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Electrode polishing material

Electrochemical Consumables

Electrode polishing material

Item Number : ELMP

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$69.00 / set


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Polishing Materials for Electrodes in Electrochemical Experiments

Electrode Polishing and Testing Instructions

  1. Prepare electrode polishing materials. Remove the backing adhesive from the chamois polishing cloth and affix it to the electrode polishing plate. Pour polishing powder (1.0/0.5/0.3/0.05um) in reverse order onto the polishing cloth and moisten it with distilled water to form a paste.
  2. Place the electrode vertically on the polishing pad and polish by drawing "8" shapes, clockwise or counterclockwise circles, or horizontal strokes. It is important to ensure that the electrode is perpendicular to the polishing cloth. After polishing, rinse the electrode surface clean with distilled water.
  3. Choose cyclic voltammetry on the electrochemical workstation and test the electrode in a standard solution of potassium ferrocyanide. If the peak position difference is within 80mv, the electrode can be considered qualified.
  4. Take two clean beakers and place a dry ethanol (a) and a secondary deionized water (b) in them. Place the tested electrode in the two solutions in order (a, b) and clean it with ultrasonic waves for no more than 60 seconds. Remove the electrode and blow it dry before use.
  5. If the electrode needs modification, invert it on the electrode drying stand and apply drops.

Detail & Parts

polishing materials A
A complete set of polishing materials A (aluminum oxide powder, suede, glass base, flannelette, sampling spoon)

alumina powder, suedepolishing blockElectrode polishing materialsuede and glass basesuede and glass baseElectrode polishing material set

Disc Electrode Polishing Steps

0.05um alumina powder is the most suitable for polishing disk-shaped electrodes. However, if scratches are found on the electrode, you need to use 1.0um, 0.3um, and 0.05um alumina powder in sequence to polish the electrode. After each polishing step, check the electrode surface, which should be flat and neat. Also, use the same alumina powder for polishing. If 1.0um alumina powder cannot remove scratches, you should first use 1200-grit metallographic sandpaper to polish and then use 0.05um alumina powder. The electrode surface will have a mirror-like luster.

Nylon polishing cloth and silk velvet cloth are used with 1.0um alumina powder, and the polishing flannel (coffee-colored) is prepared for 0.3um and 0.05um alumina powder. The back of the cloth has stickiness. Tear off the covering layer on the stickiness and press the polishing cloth tightly onto the dry and clean glass pad. Ensure that there are no bubbles between the glass pad and the polishing cloth. Before polishing, sprinkle a small amount of alumina powder on the polishing cloth and moisten it with distilled water. When polishing, hold the electrode vertically and steadily (not too hard). If the polishing cloth becomes dry, add distilled water and continue polishing.

Before using smaller alumina powder, thoroughly clean the electrode and wash your hands with water. If you accidentally sprinkle large powder on the small powder polishing cloth, you will not achieve the effect that small powder can achieve. Be careful when holding dry powder. Do not put large powder into small powder bottles. Do not exchange powder bottle caps at will. Use different spoons for different bottles when taking alumina powder from the bottle.

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FAQ

What are the materials used in electrochemical cell?

The materials used in an electrochemical cell are the anode, cathode, and electrolyte. The anode is the negative electrode that releases electrons to the external circuit and oxidizes during the electrochemical reaction. The cathode is the positive electrode that acquires electrons from the external circuit and is reduced during the electrochemical reaction. The electrolyte is the medium that provides the ion transport mechanism between the cathode and anode of a cell. The desirable properties for anode, cathode, and electrolyte materials include high efficiency, stability, good conductivity, ease of fabrication, and low cost.

What is rotating disk electrode used for?

Rotating disk electrode (RDE) is a hydrodynamic working electrode used in electrochemical applications such as corrosion studies, fuel cell research, catalyst development, and controlling mass transport of reactants to the electrode surface. It is used when defined mass transport to the sample electrode is desired. The disk's rotation induces a constant flux of analyte to the electrode, making it ideal for investigating different electrochemical phenomena such as multi-electron transfer, kinetics of slow electron transfer, adsorption/desorption steps, and electrochemical reaction mechanisms. In analytical chemistry, RDE is used in three-electrode systems for hydrodynamic voltammetry to investigate reaction mechanisms related to redox chemistry.

What are the examples of electrochemical material?

Examples of electrochemical materials include anode materials for the oxidation of acetic acid, cathode materials for the reduction of acrylonitrile, and electrode materials for the cathodic hydrodimerization of formaldehyde to ethylene glycol. Selectivity for synthetic electrochemical reactions can be determined by the materials used, with electrode materials imparting control and variation of outcomes. The choice of electrode material can also switch reactivity on or off, such as with the cathodic hydrodimerization of formaldehyde only occurring with mercury or carbon cathodes. Understanding the influence of electrode materials can facilitate improved rationalization of differences in achieved yields or selectivity.

What is the rotating electrode method?

The rotating electrode method is a technique used in electrochemical applications such as fuel cell research, corrosion studies, catalyst development, and controlling mass transport of reactants to the electrode surface. It involves using a rotating disk electrode (RDE) that rotates during experiments, inducing a constant flux of analyte to the electrode. The RDE can quickly achieve conditions in which the steady-state current is controlled by the solution flow rather than diffusion. By running experiments at various rotation rates, different electrochemical phenomena can be investigated, including multi-electron transfer, adsorption/desorption steps, and electrochemical reaction mechanisms.

What is the rotating ring-disk electrode method?

The rotating ring-disk electrode (RRDE) is a double working electrode used in analytical chemistry for hydrodynamic voltammetry. It is designed for investigating reaction mechanisms related to redox chemistry and other chemical phenomena. The RRDE has a disk electrode at its center and a ring electrode around the disk. The system takes advantage of the laminar flow created during rotation, allowing for controlled contact of the solution with the disk and ring electrodes. By varying the rate of rotation, it is possible to determine the rate of the chemical reaction and investigate different electrochemical phenomena.

What are the advantages of rotating disc electrode?

The advantages of rotating disk electrodes (RDE) include the ability to control mass transport of reactants to the electrode surface, achieve laminar flow of solution towards and across the electrode, and investigate different electrochemical phenomena such as multi-electron transfer and electrochemical reaction mechanisms. RDEs are commonly used in electrochemical applications such as corrosion studies, fuel cell research, and catalyst development. The base rotation rate of RDEs can be manually adjusted, and the electrode rotation rate can be precisely controlled with an electric motor. RDEs are a powerful tool for investigating reaction mechanisms related to redox chemistry and other chemical phenomena.
View more faqs for this product

4.9

out of

5

These polishing materials greatly enhance the quality of my experiments. The electrodes are polished to a mirror-like finish, resulting in more accurate and reproducible results.

Lucas Esteban

4.7

out of

5

I've been using these materials for a few months now and am thoroughly impressed with their durability. They last much longer than other brands I've tried, saving me both time and money.

Oliver Clark

4.8

out of

5

The polishing materials are incredibly easy to use. The instructions are clear and concise, making the process hassle-free. I highly recommend these materials to anyone looking for a reliable and efficient way to polish their electrodes.

Amelia Harrison

4.6

out of

5

The fast delivery of these materials was a lifesaver. I needed them urgently for a project and was thrilled when they arrived the next day. The quality is excellent, and I'm very satisfied with my purchase.

Jack Miller

4.9

out of

5

These polishing materials are worth every penny. They produce a superior finish on my electrodes, and I've noticed a significant improvement in the performance of my electrochemical experiments.

Isabella Garcia

4.7

out of

5

I'm very impressed with the technological advancements in these polishing materials. They're designed to minimize contamination and ensure the highest level of accuracy in my experiments. Highly recommended!

Benjamin White

4.8

out of

5

These materials are an absolute game-changer for my lab. They've streamlined our electrode polishing process, saving us valuable time and resources. The results are consistently excellent, and we're thrilled with the investment.

Ava Johnson

4.6

out of

5

I've been using these polishing materials for over a year now, and they've never let me down. They're incredibly durable and maintain their effectiveness even after multiple uses. Highly recommend!

Liam Brown

4.9

out of

5

These polishing materials are a must-have for any electrochemist. They're incredibly easy to use, and the results are consistently outstanding. I've seen a noticeable improvement in the quality of my data since switching to these materials.

Sophia Davis

PDF - Electrode polishing material

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Catalog of Electrochemical Consumables

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Catalog of Electrochemical Material

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Catalog of Rotating Disc Electrode

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