Products Thermal Equipment Vacuum Hot Press Furnace Vacuum Hot Press Furnace Machine Heated Vacuum Press
Vacuum Hot Press Furnace Machine Heated Vacuum Press

Vacuum Hot Press Furnace

Vacuum Hot Press Furnace Machine Heated Vacuum Press

Item Number : KT-VHP

Price varies based on specs and customizations


Working temperature
1500℃ / 2200℃
Working pressure
10-400T
Press distance
100-200mm
Vacuum pressure
6x10-3Pa
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Introduction

Vacuum hot pressing furnace is a complete set of equipment that heats and pressurizes materials under vacuum or atmosphere. According to different materials and heating temperatures, heating elements can be graphite heater, molybdenum heater, and induction heating, etc; and one-way or two-way pressurization can be used for hydraulic pressurization.

Under the high temperature and high pressure and vacuum or atmosphere, the raw material solid particles are bonded with each other, the grains grow up, and the voids (pores) and grain boundaries gradually decrease;Through the transfer of materials, their total volume shrinks, and their density increases, becoming a compact polycrystalline sintered body with a specific microstructure, so that the materials can be pressed and formed.

The density, hardness and other mechanical, electronic and thermal properties of the finished materials can be significantly improved under high temperature and pressure as well as under vacuum or atmosphere

Applications

The Vacuum Tube Hot Press Furnace is a versatile and powerful tool used across various industries for high-temperature processes. This furnace, capable of operating in a vacuum or controlled atmosphere, is particularly suited for applications requiring precise temperature control and a clean environment. Key application areas include:

  • Crystal Growth: Ideal for the synthesis and growth of various types of crystals, which are crucial in the electronics and semiconductor industries.
  • Heat Treatment: Used for the thermal processing of metals and alloys to enhance their mechanical properties, such as hardness, ductility, and strength.
  • Thin Film Deposition: Essential for the deposition of thin films in the manufacturing of electronic devices, solar cells, and optical coatings.
  • Materials Science Research: Widely used in laboratories for research on new materials, including ceramics, composites, and advanced alloys.
  • Metallurgy: Helps in the purification and alloying of metals, as well as in the production of refractory materials.
  • Electronics Manufacturing: Critical for processes like annealing, sintering, and the production of electronic components.
  • Chemical Industry: Utilized for high-temperature chemical reactions and the synthesis of chemicals under controlled atmospheres.
  • Glass Manufacturing: Useful in the production of specialty glasses and the modification of glass properties through heat treatment.
  • Special Materials Production: Involved in the creation of materials with unique properties, such as those used in aerospace and defense.
  • Academic and Research Institutions: A staple in university laboratories and research centers for advanced materials research and development.

Detail & Parts

Vacuum hot press furnace details

  • Double shell structure with water-cooled jacket, the inner shell is made of stainless steel and has been finely polished. Housings are high quality carbon steel with anti-rust treatment or stainless steel with pad blasting.
  • The heating element adopts graphite or molybdenum wire. Heating is divided into 1-phase or 3-phase heating. The rational design of the heating element helps to improve the uniformity of the temperature in the cavity.
  • The furnace can be easily operated through the electrical control system. The temperature and pressure are controlled by PLC analog, or the sintering process is automatically completed by using a temperature and pressure programmable controller. The control system has alarm and protection functions such as water cut off, over temperature and over current.

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Graphite die
Graphite die

Principle

The Vacuum Tube Hot Press Furnace operates by heating and pressurizing materials under vacuum or atmosphere. It utilizes heating elements like graphite or molybdenum heaters and can apply one-way or two-way pressurization. This process bonds raw material particles, reduces voids, and increases density, forming a compact sintered body. The furnace is designed for various industries, ensuring precise heat treatment and material sintering.

Advantages

The Vacuum Tube Hot Press Furnace offers a plethora of advantages that make it a superior choice for various heat treatment processes and applications. Here are some of the key benefits:

  • Versatility in Heat Treatment Processes: The furnace supports a wide range of heat treatment processes, making it suitable for various materials and industries. This versatility ensures that it can meet diverse needs in material processing.
  • High-Speed Cycles with High-Pressure Gas Quench: The furnace is designed to facilitate high-speed cycles, which are essential for efficient production. The high-pressure gas quench feature enhances the cooling process, leading to faster cycle times and increased productivity.
  • Energy and Resource Efficiency: With low consumption of energy and process gases, the furnace is environmentally friendly and cost-effective. This efficiency not only reduces operational costs but also minimizes the environmental footprint.
  • Environmentally Friendly with Low Emissions: The design of the furnace ensures low emissions of process gases, making it an eco-conscious choice for industries looking to minimize their environmental impact.
  • Simple and Modular Design: The simple design of the furnace allows for easy installation and maintenance. Its modular nature means it can be fitted and adjusted to specific tasks and plant conditions, ensuring optimal performance.
  • Guaranteed Quality and Repeatable Process Resul: The furnace is engineered to deliver guaranteed quality and repeatable process results, which is crucial for industries where precision and consistency are paramount.
  • Predictive Maintenance: Advanced features such as predictive maintenance help in identifying potential issues before they escalate, ensuring minimal downtime and prolonging the lifespan of the equipment.

Structure introduction

This electric furnace has two types of graphite heating and resistance wire heating, which are suitable for sintering metal powder, inorganic non-metallic materials, etc. under vacuum and hh temperature hot pressing; of course, hot pressing sintering can also be carried out under protective atmosphere. In this way, the densification of the material can be completed, deformation can be prevented, and the grain size of the nanopowder can be suppressed.

Specification          
  • The electric furnace is heated by a vertical furnace body (pressure ranges from 5-800T, and the pressurization method is divided into one-way and two-way). The feeding and discharging methods are divided into top and side. , electronic control system and other components.
         
Furnace shell
  • The furnace shell is a double-layer water-cooled structure, the inner layer is strictly polished stainless steel, the outer layer is stainless steel sandblasting matte treatment or carbon steel anti-rust treatment, water cooling is passed between the double layers, and the furnace shell does not exceed 60 °C. The furnace cover is lifted by a mechanical mechanism, manually rotated backwards to open (one-way pressure), and a locking device is installed on the furnace cover.
Stove side
  • The side of the furnace is equipped with an observation window, a thermocouple automatic entry and exit mechanism, an infrared thermometer and a water-cooled electrode (three-phase). The automatic entry and exit of the thermoelectric cell is electric, with high and low temperature automatic switching. In order to prevent accidents caused by abnormal furnace temperature, there is also an over-temperature protection thermocouple on the side of the furnace.
The heating element
  • The heating element is made of graphite tube (or molybdenum wire), which can be divided into single-phase and three-phase heating. The rational design of the heating element improves the uniformity of the furnace temperature.
The insulation layer
  • The insulation layer is made of graphite (or graphite paper), carbon felt, etc., which has good insulation performance, and the unique structural design reduces the vacuuming time. The insulation layer of the molybdenum wire hot pressing furnace is a metal reflective screen.
The vacuum system
  • The vacuum system consists of two-stage vacuum pumps, one oil diffusion pump and one mechanical pump to complete the high and low vacuum. The vacuum valve adopts the high-vacuum baffle valve designed and produced by our company, which can realize automatic switching and control of high and low vacuum with digital display vacuum gauge and PLC.
The main circuit of the electric control system
  • The main circuit of the electric control system is low-voltage and high-current input. The electric control cabinet is made with reference to the standard cabinet of Rittal. It is humanized design. There are graphic simulation screens and buttons on the control panel. The operation is intuitive and convenient. The temperature and pressure control are controlled by imported brand programs. Instrument, the cabinet is equipped with a PLC, and the sintering process is automatically completed near the preset program. The control system has sound and light alarm functions for abnormal phenomena such as water cut-off, over-temperature, over-current, and thermocouple automatic switching failure.

Features

  • Double layer SUS304 stainless steel vacuum chamber structure, jacket cold water circulating cooling method to keep the furnace surface temperature 
  • Double column supporting structure, stable hydraulic press system,pressure can be manual control or automatic control,precise pressure regulating and maintaining
  • Advanced thermal insulation materials with low thermal conductivity and good thermal insulation effect, which can effectively isolate heat and reduce energy consumption
  • The temperature range is wide. A variety of heating elements can be selected, such as graphite, molybdenum, tungsten, induction heating, etc. The temperature can reach 2800 ℃ in a suitable protective atmosphere, which can adapt to hot pressing sintering of different materials;
  • Diversified vacuum system configuration, different vacuum degrees are selected according to the process;
  • A charging and discharging system is provided, which can be used for hot pressing sintering in vacuum environment, inert atmosphere or reducing atmosphere;
  • Humanized configuration, both manual operation and intelligent operation can be realized;
  • One furnace for multiple purposes can be used as a simple vacuum or atmosphere sintering furnace;
  • Diversified optional functional types available, vertical upper discharge, vertical side outlet discharge, one-way pressurization, two-way pressurization, etc.

Technical specifications

Working temperature 1500℃ / 2200℃
Heating element Molybdenum/Graphite
Working pressure 10-400T
Press distance 100-200mm
Vacuum pressure 6x10-3Pa
Effective working area diameter range 90-600mm
Effective working area diameter range 120-600mm

Warnings

Operator safety is the top important issue! Please operate the equipment with cautions. Working with inflammable& explosive or toxic gases is very dangerous, operators must take all necessary precautions before starting the equipment. Working with positive pressure inside the reactors or chambers is dangerous, operator must fellow the safety procedures strictly. Extra caution must also be taken when operating with air-reactive materials, especially under vacuum. A leak can draw air into the apparatus and cause a violent reaction to occur.

Designed for You

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Would you please drop your ideas to us, our engineers are ready for you now!

FAQ

What Is The Purpose Of A Vacuum Hot Press Furnace?

The purpose of a vacuum hot press furnace is to combine vacuum or atmosphere, hot pressing, and high-temperature sintering to form new materials. It can be used in the vacuum sintering of transparent ceramics, industrial ceramics, and metals, as well as the high-temperature sintering of ceramic materials such as silicon carbide and silicon nitride. Additionally, it can be used for the heat treatment of powders and compacts at a temperature lower than the melting point of the main components, which improves their strength through metallurgical combination between particles. The finished materials have improved mechanical, electronic, and thermal properties.

What Are The Advantages Of A Vacuum Hot Press Furnace?

Advantages of a vacuum hot press furnace include hot pressing sintering of metal and ceramic powders, preparation of ceramic/metal composites and intermetallic compounds, research and development of diffusion welding process, and densification hot press sintering of oxygen/nitrogen/boron/carbon compounds and their mixtures. The high temperature and pressure under vacuum or atmosphere help to bond raw materials solid particles together, decrease voids and grain boundaries, and improve the mechanical, electronic, and thermal properties of finished materials.

How Does A Vacuum Hot Press Furnace Work?

A vacuum hot press furnace is a piece of equipment that combines vacuum, hot pressing, and high-temperature sintering. It works by heating and pressurizing materials under vacuum or atmosphere to create a compact polycrystalline sintered body with improved mechanical, electronic, and thermal properties. The furnace is composed of several systems including furnace body, heating and heat preservation, temperature measurement system, vacuum system, air charging system, water cooling system, control system, and pressure system. Heating elements can be graphite heater, molybdenum heater, or induction heating, and one-way or two-way pressurization can be used for hydraulic pressurization.

What Are The Common Applications Of Vacuum Hot Press Furnaces?

Vacuum hot press furnaces have various applications in industries such as aerospace, automotive, electronics, and materials research. They are used for the production of advanced ceramics, such as ceramic matrix composites and sintered carbides, which are used in high-temperature applications. These furnaces are also utilized for the fabrication of metallic alloys, superalloys, and intermetallic compounds with tailored properties. Vacuum hot press furnaces play a crucial role in the production of diamond tools and cutting inserts, as well as in the development of advanced electronic materials and components. Additionally, these furnaces are employed in research laboratories for the synthesis and processing of novel materials with unique properties.

What Factors Should Be Considered When Selecting A Vacuum Hot Press Furnace?

When selecting a vacuum hot press furnace, several factors need to be considered. Firstly, the size and capacity of the furnace should align with the intended application and production requirements. The furnace should accommodate the size and number of samples or components to be processed. The heating and pressure capabilities of the furnace should also be evaluated to ensure they meet the desired temperature and pressure conditions. It is important to consider the level of automation and control systems available, as well as the compatibility with specific materials and processes. Additionally, the reliability, service support, and overall cost of ownership should be assessed. Consulting with manufacturers and experts in the field can help in selecting the most suitable vacuum hot press furnace for specific processing needs.
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