Ceramic materials, such as silicon nitride (Si3N4), are known for their unique properties, which can be significantly influenced by their density.
5 Key Insights into the Density of Ceramic Properties
1. Variation with Sintering Processes
The density of silicon nitride (Si3N4) ceramic varies depending on the sintering process and conditions.
2. Impact of Thermal Insulation Time
When prepared under air pressure, the density of Si3N4 ceramic samples increased from 3.23 g/cm³ to 3.26 g/cm³ as the thermal insulation time increased from 4 hours to 12 hours.
3. Relative Density Changes
The relative density also increased from 96.75% to 97.75% during this period. Notably, the rate of density increase was higher when the insulation time increased from 4 hours to 8 hours compared to the increase from 8 hours to 12 hours.
4. Two-Step Sintering Process
In a two-step sintering process, the relative density of Si3N4 ceramic samples was 95.5% after pre-firing at 1600°C, which increased to 98.25% after high-temperature sintering at 1800°C.
5. Liquid-Phase Sintering Mechanism
The improvement in density is attributed to the liquid-phase sintering mechanism, where sintering aids (YB2O3 and AL2O3) and SIO2 form a low-melting liquid phase that enhances particle movement, leading to a dissolving-precipitation mechanism that improves the sample's density.
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