatment, and temperature measurements.

Advantages

  • Vertical or sloped positioned furnace chamber: This allows for various experiments to be conducted, including fluent bed heating, crystal pulling growth, quenching, and more.
  • Variety of mechanical functions:  These functions include sample hanging, pulling, spinning, and releasing, providing versatility in experimental setups.
  • Wide working temperature range:  Max. Temperature of up to 1800℃ enables a diverse range of applications.
  • Specialized frock equipment customization:  Adapts the furnace to specific experimental requirements.
  • Double furnace shell design:  Forced air flow between inner and outer shell maintains a low furnace surface temperature for safety.
  • PID programmable temperature control:  Excellent control accuracy and stable heating performance, with remote and centralized control options.
  • VTF Pro touch screen controller:  User-friendly program setting, data analysis, and recipe management.
  • Safety features:  Over current protection, over temperature alarming, and thermal couple detection for enhanced safety.
  • Power failure restart function:  Resumes heating program after power failure, ensuring experiment continuity.

Safety Advantage

  • Kindle Tech tube furnace owns over current protection and over temperature alarming function, furnace will turn off the power automatically once over current detected
  • Furnace build in thermal couple detecting function, furnace will stop heating and alarm will be on once thermal couple broken or failure detected
  • VTF Pro support power failure restarting function,furnace will resume the furnace heating program when power is incoming after failure

Technical specifications

Furnace model KT-VTF KT-VTF PRO
Temperature controller Digital PID controller Touch screen PID controller
Multi program preset no yes
Power failure restarting no yes
Max. temperature 1800℃
Furnace tube material High grade Quartz/ Al2O3 alumina
Furnace tube diameter 50 / 60 / 80 / 100 mm
Heating zone length 300 / 450 / 600 / 800 mm
Vacuum sealing solution SS 304 flange with solid copper seal ring
Rated vacuum pressure 0.001Pa/10E5 torr
Chamber material  Japan Al2O3 alumina fiber
Heating element Cr2Al2Mo2 wire coil/SiC/MoSi2
Thermal couple  K /S/B type
Temperature control accuracy ±1℃
Electric power supply AC110-220V,50/60HZ
Other furnace tube size and heating zone length can be customized

Standard Package

No. Description Quantity
1 Furnace 1
2 Alumina tube 1
3 Vacuum flange 2
4 Tube thermal block 2
5 Tube thermal block hook 1
6 Heat resistant glove 1
7 Operation manual 1

Optional Setup

  • In tube gases detecting and monitoring,like H2, O2 and so on
  • Independent furnace temperature monitoring and recording
  • RS 485 communication port for PC remote control and data exporting
  • Insert gases feeding flow rate control,like mass flowmeter and float flowmeter
  • Touch screen temperature controller with versatile operator friendly functions
  • High vacuum pump station setups, like vane vacuum pump,molecular pump,diffusion pump

Warnings

Operator safety is the top important issue! Please operate the equipment with cautions. Working with inflammable& explosive or toxic gases is very dangerous, operators must take all necessary precautions before starting the equipment. Working with positive pressure inside the reactors or chambers is dangerous, operator must fellow the safety procedures strictly. Extra caution must also be taken when operating with air-reactive materials, especially under vacuum. A leak can draw air into the apparatus and cause a violent reaction to occur.

Designed for You

KinTek provide deep custom made service and equipment to worldwide customers, our specialized teamwork and rich experienced engineers are capable to undertake the custom tailoring hardware and software equipment requirements, and help our customer to build up the exclusive and personalized equipment and solution!

Would you please drop your ideas to us, our engineers are ready for you now!

FAQ

What is a tube furnace?

Laboratory tube furnace is one classic external heating high temperature tube furnace, also named hot wall heating furnace.

According to the different working temperature, furnace tube material usually can be transparent quartz tubes, high purity alumina ceramic tubes and high strength metal alloy tubes.

To meet different thermal researching purposes, tube furnace can be designed with multi heating zones, so as to have a flexible control of temperature gradient in the tube working chamber; furnace tube can work with a controlled atmosphere working environment or a high vacuum working environment.

What is CVD furnace?

Chemical vapor deposition (CVD) is a technology that uses various energy sources such as heating, plasma excitation or light radiation to chemically react gaseous or vapor chemical substances on the gas phase or gas-solid interface to form solid deposits in the reactor by means of chemical reaction.To put it simply, two or more gaseous raw materials are introduced into a reaction chamber, and then they react with each other to form a new material and deposit it on the substrate surface.

CVD furnace is one combined furnace system with high temperature tube furnace unit,gases control unit, and vacuum unit, it is widely used for experiment and production of composite material preparation, microelectronics process, semiconductor optoelectronic, solar energy utilization, optical fiber communication, superconductor technology, protective coating field.

What is a rotary tube furnace?

A rotary tube furnace is a circular furnace that rotates during heat-treatment. It is designed to heat loose materials for physiochemical processing and is used for continuous materials processing. These furnaces feature a metal drum lined with refractory, which is mounted at an angle and can burn pulverized, solid, gaseous or liquid fuel into its working section. Rotary tube furnaces have a wide range of applications, including the manufacturing of materials such as alumina, vermiculite, iron ore pellets and cement clinker, as well as for oxidation and calcination processes.

How does a tube furnace work?

Tube furnace heating elements are placed surrounding the cylindrical cavity, furnace can only heat the samples in the cylindrical cavity through indirect thermal radiation, since furnace tube can prevent sample material from contacting with furnace heating elements and insulation materials, so tube furnace creates a clean isolated heat chamber and reduce risks of the sample material contaminating by the furnace.

How does CVD furnace work?

CVD furnace system consists of high temperature tube furnace unit, reacting gas source precise control unit, vacuum pump station and corresponding assembling parts.

Vacuum pump is to remove the air from the reacting tube,and make sure there is no unwanted gases inside the reaction tube, after that the tube furnace will heat the reaction tube to a target temperature, then reacting gas source precise control unit can introduce different gases with a set ratio into the furnace tube for the chemical reaction, the chemical vapor deposition will be formed in the CVD furnace.

What is a atmospheric furnace?

An atmospheric furnace is a type of laboratory equipment that provides a controlled environment for various procedures. It is designed to maintain a specific temperature and atmosphere, which is essential for completing tasks that require precision and accuracy. The furnace is sealed tightly to ensure the proper environment, and the mixture of gases used is precisely measured to achieve the desired results. This type of furnace is commonly used for bonding, curing, and heat treating of samples that are prone to oxidation in an inert atmosphere.

What types of materials can be processed in a rotary furnace?

Rotary furnaces can process a wide range of materials, including ores, minerals, metals, chemicals, and waste materials. They are commonly used for processes such as calcination, drying, roasting, and thermal decomposition. For example, rotary furnaces are utilized in the cement industry for clinker production, in the metallurgical industry for smelting and refining operations, and in the chemical industry for the production of catalysts or chemical reactions requiring heat treatment. The versatility of rotary furnaces allows them to handle different material forms, such as powders, granules, and bulk solids, making them suitable for various applications across multiple industries.

How does a rotary tube furnace work?

A rotary tube furnace is a circular furnace that rotates during heat-treatment. It burns fuel and the heating gases created flow towards the sample. The furnace features a metal drum lined with refractory, mounted at an angle. Loose materials are heated for physiochemical processing and the heat is transferred from a heat source to a rotating tube which holds the sample. Rotary tube furnaces are designed for continuous materials processing and have multiple thermal control zones. They have a wide range of applications, including the manufacture of alumina, vermiculite, iron ore pellets, and cement clinker.

What is the application for tube furnace?

Tubular furnace is mainly used in metallurgy, glass, heat treatment, lithium anode and cathode materials, new energy, abrasives and other industries, and is a professional equipment for measuring materials under certain temperature conditions.

Tube furnace features simple structure, easy operation, easy control and continuous production.

Tube furnace is also widely applied in the CVD (chemical vapor deposition) and plasma enhanced CVD systems.

Which gas is used in CVD process?

There are tremendous gas sources can be used in the CVD process, the common chemical reactions of CVD includes Pyrolysis, photolysis, reduction, oxidation, redox,so the gases involved in these chemical reactions can be used in the CVD process.

We take CVD Graphene growth for an example, the gases used in the CVD process will be CH4,H2,O2 and N2.

What is the use of atmosphere furnace?

An atmosphere furnace is used in laboratories to provide a controlled environment for various processes. The furnace allows for precise temperature and atmospheric control, which is critical for procedures that require exact temperatures. The furnace is sealed tightly to ensure the proper environment for the project. The atmosphere furnace's main component is the correct mixture of gases, which is essential to the success of the project. The atmosphere furnace plays a vital role in the success of the heat-treating process. It is used to protect the material being processed or to allow the surface of the material being processed to change.

What are the rotary furnace types?

The rotary furnace types include rotary and tilting furnaces which have the ability to rotate and tilt, allowing for uniformity in drying and coating applications. KINTEK furnaces increase efficiency by offering multi-zone heating options, utilizing alumina fiber for refractory linings, and using temperature controllers. These furnaces are suitable for continuous processing and batch operations. Additionally, they can be opened up to use different tubes or reactors. The galvanized coating covered epoxy painted structure provides a longer lifetime and aesthetics. Overall, the rotary and tilting furnaces are popular for materials production, drying, aging, and oxidation processes.

What are the advantages of a rotary tube furnace?

The advantages of a rotary tube furnace include improved gas diffusion, reduced gas consumption, increased heat treatment efficiency, and improved product homogeneity. These furnaces provide an efficient way to transfer heat over a short time and continuously run batches of materials. Rotary tube furnaces can be custom designed for specific requirements, including temperature control, workspace size, residence time, tube rotation rate, and atmosphere flow rate. When choosing a tube for a rotary tube furnace, key points to consider include rotational speed, amount of material, tube diameter, suspended length, and tube thickness.

What is the function of rotary tube furnace?

The function of a rotary tube furnace is to heat loose materials for physiochemical processing. The furnace features a rotating tube that holds the sample and applies heat in multiple thermal control zones. Heating gases created by burning fuel flow towards the sample through the furnace. Rotary tube furnaces are used for manufacturing materials such as alumina, vermiculite, iron ore pellets, and cement clinker, as well as for oxidation and calcination processes. These furnaces can be made of ceramic, quartz, or high-temperature alloy and can be built with a wide temperature range for various applications.

How many different types tube furnace?

Tube furnace can work with different mechanical functions smoothly, so there are many different types tube furnace variations for different experiment purposes, typical furnace furnaces are as below:

  • Horizontal tube furnace
  • Vertical tube furnace
  • Split tube furnace
  • Rotary tube furnace
  • Tilting tube furnace
  • Sliding tube furnace
  • Fast heating and cooling tube furnace
  • Continuous feeding and discharging tube furnace

What is the advantage of CVD system?

  • Wide range of films can be produced, metal film, nonmetal film and multi-component alloy film as required. At the same time, it can prepare high-quality crystals that are difficult to obtain by other methods, such as GaN, BP, etc.
  • The film forming speed is fast, usually several microns per minute or even hundreds of microns per minute. It is possible to simultaneously deposit large quantities of coatings with uniform composition, which is incomparable to other film preparation methods, such as liquid phase epitaxy (LPE) and molecular beam epitaxy (MBE).
  • The working conditions are carried out under normal pressure or low vacuum conditions, so the coating has good diffraction, and the workpieces with complex shapes can be uniformly coated, which is much superior to PVD.
  • Due to the mutual diffusion of reaction gas, reaction product and substrate, a coating with good adhesion strength can be obtained, which is crucial for preparing surface strengthened films such as wear-resistant and anti-corrosion films.
  • Some films grow at a temperature far lower than the melting point of the film material. Under the condition of low temperature growth, the reaction gas and reactor wall and impurities contained in them almost do not react, so a film with high purity and good crystallinity can be obtained.
  • Chemical vapor deposition can obtain a smooth deposition surface. This is because compared with LPE, chemical vapor deposition (CVD) is carried out under high saturation, with high nucleation rate, high nucleation density, and uniform distribution on the whole plane, resulting in a macroscopic smooth surface. At the same time, in chemical vapor deposition, the average free path of molecules (atoms) is much larger than LPE, so the spatial distribution of molecules is more uniform, which is conducive to the formation of a smooth deposition surface.
  • Low radiation damage, which is a necessary condition for manufacturing metal oxide semiconductors (MOS) and other devices

How does an atmosphere furnace work?

An atmosphere furnace works by heating materials or components in a controlled environment to achieve specific heat treatment or processing objectives. The furnace chamber is designed to accommodate the desired materials and can be sealed to maintain the selected atmosphere. The atmosphere is typically controlled by introducing specific gases or gas mixtures into the chamber, either continuously or intermittently, to create the desired environment. The furnace is equipped with heating elements, insulation, and temperature control systems to achieve and maintain the desired temperature. The materials or components are placed within the furnace chamber, and the furnace is heated to the desired temperature and held for the required duration to achieve the desired heat treatment or processing effect.

What are the advantages of rotor furnace?

Rotary tube furnaces offer several advantages over static processes. The continuous movement of the sample ensures that the entire surface area is exposed to the atmosphere during processing which improves gas diffusion, reduces gas consumption and increases heat treatment efficiency. Additionally, the material is continuously passed through a hot furnace that is maintaining a consistent temperature profile, improving product homogeneity. Rotary furnaces also offer significant advantages of throughput and energy efficiency over other forms of continuous, high temperature equipment, making them the latest technology for high-temperature processing of powdered materials.

What are the advantages of rotary tube furnace?

Rotary tube furnaces offer efficient heat transfer over a short period, continuously processing batches of material while minimizing material handling. The furnace's continuous movement exposes the entire sample surface to the atmosphere, improving gas diffusion and reducing gas consumption to increase heat treatment efficiency.

What are the advantages of using a tube furnace?

Tube furnaces offer several advantages for high-temperature applications. Firstly, they provide precise and uniform temperature control, allowing for accurate and repeatable heating processes. This is crucial for materials research and heat treatment applications where temperature consistency is essential. Secondly, tube furnaces have a compact design, making them suitable for use in limited laboratory or industrial spaces. They are also versatile and can accommodate a wide range of sample sizes and shapes. Additionally, tube furnaces are energy-efficient, as they typically have good insulation and can reach high temperatures quickly. Some models also offer programmable temperature profiles, allowing for automated heating and cooling cycles. Overall, tube furnaces enable efficient and controlled high-temperature processes in various scientific and industrial fields.

What does PECVD stand for?

PECVD is a technology that uses plasma to activate reaction gas, promote chemical reaction on the surface of substrate or near surface space, and generate solid film. The basic principle of plasma chemical vapor deposition technology is that under the action of RF or DC electric field, the source gas is ionized to form a plasma, the low-temperature plasma is used as the energy source, an appropriate amount of reaction gas is introduced, and the plasma discharge is used to activate the reaction gas and realize chemical vapor deposition.

According to the method of generating plasma, it can be divided into RF plasma, DC plasma and microwave plasma CVD, etc...

What are the advantages of using atmosphere furnaces?

Atmosphere furnaces offer several advantages for heat treatment and processing applications. The controlled atmosphere within the furnace allows for precise control over the material's surface chemistry and microstructure, resulting in improved mechanical properties or desired surface characteristics. The ability to create specific atmospheres, such as oxidizing, reducing, or inert, provides flexibility in achieving different heat treatment objectives. Atmosphere furnaces enable the processing of a wide range of materials, including metals, alloys, ceramics, and composites, allowing for diverse applications across various industries. The controlled environment within the furnace also helps prevent oxidation or decarburization of the materials during heating, ensuring consistent and reliable results. Additionally, atmosphere furnaces can be equipped with advanced temperature control and automation systems, enhancing process repeatability, efficiency, and productivity.

What is the efficiency of a rotary furnace?

Rotary tube furnaces are highly efficient in transferring heat over a short period of time while continuously running batches of materials. They also minimize material handling, making them ideal for powder processing. KINTEK offers custom-designed rotary tube furnaces that can be built to specific requirements for maximum temperature control, workspace size, residence time, tube rotation rate, tube inclination angle, temperature profile, atmosphere flow rate, powder bed depth, and feed rate. When choosing a tube for the furnace, key considerations include rotational speed, amount of material, tube diameter, suspended length, and tube thickness. The choice of tube material should also be based on potential applications.

What safety precautions should be taken when using a tube furnace?

When using a tube furnace, it is important to follow safety precautions to prevent accidents and ensure operator and sample safety. Firstly, proper training should be provided to personnel operating the furnace to ensure they understand its operation, safety features, and emergency procedures. Secondly, appropriate personal protective equipment (PPE), such as heat-resistant gloves, goggles, and lab coats, should be worn to protect against burns and potential hazards. Thirdly, it is crucial to properly load the sample or material inside the furnace, ensuring it is securely positioned and does not obstruct airflow. Adequate ventilation should be provided to remove any potential gases or fumes generated during heating. It is also important to regularly inspect and maintain the furnace, including checking the heating elements and electrical connections, to ensure safe and reliable operation.

What is the difference between CVD and PECVD?

The difference between PECVD and traditional CVD technology is that the plasma contains a large number of high-energy electrons, which can provide the activation energy required in the chemical vapor deposition process, thus changing the energy supply mode of the reaction system. Since the electron temperature in the plasma is as high as 10000K, the collision between electrons and gas molecules can promote the chemical bond breaking and recombination of the reaction gas molecules to generate more active chemical groups, while the whole reaction system maintains a lower temperature.

So compared to the CVD process, PECVD can carry out the same chemical vapor deposition process with a lower temperature.

What factors should be considered when selecting an atmosphere furnace?

Several factors should be considered when selecting an atmosphere furnace. The desired temperature range and heating rate capability of the furnace should match the requirements of the heat treatment or processing application. The furnace size and capacity should be suitable for the size and quantity of materials or components to be processed. The control and monitoring features, such as temperature control accuracy, gas flow control, and data logging capabilities, should be evaluated to ensure precise and reliable operation. The compatibility of the furnace design with the desired atmosphere and gas handling requirements should also be taken into account. Other factors to consider include safety features, maintenance requirements, and cost. It is advisable to consult with furnace manufacturers or industry experts to select the most suitable atmosphere furnace for specific application needs.

Can a rotary furnace be used for continuous production?

Yes, rotary furnaces can be used for continuous production depending on the specific application and process requirements. Continuous operation is achieved by feeding materials into the furnace at a controlled rate while maintaining a steady rotation speed. This allows for a continuous flow of processed materials out of the furnace. Rotary furnaces are often utilized in industries requiring continuous thermal treatment, such as cement production or metallurgical processes. However, it is important to ensure proper design, sizing, and integration of auxiliary equipment, such as feed systems and discharge mechanisms, to enable continuous operation effectively. Additionally, proper monitoring and control systems should be in place to maintain consistent process parameters and product quality throughout the continuous production cycle.

How can the performance of a rotary furnace be optimized?

The performance of a rotary furnace can be optimized through various means. Proper selection and control of process parameters, such as temperature, rotation speed, and residence time, are critical for achieving the desired results. Optimization can be achieved by adjusting these parameters based on the specific materials and process requirements. Regular maintenance, including cleaning, lubrication, and inspection of the furnace components, is essential to ensure optimal performance and prevent unexpected failures. Implementing advanced control systems and automation can enhance process efficiency, accuracy, and repeatability. Additionally, monitoring and analyzing process data, such as temperature profiles and energy consumption, can help identify opportunities for improvement and optimize energy efficiency. Collaboration with furnace manufacturers or process experts can provide valuable insights and recommendations for optimizing the performance of a rotary furnace.
View more faqs for this product

4.8

out of

5

I am amazed by the precision and consistency of this vertical tube furnace. It has made our research work so much more efficient.

Elvin Soto

4.9

out of

5

The build quality of this furnace is top-notch. It's evident that it's made with high-quality materials and with great attention to detail.

Alwin Howell

4.7

out of

5

The vertical design of this furnace makes it so easy to load and unload samples. It's a huge time-saver, especially when we're running multiple experiments.

Ayanna Hudson

4.8

out of

5

The temperature uniformity of this furnace is exceptional. It ensures that our samples are heated evenly and consistently, leading to accurate and repeatable results.

Gavin Chambers

4.9

out of

5

This furnace's compact footprint is a lifesaver in our small lab. It fits perfectly on our benchtop without taking up too much space.

Chloe Reyes

4.7

out of

5

The customer service from Kintek Solution was outstanding. They were always responsive and helpful, answering all of our questions promptly.

Maximus Patel

4.8

out of

5

The delivery of this furnace was incredibly fast. We received it within a few days of placing our order, which was a pleasant surprise.

Isabelle Rodriguez

4.9

out of

5

The value for money of this furnace is unbeatable. It's a high-quality piece of equipment at an affordable price.

Liam Clark

4.7

out of

5

The technological advancements incorporated into this furnace are impressive. It has features that make our research work more efficient and accurate.

Sophia Baker

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