FTIR spectroscopy is a powerful analytical technique, but it requires careful handling to ensure safety and accuracy.
15 Essential Tips for Safe FTIR Spectroscopy
Engineering Controls
- Work in a well-ventilated area to ensure sufficient ventilation of escaping fumes.
- Put the furnace in a fume hood if it fits, or use other appropriate local exhaust ventilation in case the unit malfunctions, which can release hazardous gases into the occupied lab space.
Administrative Controls
- Furnace operators must complete safety training specific to the furnace they will work with and read the instrument’s manual thoroughly.
- Consult with the manufacturer and your PI to ensure that your planned experiments are appropriate for the unit.
- Do not overheat materials or their containers.
- Do not use containers for applications outside of the recommended temperature range.
- Attach an external temperature controlled power circuit that would cut the power to the unit in the event of elevated temperatures.
- Keep the furnace’s wiring tidy and away from other heat-generating sources.
- Do not disable safety features.
- Do not heat a furnace to its maximum temperature.
- Do not heat samples or glassware with chemicals that pose respiratory hazards unless the units are contained in a fume hood or provided with other appropriate local exhaust.
- Keep the area around the furnace decluttered.
- Always place and remove items from the furnace with thermal-rated tongs or forceps.
- Regularly inspect furnace for any loose or damaged wiring, water, and heat damage, or other visual defects.
- Dispose of furnace units that are beyond their usable lifetime.
Personal Protective Equipment (PPE)
- Always wear long pants, closed-toe shoes, a lab coat, and safety glasses when working with a furnace.
- Always wear the appropriate thermal gloves and regularly check them for rips, holes, or tears.
- Heat- or flame-resistant gloves are required when using furnaces at higher temperatures.
General Rules for Usage of Equipment
- Conduct a careful examination of glassware prior to using it with pressure.
- Consider working behind a blast shield or fume hood sash to protect the head and body.
- Wear protective gloves and arm sleeves.
- Use a tool to be farther from glass reactors.
These precautions ensure the safety of the operator, prevent equipment damage, and maintain the accuracy of the experiment during FTIR spectroscopy.
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