The heat treatment for molybdenum involves several processes to enhance its properties, particularly its strength, ductility, and creep resistance. Molybdenum is sensitive to oxygen and moisture, which can cause it to become brittle and prone to cracking. Therefore, it is often alloyed with materials like titanium, copper, zirconium, and others to improve its performance. The heat treatment process typically includes sintering, forging, and machining to achieve the desired surface roughness and structural integrity.
Sintering: Molybdenum is initially processed through a sintering process, which involves heating the molybdenum powder in a controlled environment to bond the particles together without melting the entire material. This is typically done using a circulating water-cooled intermediate frequency sintering furnace, which helps in maintaining the integrity of the material. The sintering process takes about 9-10 hours.
Forging: After sintering, the molybdenum rod is subjected to forging using an air hammer with an impact force of 1000 kg. This process is repeated 30-40 times to shape and strengthen the molybdenum. Forging helps in improving the material's ductility and resistance to deformation under load.
Machining: The final step in the heat treatment of molybdenum involves machining to form grooves and finish the end face. This ensures that the molybdenum crucible achieves the desired surface roughness, which is crucial for its performance in high-temperature applications. The surface roughness typically needs to reach between Ra1.6 to Ra3.2μm.
These steps are crucial for preparing molybdenum for use in high-temperature applications such as furnaces, where it needs to withstand extreme conditions without failing. The heat treatment processes not only enhance the mechanical properties of molybdenum but also protect it from environmental factors like oxygen and moisture that could otherwise degrade its performance.
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